Tetrachloropropene Basic information Product Name: Tetrachloropropene Synonyms: Tetrachloropropene;1,1,2,3-Tetrachloropropene;1,1,2,3-tetrachloro-1-propen;1,1,2,3-t
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inquiryTetrachloropropene Chemical Properties Boiling point 141.38°C (rough estimate) density 1.5500 refractive index 1.5121 (estimate) EPA Substance Registry System 1,1,2,3-Tetrachloropropene (10436-39-2)
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inquiryTetrachloropropene CAS NO.10436-39-2 Application:Tetrachloropropene CAS NO.10436-39-2
1,1,2,2,3-pentachloropropane
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
With sodium hydroxide; cetylpyridinium bromide at 130℃; for 2h; | 97% |
With potassium hydroxide | |
With sodium hydroxide |
1,1,1,2,2,3-hexachloropropane
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
With hydrogenchloride; zinc In 1,4-dioxane; water at 45℃; for 49h; Autoclave; Inert atmosphere; | 90% |
1,1,1,3-tetrachloropropane
A
1,1,1,2,3-pentachloro-propane
B
3,3-dichloroallyl chloride
C
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
With iron(III) chloride; chlorine at 82℃; under 1277.21 Torr; for 15.33h; Product distribution / selectivity; | A 82.9% B 3.4% C 8.1% |
1,1,1,2,3-pentachloro-propane
A
1,1,2,3-Tetrachloropropene
B
2,3,3,3-tetrachloropropene
Conditions | Yield |
---|---|
With potassium hydroxide at 0℃; | |
With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h; | |
With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h; | |
With potassium hydroxide; Aliquat 336 In water at 8℃; for 3h; |
2,3,3,3-tetrachloropropene
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
at 180℃; | |
With aluminium trichloride at 0℃; | |
With antimonypentachloride | |
at 150 - 180℃; |
methanol
2,3,3-trichloro-2-propen-1-ol
A
methyl 2-chloroacrylate
B
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
With sulfuric acid; water 1) 105 deg C, 4 h, 2) 30 min; Yield given. Multistep reaction. Yields of byproduct given; |
1,1,1,2,3-pentachloro-propane
A
3,3,3-trichloro-1-propene
B
1,1,2,3-Tetrachloropropene
Conditions | Yield |
---|---|
at 400℃; under 750.075 Torr; for 0.0130556h; Inert atmosphere; |
1,1,1,2,3-pentachloro-propane
A
2,3-dichloro-3,3-difluoroprop-1-ene
B
1,1,2,3-Tetrachloropropene
C
1,1,2,3-tetrachloro-1-fluoro-propane
Conditions | Yield |
---|---|
With hydrogen fluoride at 290℃; under 750.075 Torr; for 3h; Inert atmosphere; tubular reactor; |
Conditions | Yield |
---|---|
Stage #1: prop-1-yne With chlorine at 60 - 80℃; Stage #2: With chlorine; dibenzoyl peroxide at 40 - 50℃; Stage #3: With sodium hydroxide at 40 - 50℃; |
Conditions | Yield |
---|---|
at 100 - 450℃; under 1018.63 Torr; Temperature; Reagent/catalyst; Pressure; Inert atmosphere; | 8.1 %Spectr. |
1,1,1,2,3-pentachloro-propane
A
2-chloro-1,1,1-trifluoropropene
B
1,1,1-trifluoropropylene
C
1,1,2,3-Tetrachloropropene
D
2,3,3,3-tetrachloropropene
E
2,3,3-trichloro-3-fluoro-propene
Conditions | Yield |
---|---|
With hydrogen fluoride at 350℃; under 750.075 Torr; Temperature; | A 77 %Chromat. B 11 %Chromat. C 42.7 %Spectr. D 22.3 %Spectr. E 6.6 %Spectr. |
1,1,1,2,3-pentachloro-propane
A
2-chloro-1,1,1-trifluoropropene
B
1,1,1-trifluoropropylene
C
1,1,2,3-Tetrachloropropene
D
2,3,3-trichloro-3-fluoro-propene
E
1,1,2,3-tetrachloro-1-fluoro-propane
Conditions | Yield |
---|---|
With hydrogen fluoride at 275℃; under 750.075 Torr; | A 80 %Chromat. B 13 %Chromat. C 53.3 %Spectr. D 6.9 %Spectr. E 6.9 %Spectr. |
1,1,2,3-Tetrachloropropene
hexamethylenetetramine
Conditions | Yield |
---|---|
In chloroform at 60℃; for 12h; | 99.6% |
piperazine
1,1,2,3-Tetrachloropropene
N,N'-bis(1,2,2-trichloroallyl)piperazine
Conditions | Yield |
---|---|
In isopropyl alcohol at 90 - 95℃; for 4h; | 86.8% |
1,3-dioxolane-4-methanol
1,1,2,3-Tetrachloropropene
4-(2,3,3-Trichloro-allyloxymethyl)-[1,3]dioxolane
Conditions | Yield |
---|---|
With potassium hydroxide; 18-crown-6 ether for 4h; Ambient temperature; | 80% |
1,1,2,3-Tetrachloropropene
dithiobenzoic acid triethylammonium salt
dithiobenzoic acid β,γ,γ-trichloroallyl ester
Conditions | Yield |
---|---|
In acetone | 78% |
1,1,2,3-Tetrachloropropene
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride; chlorine; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In 1,1,2-trichloro-2,2-difluoroethane at 132.1℃; under 6000.6 Torr; Product distribution / selectivity; | 72.6% |
With hydrogen fluoride; diisopropylamine; chromium(III) oxide at 200 - 300℃; under 760.051 Torr; for 0.000569444 - 0.00277778h; Product distribution / selectivity; | |
With methoxyhydroquinone; hydrogen fluoride; chromium(III) oxide at 243 - 254℃; under 760.051 Torr; for 66.75h; Product distribution / selectivity; |
aminoethylpiperazine
1,1,2,3-Tetrachloropropene
N-(1,1,2-trichloroallyl)-N'-(β-1,2,2-trichloroallylaminoethyl)piperazine
Conditions | Yield |
---|---|
In isopropyl alcohol Heating; | 70% |
1,1,2,3-Tetrachloropropene
sodium thiophenolate
phenyl-(2,3,3-trichloro-allyl)-sulfide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 70% |
1,1,2,3-Tetrachloropropene
1,5-diamino-3-azapentane
N,N'-bis(1,2,3-trichloroallyl)diethylenetriamine
Conditions | Yield |
---|---|
In isopropyl alcohol Heating; | 65% |
1,1,2,3-Tetrachloropropene
1,1,1,2,3-pentafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 150℃; under 47821.8 Torr; for 8h; Product distribution / selectivity; | 59% |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-1,1,1,2-tetrafluoropropane
C
1,1,1,2,3-pentafluoropropane
D
2,3-dichloro-1,1,1-trifluoropropane
E
1-chloro-2,3,3,3-tetrafluoropropane
F
2-chloro-1,1,1,3-tetrafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 100 - 125℃; under 33082.7 - 39185.2 Torr; for 12h; Product distribution / selectivity; | A n/a B n/a C 53% D n/a E n/a F n/a |
p-cresol
1,1,2,3-Tetrachloropropene
4-methyl-2-(2,3,3-trichloro-2-propenyl)phenol
Conditions | Yield |
---|---|
31% |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-2,3,3-trifluoro-butane
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride; chlorine; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In 1,1,2-trichloro-2,2-difluoroethane at 133.2℃; under 6000.6 Torr; Product distribution / selectivity; | A 25.5% B 6.6% |
1,1,2,3-Tetrachloropropene
sodium methylate
methyl-(2,3,3-trichloro-allyl)-ether
Conditions | Yield |
---|---|
With methanol |
Conditions | Yield |
---|---|
With chlorine at 400℃; under 36775.4 Torr; |
1,1,2,3-Tetrachloropropene
3-bromo-1,1,2-trichloro-propene
Conditions | Yield |
---|---|
With acetone; sodium bromide | |
With hydrogen bromide; iron(III) chloride |
1,1,2,3-Tetrachloropropene
1,1,2-trichloropropene
Conditions | Yield |
---|---|
With tetrahydrofuran; lithium aluminium tetrahydride | |
With ethanol; zinc |
1,1,2,3-Tetrachloropropene
1,1,1,2,2,3-hexachloropropane
Conditions | Yield |
---|---|
With chlorine Irradiation.mit UV-Licht; |
1,1,2,3-Tetrachloropropene
2,3,3-trichloro-2-propen-1-ol
Conditions | Yield |
---|---|
With sodium carbonate |
1,1,2,3-Tetrachloropropene
1,1,2-trichloro-3-phenyl-propene
Conditions | Yield |
---|---|
With aluminium trichloride; benzene |
1,1,2,3-Tetrachloropropene
diethylamine
diethyl-(2,3,3-trichloro-allyl)-amine
Conditions | Yield |
---|---|
With methanol |
morpholine
1,1,2,3-Tetrachloropropene
4-(2,3,3-trichloro-allyl)-morpholine
Conditions | Yield |
---|---|
In methanol Heating; |
1,1,2,3-Tetrachloropropene
sodium ethanolate
1,1,2-trichloro-3-ethoxy-propene
Conditions | Yield |
---|---|
With phenol In ethanol |
1,1,2,3-Tetrachloropropene
sodium thiocyanide
2,3,3-Trichlor-allyl-thiocyanat
Conditions | Yield |
---|---|
In ethanol |
1,1,2,3-Tetrachloropropene
sodium diethylmalonate
Bis(β.γ.γ-trichlorallylmalonic Acid)-Diethyl Ester
Conditions | Yield |
---|---|
In ethanol |
1,1,2,3-Tetrachloropropene
sodium diethylmalonate
β.γ.γ-Trichlorallylmalonic Acid-Diethyl Ester
Conditions | Yield |
---|---|
In ethanol |
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