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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
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inquiryCAS No.: 540-72-7 Other Names: Sodium rhodanide MF: NaSCN EINECS No.: 208-754-4 Place of Origin: China (Main
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Sodium thiocyanate Basic information Product Name: Sodium thiocyanate Synonyms: haimased;natriumrhodanid;scyan;sodiumthiocyanatesolution(56%orless);sodiumthiocyanide;thiocyanatesodium;us
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inquiryProduct name: Sodium Thiocyanate Molecular formula: NaSCN Molecular weight: 81.07 Physico-chemical property: White orthorhombic crystal or powder; relative density: 1.735; melting point: 287℃; easily soluble in solvent, for example, water, ethyl
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inquiryB
sodium thiocyanide
Conditions | Yield |
---|---|
In tetrahydrofuran Kinetics; storage at 23°C for 24 h (or at 25°C for kinetic); solvent removed in vac.; residue dissolved in Et2O; filtered through fine sintered-glass frit; dried; NMR; | A 94% B 96% |
Conditions | Yield |
---|---|
With sodium azide; ethanol |
Conditions | Yield |
---|---|
With sodium hydrogensulfide at 200 - 500℃; | |
With sodium hydrogensulfide at 200 - 500℃; |
Conditions | Yield |
---|---|
With sulfur; acetone |
ammonium thiocyanate
sodium thiocyanide
Conditions | Yield |
---|---|
With sodium hydroxide |
thiourea
sodium thiocyanide
Conditions | Yield |
---|---|
With sodium hydrogensulfide at 200 - 500℃; | |
With sodium hydrogensulfide at 200 - 500℃; |
N-Cyanoguanidine
sodium thiocyanide
Conditions | Yield |
---|---|
With sodium hydrogensulfide at 200 - 500℃; | |
With sodium hydrogensulfide at 200 - 500℃; |
Conditions | Yield |
---|---|
In acetonitrile at 24.9℃; Equilibrium constant; |
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
1,8-bis<2-(diphenylphosphinoylmethyl)phenoxy>-3,6-dioxaoctane
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
tris<2-(diphenylphosphorylmethoxy)ethyl>amine
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
tris<2-(diphenylphosphorylmethoxy)ethyl>amine
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
tris<2-(diphenylphosphorylmethoxy)ethyl>amine
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
tris<3-oxa-5-(diphenylphosphoryl)pentyl>amine
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
A
sodium thiocyanide
B
tris<3-oxa-5-(diphenylphosphoryl)pentyl>amine
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
Conditions | Yield |
---|---|
In acetonitrile at 24.85℃; Equilibrium constant; Thermodynamic data; ΔG, ΔH, ΔS; |
benzo[d]thiazol-2-yl thiocyanate
sodium 2-mercaptobenzothiazole
A
2,2'-thiobis(benzothiazole)
B
di(benzothiazol-2-yl)disulfide
C
sodium cyanide
D
sodium thiocyanide
sodium thiocyanide
Conditions | Yield |
---|---|
With sodium sulfide | |
With sodium thiosulfate |
sodium thiocyanide
Conditions | Yield |
---|---|
With water; methyllithium; calcium carbonate |
sodium thiocyanide
Conditions | Yield |
---|---|
With tetrachloromethane; sodium thiosulfate |
sodium thiocyanide
Conditions | Yield |
---|---|
In tetrachloromethane; water | |
In tetrachloromethane; water |
sodium thiocyanide
16,19-Dioxo-2,5,8,11,14-pentaoxabicyclo[13.4.0]-115,1718-nonadecadien
Conditions | Yield |
---|---|
In dichloromethane for 2h; | 100% |
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide | 100% |
In acetonitrile at 60℃; for 1h; Solvent; Inert atmosphere; |
Conditions | Yield |
---|---|
In acetonitrile at 20 - 25℃; for 0.0833333h; | 100% |
5-bromo-3-(2-methylpyridin-3-yloxy)pyridin-2-amine
1-acetyl-N-(methylsulfonyloxy)piperidine-4-carbimidoyl chloride
sodium thiocyanide
1-(4-(5-(5-bromo-3-(2-methylpyridin-3-yloxy)pyridin-2-ylamino)-1,2,4-thiadiazol-3-yl)piperidin-1-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 1-acetyl-N-(methylsulfonyloxy)piperidine-4-carbimidoyl chloride; sodium thiocyanide With pyridine In acetonitrile at 40℃; for 0.666667h; Stage #2: 5-bromo-3-(2-methylpyridin-3-yloxy)pyridin-2-amine In acetonitrile at 60℃; | 100% |
4-methyl-N-(thiazol-2-yl)pyridine-2-amine
sodium thiocyanide
N-(4-methylpyridin-2-yl)-5-thiocyanatothiazol-2-amine
Conditions | Yield |
---|---|
With bromine In methanol at 23℃; for 1.33333h; | 100% |
With bromine In methanol at 23℃; for 1.33333h; | 100% |
sodium thiocyanide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 6h; | 100% |
Conditions | Yield |
---|---|
Stage #1: [[chloro-(3-nitrophenyl)methylene]amino]methanesulfonate; sodium thiocyanide With pyridine In acetonitrile at 40℃; for 1.5h; Stage #2: 4-chloro-1H-indazol-5-amine In acetonitrile at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
With MA-PVC In water at 15℃; Temperature; | 99.7% |
With sodium acetate In water at 10℃; for 6h; Time; Large scale; | |
In ethyl acetate at 40 - 50℃; for 3h; | |
Stage #1: sodium thiocyanide With dmap In water for 6h; Stage #2: methyl chloroformate In water at 20℃; |
2,3-Dichloroprop-1-ene
sodium thiocyanide
2-chloro-3-isothiocyanato-1-propene
Conditions | Yield |
---|---|
In dichloromethane at 0 - 5℃; for 3h; Temperature; Solvent; Reflux; | 99.5% |
With N-benzyl-N,N,N-triethylammonium chloride In toluene at 100 - 105℃; for 1.5h; Large scale; | 80% |
With N-benzyl-N,N,N-triethylammonium chloride In toluene at 100 - 105℃; for 1.5h; Large scale; | 80% |
With N-benzyl-N,N,N-triethylammonium chloride In toluene at 100 - 105℃; for 1.5h; Large scale; | 80% |
In water at 100℃; for 14h; Temperature; |
sodium thiocyanide
2-Dimethylamino-ethanesulfonic acid hexadecyl ester; compound with toluene-4-sulfonic acid
n-cetyl thiocyanate
Conditions | Yield |
---|---|
In water at 25℃; for 2h; | 99% |
sodium thiocyanide
chloroformic acid ethyl ester
Ethoxycarbonyl isothiocyanate
Conditions | Yield |
---|---|
With pyridine In water; toluene | 99% |
quinoline In water at 8 - 12℃; for 7.5h; | 80.4% |
With N,N-dimethyl-aniline In water at -1 - 8℃; for 4.5h; | 76.4% |
Conditions | Yield |
---|---|
With triphenyl phosphite; 2,6-dimethylpyridinium tetrafluoroborate In dichloromethane for 9.83333h; Product distribution; Ambient temperature; electrolysis; other alcohols; variation of conditions; | 99% |
With triphenyl phosphite; 2,6-lutidinium perchlorate In dichloromethane for 9.83333h; Ambient temperature; electrolysis; | 99% |
With trichloroisocyanuric acid; triphenylphosphine In acetonitrile at 82℃; for 3h; |
sodium thiocyanide
ω-(4-chloroanilino)-3-acetylbenzopyran-2-one
1-(4-chlorophenyl)-2-mercapto-4-(coumarin-3-yl)imidazole
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 3h; Heating; | 99% |
sodium thiocyanide
4-Nitrophenacyl bromide
2-(4-nitrophenyl)-2-oxoethyl thiocyanate
Conditions | Yield |
---|---|
In acetonitrile at 45℃; for 3h; | 99% |
With tetrabutylammomium bromide In water at 20℃; for 0.5h; | 93% |
With 1,4-bis(imidazol-1-yl)butane-based poly(ionic liquid) In water at 60℃; for 0.166667h; Green chemistry; | 92% |
(Indan-4-yloxy)-acetic Acid Methyl Ester
sodium thiocyanide
(7-thiocyanato-indan-4-yloxy)-acetic acid methyl ester
Conditions | Yield |
---|---|
With bromine; sodium bromide In methanol at 0℃; | 99% |
Conditions | Yield |
---|---|
In acetone at 25℃; for 1h; | 99% |
With tetrabutylammomium bromide In water at 20℃; for 0.666667h; | 92% |
With 1,4-bis(imidazol-1-yl)butane-based poly(ionic liquid) In water at 60℃; for 0.166667h; Green chemistry; | 88% |
sodium thiocyanide
2-(2'-pyridyl)imidazole
Conditions | Yield |
---|---|
In methanol methanolic soln. of KNCS (0.25 mmol) added dropwise to methanolic soln. of Mn compd. (0.125 mmol) and ligand (0.25 mmol) with stirring; crystd. on storage at room temp. for 1 wk, filtered off, washed (cold MeOH, Et2O), dried over CaCl2, elem. anal.; | 99% |
styrene
chloro-trimethyl-silane
ethyl benzenesulfenate
sodium thiocyanide
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: styrene; ethyl benzenesulfenate In chloroform | 99% |
chloro-trimethyl-silane
1,5-cis,cis-cyclooctadiene
ethyl benzenesulfenate
sodium thiocyanide
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: 1,5-cis,cis-cyclooctadiene; ethyl benzenesulfenate In chloroform | 99% |
chloro-trimethyl-silane
norbornene
ethyl benzenesulfenate
sodium thiocyanide
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: norbornene; ethyl benzenesulfenate In chloroform | 99% |
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: ethyl benzenesulfenate; 3',6'-dimethoxybenzonorborna-2,5-diene In chloroform | 99% |
chloro-trimethyl-silane
ethyl benzenesulfenate
sodium thiocyanide
E-1-(4'-methoxyphenyl)prop-1-ene
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: ethyl benzenesulfenate; E-1-(4'-methoxyphenyl)prop-1-ene In chloroform | 99% |
chloro-trimethyl-silane
ethyl benzenesulfenate
sodium thiocyanide
cyclohexene
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; sodium thiocyanide In chloroform at 20℃; for 1h; Stage #2: ethyl benzenesulfenate; cyclohexene In chloroform | 99% |
Conditions | Yield |
---|---|
In dichloromethane for 17h; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With N-chloro-succinimide In ethanol at 0 - 20℃; for 0.5h; | 99% |
With N-chloro-succinimide In ethanol at 20℃; | 94% |
With oxygen In tetrahydrofuran at 25℃; under 750.075 Torr; for 7h; Irradiation; | 50% |
With air; Ag/TiO2 nanotubes In tetrahydrofuran at 20℃; for 18h; Irradiation; Green chemistry; | 38% |
Conditions | Yield |
---|---|
In dichloromethane for 24h; Inert atmosphere; | 99% |
sodium thiocyanide
Conditions | Yield |
---|---|
With Sodium thiosulfate pentahydrate In acetonitrile at 20℃; for 12h; | 99% |
sodium thiocyanide
Conditions | Yield |
---|---|
In methanol; water at 80℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 99% |
1-(4-chlorophenyl)sulfonyl-2-phenyl aziridine
sodium thiocyanide
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water at 20℃; for 16h; | 98.5% |
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