CAS No.120-78-5,2,2'-Dithiobis(benzothiazole) Suppliers,MSDS download

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance Grayish white or light yellow powder Conforms Initial Melting point

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Product Description Product name 2,2'-Dithiobis(benzothiazole) CAS 120-78-5 Assay Appearance Gray-white to yellowish powder or particles Capacity 1000mt/year Min.package

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Dayang Chem (Hangzhou) Co.,Ltd.

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About Product Details CAS: 1

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Henan Sinotech Import&Export Corporation

CAS No. 120-78-5 Name 2,2'-Dithiobis(benzothiazole) MF C14H8N2S4 EINECS No. 204-424-9 Appearance:Cream to pale-yellow powder Sto

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Shanghai Minstar Chemical Co., Ltd

Product Name: 2,2'-Dithiobis(benzothiazole) CAS: 120-78-5 MF: C14H8N2S4 MW: 332.49 EINECS: 204-424-9 2,2'-Dithiobis(benzothiazole) Structure 2,2'-Dithiobis(benzothiazole) Chemical Properties Melting point 177-180 &deg

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Afine Chemicals Limited

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2,2'-DITHIOBIS(BENZOTHIAZOLE)

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Synthetic route

: 149-30-4
2-Mercaptobenzothiazole

: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With bis(2,2'-bipyridyl) copper(II) permanganate In dichloromethane for 0.166667h;	100%
With tris paraperiodate In benzene for 0.5h; Heating;	100%
With dihydrogen peroxide In water	100%

: 333-20-0
potassium thioacyanate

: 71355-12-9, 95835-16-8
p-nitrobenzyl <(R)-4-(2-benzothiazol-2-yldithio)-2-oxo-1-azetidinyl>isopropenylacetate

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 112110-51-7
(2S,3R)-3-Methyl-7-oxo-3-thiocyanatomethyl-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 4-nitro-benzyl ester

Conditions

Conditions	Yield
In dichloromethane; sulfuric acid; water for 12h; Ambient temperature; electrolysis procedure;	A 99% B 97%

...Expand

: 2492-26-4
sodium 2-mercaptobenzothiazole

: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With bromonitromethane In methanol	98%
With water; chlorine; ammonium chloride
With sulfuric acid; water; dihydrogen peroxide

: 80756-85-0
(Z)-S-benzo[d]thiazol-2-yl 2-(2-aminothiazol-4-yl)-2-(methoxyimino)ethanethioate

: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With tetrabutylammomium bromide; ozone In methanol at 44℃; for 1.5h; Concentration; Temperature; Large scale;	97.5%

: 41475-98-3
S-(benzo[d]thiazol-2-yl) benzenesulfonothioate

: 57562-33-1, 68128-75-6
2-[(2R,3R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-3-enoic acid benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

: 91939-45-6, 106138-52-7
4-phenylsulfonylthio-3-phenoxyacetamido-1-(1-benzyloxycarbonyl-2-methyl-2-propenyl)-2-azetidinone

Conditions

Conditions	Yield
sodium benzenesulfonate In water; acetone for 3.5h; Ambient temperature;	A 96% B 91%

...Expand

: 72844-42-9
2-(Benzothiazol-2-ylsulfanyl)-2-(3-methyl-but-2-enyl)-hexanedioic acid dimethyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 72844-50-9
2-(3-Methyl-but-2-enyl)-hexanedioic acid dimethyl ester

Conditions

Conditions	Yield
In methanol; sulfuric acid Ambient temperature; Electrochemical reduction;	A 96% B 74%

: 149-30-4
2-thioxo-3H-1,3-benzothiazole

: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With 3,3-dimethyldioxirane In dichloromethane; acetone at 25℃;	95%
With dilauryl peroxide In 1,2-dichloro-ethane for 1h; Reflux;	90%
With potassium dichromate; acetic acid

: (R)-2-[2-(Benzothiazol-2-yldisulfanyl)-3,3-dibromo-4-oxo-azetidin-1-yl]-3-methyl-but-3-enoic acid benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: benzhydryl 6,6-dibromo-2β-chloromethyl-2α-methylpenam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 5h;	A n/a B 95%

: 67-56-1
methanol

: 70203-06-4
2-benzothiazol-2-ylsulfanyl-octanoic acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74391-99-4
2,2-Dimethoxy-octanoic acid methyl ester

Conditions

Conditions	Yield
With sulfuric acid; copper dichloride Ambient temperature; electrosynthesis;	A 58% B 94%
With tetraethylammonium perchlorate; copper dichloride for 2.4h; Product distribution; Ambient temperature; electrosynthesis; further electrolytes, further α-sulfenylalkanoates; also without CuCl2;	A 80% B 83%

...Expand

: 667-20-9
N,N'-bis(phenylsulfonyl)sulfur diimide

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 81955-02-4
N,N'-bis(phenylsulfonyl)sulfoxylic diamide

Conditions

Conditions	Yield
With 2-Mercaptobenzothiazole In benzene for 8h; Heating;	A 94% B 90%

: (R)-2-[2-(Benzothiazol-2-yldisulfanyl)-3,3-dibromo-4-oxo-azetidin-1-yl]-3-methyl-but-3-enoic acid 4-methoxy-benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: p-methoxybenzyl 6,6-dibromo-2β-chloromethyl-2α-methylpenam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 5h;	A n/a B 93%

: 41475-98-3
S-(benzo[d]thiazol-2-yl) benzenesulfonothioate

: 98231-55-1
2-[(2R,3R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-phenylacetylamino-azetidin-1-yl]-3-methyl-but-3-enoic acid 4-methoxy-benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

: 93788-86-4, 106247-27-2
4-phenylsulfonylthio-3-phenylacetamido-1-(1-(p-methoxybenzyloxycarbonyl)-2-methyl-2-propenyl)-2-azetidinone

Conditions

Conditions	Yield
sodium 2-mercaptobenzothiazole In water; acetone for 1.5h; Ambient temperature;	A n/a B 92%

...Expand

: 85573-72-4, 87579-79-1
(R)-2-[2-(benzothiazol-2-yldisulfanyl)-4-oxo-azetidin-1-yl]-3-methyl-butyl-3-enoic acid benzhydryl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 85573-73-5, 115546-67-3
2β-chloromethyl-2α-methylpenicillin-3α-carboxylic acid diphenylmethyl ester

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 2h;	A n/a B 92%

: 118331-41-2
(R)-2-[2-(Benzothiazol-2-yldisulfanyl)-4-oxo-azetidin-1-yl]-3-methyl-but-3-enoic acid 4-methoxy-benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: p-methoxybenzyl 2β-chloromethyl-2α-methylpenam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 2h;	A n/a B 92%

: 71355-12-9, 95835-16-8
p-nitrobenzyl <(R)-4-(2-benzothiazol-2-yldithio)-2-oxo-1-azetidinyl>isopropenylacetate

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 89051-52-5
p-nitrobenzyl 2β-(chloromethyl)-2α-methylpenam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane at 0℃; for 2h; Product distribution; Mechanism; reactions of derivatives with HCl and HBr;	A n/a B 91%
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 2h;	A n/a B 91%

: 95122-89-7, 126577-33-1
2-(2-benzothiazolyldithio)-3-bromo-α-(1-methylethylidene)-4-oxo-1-azetidineacetic acid β-nitrobenzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: p-nitrobenzyl 6α-bromo-2β-chloromethyl-2α-methylpenam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 3h;	A n/a B 91%

: 84734-39-4, 91176-99-7, 93132-97-9
(R)-2-[(R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-phenylacetylamino-azetidin-1-yl]-3-methyl-but-3-enoic acid benzyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: benzyl 2β-chloromethyl-2α-methyl-6β-(phenylacetamido)-penam-3α-carboxylate

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrite In dichloromethane; water at 0℃; for 2h;	A n/a B 91%

: 149-30-4
2-Mercaptobenzothiazole

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 4845-58-3
2-mercapto-6-nitrobenzothiazole

Conditions

Conditions	Yield
In sulfuric acid	A 90% B n/a

: 41475-98-3
S-(benzo[d]thiazol-2-yl) benzenesulfonothioate

: 873-55-2
sodium benzenesulfonate

A: 93788-86-4
p-methoxybenzyl 2-(3-phenylacetamido-4-benzenesulfonylthio-2-azetidinon-1-yl)-3-methyl-3-butenoate

B: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
In acetone	A 90% B n/a

...Expand

: 75-15-0
carbon disulfide

: 615-43-0
2-iodophenylamine

: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With copper(l) iodide; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 110℃; for 6h; Mechanism; Sealed tube;	89%

: 67-56-1
methanol

: 70203-07-5
2-benzothiazol-2-ylsulfanyl-hexanedioic acid dimethyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74400-47-8
2,2-Dimethoxy-hexanedioic acid dimethyl ester

Conditions

Conditions	Yield
With tetraethylammonium perchlorate; copper dichloride Ambient temperature; electrosynthesis;	A 88% B 57%

...Expand

: 70203-07-5
2-benzothiazol-2-ylsulfanyl-hexanedioic acid dimethyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74400-47-8
2,2-Dimethoxy-hexanedioic acid dimethyl ester

Conditions

Conditions	Yield
With tetraethylammonium perchlorate; copper dichloride In methanol Ambient temperature; electrosynthesis;	A 88% B 57%

: 72844-40-7
dimethyl 2-n-pentyl-(2-benzothiazolylthio)adipate

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 72844-48-5
2-Pentyl-hexanedioic acid dimethyl ester

C: 149-30-4
2-Mercaptobenzothiazole

Conditions

Conditions	Yield
In methanol; sulfuric acid Ambient temperature; Electrochemical reduction;	A 31% B 87% C 53%

...Expand

: 72844-45-2
2-(Benzothiazol-2-ylsulfanyl)-2-(3-methyl-but-2-enyl)-octanoic acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 72844-53-2
2-(3-Methyl-but-2-enyl)-octanoic acid methyl ester

C: 149-30-4
2-Mercaptobenzothiazole

Conditions

Conditions	Yield
In methanol; sulfuric acid Ambient temperature; Electrochemical reduction;	A 63% B 84% C 24%

...Expand

: 67-56-1
methanol

: 74391-97-2
2-(Benzothiazol-2-ylsulfanyl)-4-methoxy-butyric acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74392-00-0
2,2,4-Trimethoxy-butyric acid methyl ester

Conditions

Conditions	Yield
With tetraethylammonium perchlorate; copper dichloride Ambient temperature; electrosynthesis;	A 83% B 70%

...Expand

: 70203-06-4
2-benzothiazol-2-ylsulfanyl-octanoic acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74391-99-4
2,2-Dimethoxy-octanoic acid methyl ester

Conditions

Conditions	Yield
With tetraethylammonium perchlorate; copper dichloride In methanol for 2.4h; Ambient temperature; electrosynthesis;	A 80% B 83%

: 74391-97-2
2-(Benzothiazol-2-ylsulfanyl)-4-methoxy-butyric acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 74392-00-0
2,2,4-Trimethoxy-butyric acid methyl ester

Conditions

Conditions	Yield
With tetraethylammonium perchlorate; copper dichloride In methanol Ambient temperature; electrosynthesis;	A 83% B 70%

: 149-30-4
2-thioxo-3H-1,3-benzothiazole

A: 95-16-9
1,3-Benzothiazole

B: 120-78-5
di(benzothiazol-2-yl)disulfide

Conditions

Conditions	Yield
With ozone In methanol; dichloromethane at 25℃;	A 11% B 83%
With ozone In dichloromethane at 25℃; Product distribution; other 2-mercaptoheterazoles at different reaction conditions;	A 5% B 75%
With dihydrogen peroxide; acetic acid at 25℃; for 0.0833333h;	A 35% B 43%

: 72844-41-8
dimethyl 2-(2-pentynyl)-2-(2-benzothiazolylthio)adipate

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 72844-49-6
2-Pent-2-ynyl-hexanedioic acid dimethyl ester

C: 149-30-4
2-Mercaptobenzothiazole

Conditions

Conditions	Yield
In methanol; sulfuric acid Ambient temperature; Electrochemical reduction;	A 50% B 82% C 22%

...Expand

: 70905-82-7
2-benzothiazol-2-ylsulfanyl-2-(3-oxo-butyl)-octanoic acid methyl ester

A: 120-78-5
di(benzothiazol-2-yl)disulfide

B: 72844-54-3
2-(3-Oxo-butyl)-octanoic acid methyl ester

C: 149-30-4
2-Mercaptobenzothiazole

Conditions

Conditions	Yield
In methanol; sulfuric acid Ambient temperature; Electrochemical reduction;	A 33% B 80% C 25%

...Expand

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 316123-88-3
(5-Amino-[1,2,4]thiadiazol-3-yl)-[(Z)-1-ethyl-propoxyimino]-acetic acid

: 316123-90-7
(5-amino-[1,2,4]thiadiazol-3-yl)-(1-ethyl-propoxyimino)-thioacetic acid S-benzothiazol-2-yl ester

Conditions

Conditions	Yield
With tributyl-amine; triethyl phosphite In acetonitrile at -10℃;	100%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 108-91-8
cyclohexylamine

: 95-33-0
N-(cyclohexyl)benzothiazole-2-sulfenamide

Conditions

Conditions	Yield
With sodium hydroxide In water; toluene	100%

: 110-91-8
morpholine

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 102-77-2
4-(benzothiazole-2-sulfenyl)-morpholine

Conditions

Conditions	Yield
With sodium hydroxide In toluene	99.5%
With tetraethylammonium perchlorate In N,N-dimethyl-formamide for 16h; (electrolysis);

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 75-64-9
tert-butylamine

: 95-31-8
N-(tert-butyl)benzothiazole-2-sulfenamide

Conditions

Conditions	Yield
With sodium hydroxide In methanol at 40 - 85℃; for 2.5h; Reagent/catalyst; Solvent; Large scale;	99.5%
Stage #1: di(benzothiazol-2-yl)disulfide In water at 20℃; for 0.5h; Reflux; Stage #2: tert-butylamine In water at 30 - 50℃; for 3h; Stage #3: With sodium hydroxide In water at 80 - 85℃; for 1h; Reagent/catalyst;	98.5%
With tetrabutylammonium tetrafluoroborate In acetonitrile at 30℃; for 2h; Sealed tube; Electrochemical reaction;	95%
With oxygen In water at 60℃; under 2250.23 Torr; for 4h; Reagent/catalyst;	76%
With tetraethylammonium perchlorate In N,N-dimethyl-formamide at 15 - 22℃; for 8h; (electrolysis);

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 143-15-7
1-dodecylbromide

: 106184-47-8
2-(dodecylthio)benzo[d]thiazole

Conditions

Conditions	Yield
With RhCl(PPh3)3; hydrogen; triethylamine In tetrahydrofuran at 50℃; under 760 Torr; for 24h;	99%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 86299-47-0
(Z)-2-(2-aminothiazol-4-yl)-2-(1-tert-butoxycarbonyl-1-methylethoxy)iminoacetic acid

: 89604-92-2
2-benzothiazolyl 2-(2-aminothiazol-4-yl)-2-<<1-(tert-butoxycarbonyl)-1-methylethoxy>imino>thioacetate

Conditions

Conditions	Yield
With pyridine; N,N-dimethyl-aniline; triethyl phosphite In acetonitrile; benzene at 18 - 25℃; for 0.5h; Reagent/catalyst; Microwave irradiation; Green chemistry;	98.5%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 75-66-1
2-methylpropan-2-thiol

: 27657-22-3
2-(tert-butyldisulfanyl)benzo[d]thiazole

Conditions

Conditions	Yield
With palladium dichloride In dimethyl sulfoxide at 80℃; for 2h; Schlenk technique; Inert atmosphere;	98%
In chloroform for 6h; Ambient temperature;	88%
With methanol; tetrabutylammonium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; for 4h; Electrochemical reaction; Inert atmosphere;	65%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 2-Methyl-3-(trityl-amino)-propan-1-ol

: 219126-59-7
[3-(Benzothiazol-2-ylsulfanyl)-2-methyl-propyl]-trityl-amine

Conditions

Conditions	Yield
With tributylphosphine In tetrahydrofuran	98%

: 60-80-0
antipyrine

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 4-(benzo[d]thiazol-2-ylthio)-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one

Conditions

Conditions	Yield
With dipotassium peroxodisulfate; potassium iodide In acetonitrile at 60℃; for 16h;	97%
With 1,4-diaza-bicyclo[2.2.2]octane; silver(I) acetate In methanol at 20℃; for 2h; Sealed tube;	84%

: 91868-79-0
2-(2-amino-1,3-thiazol-4-yl)-2-(methoxyimino)acetic acid

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 94088-75-2
2-(2-amino-1,3-thiazol-4-yl)-1-(1,3-benzothiazol-2-ylsulfanyl)-2-(methoxyimino)ethan-1-one

Conditions

Conditions	Yield
With pyridine; triethylamine; triethyl phosphite In dichloromethane; acetonitrile at 16.5 - 23℃; for 2h; Temperature; Reagent/catalyst;	97%
Stage #1: 2-(2-amino-1,3-thiazol-4-yl)-2-(methoxyimino)acetic acid With N,N-dimethyl acetamide; triethylamine In dichloromethane; acetonitrile for 1.5h; Stage #2: di(benzothiazol-2-yl)disulfide With phosphonic Acid; triethyl phosphite In dichloromethane; acetonitrile at 31℃; for 2h; Reagent/catalyst; Temperature;	92.74%

: 110-91-8
morpholine

dibenzolthiazolyl disulphide: dibenzolthiazolyl disulphide

N-Cyclohexyl-2-benzothiazole sulphene amide: N-Cyclohexyl-2-benzothiazole sulphene amide

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 102-77-2
4-(benzothiazole-2-sulfenyl)-morpholine

Conditions

Conditions	Yield
In ethanol	96.5%

...Expand

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 169956-70-1
(5-Amino-[1,2,4]thiadiazol-3-yl)-[(Z)-3,3-dimethyl-cyclobutoxyimino]-acetic acid

: 169956-71-2
(5-amino-[1,2,4]thiadiazol-3-yl)-(3,3-dimethyl-cyclobutoxyimino)-thioacetic acid S-benzothiazol-2-yl ester

Conditions

Conditions	Yield
With tributyl-amine; triethyl phosphite In acetonitrile at -10℃;	96%

: 909025-52-1
tridec-1-ene-3-thiol

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 909025-34-9
2-(2-(tridec-1-en-3-yl)disulfanyl)benzo[d]thiazole

Conditions

Conditions	Yield
In chloroform at 20℃;	96%
In chloroform	96%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 620973-40-2
benzothiazolyl-2-sulfur trifluoride

Conditions

Conditions	Yield
With potassium fluoride; chlorine In acetonitrile at 20℃; for 4h;	95.5%
With potassium fluoride; chlorine In acetonitrile at 20℃;

: 629-45-8
dibutyl disulfide

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 2-(butyldisulfanyl)benzo[d]thiazole

Conditions

Conditions	Yield
bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate In dichloromethane at 80℃; for 3h;	95%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 179162-55-1
4-{5-[4-(pentyloxy)phenyl]-1,2-oxazol-3-yl}benzoic acid

: 1426839-84-0
PPIB-MBT

Conditions

Conditions	Yield
With triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 2h;	95%
With triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 2h;	95%

: 108-86-1
bromobenzene

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 4276-60-2
2-(phenylthio)benzothiazole

Conditions

Conditions	Yield
With tetra(n-butyl)ammonium hydroxide In water; N,N-dimethyl-formamide at 80℃; for 0.166667h; Microwave irradiation;	95%

: 490-64-2
asaronic acid

: 120-78-5
di(benzothiazol-2-yl)disulfide

: C17H15NO4S2

Conditions

Conditions	Yield
Stage #1: di(benzothiazol-2-yl)disulfide With triphenylphosphine In dichloromethane at 5℃; for 1h; Inert atmosphere; Stage #2: asaronic acid In dichloromethane at 5℃; for 1h;	94.4%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 119-53-9
2-hydroxy-2-phenylacetophenone

: 109275-18-5
2-[(1,3-benzothiazol-2-yl)sulfanyl]-1,2-diphenylethanone

Conditions

Conditions	Yield
With tributylphosphine In toluene for 8h; Heating;	94%

: 503614-92-4
1-(4-methoxyphenyl)-7-oxo-6-(4-(2-oxopiperidin-1-yl)phenyl)-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid

: 120-78-5
di(benzothiazol-2-yl)disulfide

: C32H27N5O4S2

Conditions

Conditions	Yield
Stage #1: di(benzothiazol-2-yl)disulfide With triphenylphosphine In dichloromethane at 20℃; for 1.5h; Stage #2: 1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxopiperidin-1-yl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid In dichloromethane at 20℃; for 1h;	94%