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1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:152459-95-5
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryUnique advantages of Imatinib Cas 152459-95-5 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or almost white powder Storage:Cool dry place Package:1kg/foil bag
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Imatinib English name: Imatinib Chemical name: 4-[(4-Methylpiperazin-1-yl)methyl]-N-[4-methyl-3-[(4-pyridin-3-ylpyrimidin-2-yl)amino]phenyl]benzamide Category involved: bulk pharmace
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryName: Imatinib Synonyms: 4-[(4-methylpiperazin-1-yl)methyl]-N-(4-methyl-3-{[4-(pyridin-3-yl)pyrimidin-2-yl]amino}phenyl)benzamide CAS: 152459-95-5 MF: C30H35N7O4S Appearance: white powder Storage:Store in cool and dry place, away from sun li
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem specialized in APIs, chemical intermediate
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inquiryWe have two GMP facilities in Hubei Province and cooperative factories in Zhejiang Province We are concentrating on the R&D and technical service of APIs and pharmaceutical intermediates FDA Approved Appearance:white Storage:2-8°C Packag
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Superiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes
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inquiryAppearance:Off white powder Storage:Room temperature Package:25kg/drum Application:API Transportation:Express/Sea/Air Port:Any port in china
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Min.Order:25 Kilogram
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
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inquiryAPI name:Gleevec Certificates: GMP, DMF CAS No.: 152459-95-5 Chemical name: 4-(4-METHYL-PIPERAZIN-1-YLMETHYL)-N-[4-METHYL-3-(4-PYRIDIN-3-YL-PYRIMIDIN-2-YLAMINO)-PHENYL]-BENZAMIDE;Imatinib(4-[(4-Methylpiperazin-1-yl)methyl]-N-[4-methyl-3
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Cas:152459-95-5
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
Stage #1: 4-((4-methylpiperazin-1-yl)methyl)benzoyl chloride dihydrochloride; 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine In water at 0℃; Stage #2: With sodium hydroxide In water at 50 - 55℃; pH=9 - 9.5; Product distribution / selectivity; | 99.26% |
With pyridine at 0 - 20℃; for 1h; Product distribution / selectivity; | 95% |
Stage #1: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine With pyridine for 0.333333h; Autoclave; Stage #2: 4-((4-methylpiperazin-1-yl)methyl)benzoyl chloride dihydrochloride at 0 - 25℃; for 8h; | 92.7% |
imatinib
Conditions | Yield |
---|---|
With sodium hydroxide In water at 0 - 55℃; pH=9 - 9.5; | 99.26% |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 40 - 50℃; for 6h; Time; | 97.8% |
1-methyl-piperazine
4-(chloromethyl)-N-(4-methyl-3-{[4-(pyridin-3-yl)pyrimidin-2-yl]-amino}phenyl)benzamide
imatinib
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 4.5h; Temperature; | 97.52% |
In 1,4-dioxane at 135℃; for 3h; Conversion of starting material; | 91% |
at 120 - 130℃; for 1.5h; Conversion of starting material; | 91% |
imatinib
Conditions | Yield |
---|---|
With ammonia In water Product distribution / selectivity; | 97% |
4-[(4-methylpiperazin-1-yl)methyl]bromobenzene
carbon monoxide
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 50℃; under 760.051 Torr; for 36h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 95.8% |
imatinib
Conditions | Yield |
---|---|
With ammonia In water; isopropyl alcohol at 20℃; for 4h; pH=7.6 - 8.5; | 93% |
3-(N,N-dimethylamino)-1-(pyridin-3-yl)prop-2-en-1-one
imatinib
Conditions | Yield |
---|---|
In butan-1-ol at 120 - 150℃; for 5h; Inert atmosphere; | 93% |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
Stage #1: 4-[(4-methylpiperazin-1-yl)methyl]benzoic acid dihydrochloride With pyridine; thionyl chloride at 50 - 60℃; for 3h; Stage #2: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine at -10 - 0℃; for 1h; | 92.5% |
Stage #1: 4-[(4-methylpiperazin-1-yl)methyl]benzoic acid dihydrochloride With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 50℃; for 2h; Stage #2: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine In N,N-dimethyl-formamide at 70℃; for 12h; | 91% |
Stage #1: 4-[(4-methylpiperazin-1-yl)methyl]benzoic acid dihydrochloride With pyridine; thionyl chloride at 20 - 50℃; for 1 - 2h; Stage #2: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine With pyridine at 0 - 25℃; for 1h; Product distribution / selectivity; | 90% |
N-(3-bromo-4-methylphenyl)-4-((4-methylpiperazin-1-yl)-methyl)benzamide
4-pyridin-3-ylpyrimidin-2-ylamine
imatinib
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 5h; Temperature; | 92% |
Stage #1: N-(3-bromo-4-methylphenyl)-4-((4-methylpiperazin-1-yl)-methyl)benzamide; 4-pyridin-3-ylpyrimidin-2-ylamine In ethanol at 60℃; for 3h; Inert atmosphere; Stage #2: With sodium hydroxide In water pH=8.7; Reagent/catalyst; | 91% |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 5.16667h; Inert atmosphere; Reflux; Sonication; | 72% |
4-(4-methyl piperazin-1-ylmethyl)-benzoic acid ethyl ester
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With sodium methylate In dichloromethane at 40℃; | 92% |
imatinib
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 92% |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
4-(4-methylpiperazin-1-ylmethyl)benzoic acid
imatinib
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20 - 30℃; Solvent; | 91.72% |
Stage #1: 4-(4-methylpiperazin-1-ylmethyl)benzoic acid With pyridine; thionyl chloride at 0 - 50℃; for 1 - 2h; Stage #2: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine With pyridine at 0 - 20℃; for 1h; Product distribution / selectivity; | 88% |
Stage #1: 4-(4-methylpiperazin-1-ylmethyl)benzoic acid With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 18h; Stage #2: 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine With dmap In dichloromethane at 15 - 25℃; for 49h; Product distribution / selectivity; | 77% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran; water at 20℃; for 1.16667h; | 72% |
Conditions | Yield |
---|---|
Stage #1: 4-[(4-methylpiperazin-1-yl)methyl]benzoic acid dihydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 10 - 20℃; for 0.5h; Stage #2: With tetrabutyl ammonium fluoride; 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 3h; Stage #3: C22H31N5Si2 In dichloromethane at 0 - 20℃; for 3h; Solvent; Reagent/catalyst; | 91.3% |
Stage #1: 4-[(4-methylpiperazin-1-yl)methyl]benzoic acid dihydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 10 - 20℃; for 0.5h; Stage #2: With tetrabutyl ammonium fluoride; 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 3h; Stage #3: C22H31N5Si2 In dichloromethane at 20℃; for 3h; Solvent; Reagent/catalyst; | 91.3% |
N,N-(4-methyl-3-aminophenyl)[4-(pyridin-3-yl)-pyrimidin-2-yl]amine
4-((4-methylpiperazin-1-yl)methyl)-benzoic acid methyl ester
imatinib
Conditions | Yield |
---|---|
With sodium methylate In tetrahydrofuran; methanol Product distribution / selectivity; Reflux; | 91% |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
4-((4-methylpiperazin-1-yl)methyl)-benzoic acid methyl ester
imatinib
Conditions | Yield |
---|---|
With sodium methylate In tetrahydrofuran at 70℃; | 91% |
With trimethylaluminum In toluene at 40℃; for 0.5h; Inert atmosphere; |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With cesium hydroxide In propan-1-ol at 80℃; | 90.5% |
4-(4-methyl-piperazin-1-methyl)-benzoic acid benzyl ester
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With sodium ethanolate In toluene at 50℃; Reagent/catalyst; Solvent; | 90% |
4-(4-methyl-piperazin-1-methyl)-benzoic acid propyl ester
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 50℃; Large scale; | 90% |
4-(4-methyl-piperazin-1-methyl)-benzoic acid 4-methoxy-benzyl ester
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With n-butyllithium In acetonitrile at 20℃; | 90% |
4-(4-methyl-piperazin-1-methyl)-benzoic acid p-tolyl ester
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With potassium carbonate In ethyl acetate at 50℃; Reagent/catalyst; Solvent; | 90% |
imatinib
Conditions | Yield |
---|---|
With dmap In 5,5-dimethyl-1,3-cyclohexadiene at 135℃; for 4h; Temperature; Solvent; Reagent/catalyst; | 87.1% |
1-methyl-piperazine
p-(chloromethyl)benzoyl chloride
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
Stage #1: p-(chloromethyl)benzoyl chloride; 6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine With triethylamine In tetrahydrofuran at 0℃; for 3h; Buchwald-Hartwig Coupling; Inert atmosphere; Stage #2: 1-methyl-piperazine In tetrahydrofuran at 80℃; for 12h; Reflux; Inert atmosphere; chemoselective reaction; | 87% |
With pyridine In 1-methyl-pyrrolidin-2-one at 40 - 80℃; |
1-methyl-piperazine
N-(3-bromo-4-methylphenyl)-4-(chloromethyl)benzamide
4-pyridin-3-ylpyrimidin-2-ylamine
imatinib
Conditions | Yield |
---|---|
With copper(l) iodide; sodium acetate; N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 100℃; for 4h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 86% |
N-5-bromo-2-methylphenyl(4-pyridine-3-yl)pyrimidine-2-amine
imatinib
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; N,N-dimethylethylenediamine In 1,4-dioxane at 85℃; for 18h; Reflux; Inert atmosphere; | 85.4% |
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine In water; toluene for 24h; Solvent; Reflux; Green chemistry; | 84.1% |
imatinib
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran at 65℃; for 7h; Temperature; Solvent; Reagent/catalyst; | 85.2% |
2-chloro-4-(pyridin-3-yl)pyrimidine
imatinib
Conditions | Yield |
---|---|
With acetic acid In 1,4-dioxane at 110℃; for 6h; Temperature; Solvent; Green chemistry; | 84.5% |
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
imatinib
Conditions | Yield |
---|---|
With Imidazole hydrochloride at 15 - 20℃; Reagent/catalyst; Temperature; | 84% |
N-(5-amino-2-methylphenyl)-4-(3-pyridyl)-2-pyridineamine
S-benzotrizol-2-yl-4-[(4-methylpiperazin-1-yl)methyl]benzoate
imatinib
Conditions | Yield |
---|---|
In toluene at 25 - 50℃; | 80.15% |
S-benzotrizol-2-yl-4-[(4-methylpiperazin-1-yl)methyl]benzoate
C17H16N4
imatinib
Conditions | Yield |
---|---|
In toluene at 25 - 50℃; | 80.15% |
dichloro-acetic acid
imatinib
4-[(4-methyl-1-piperazinyl)methyl]-N-[4-methyl-3-[[4-(3-pyridyl)-2-pyrimidinyl]amino]phenyl]benzamide dichloroacetate
Conditions | Yield |
---|---|
In isopropyl alcohol at 20 - 25℃; for 3h; Product distribution / selectivity; | 100% |
In isopropyl alcohol at 20 - 25℃; for 3h; Product distribution / selectivity; | 100% |
Conditions | Yield |
---|---|
In acetone at 55 - 60℃; for 2h; Concentration; Temperature; Time; | 99.89% |
In di-isopropyl ether; isopropyl alcohol at 20℃; for 3.16667h; Product distribution / selectivity; Reflux; | 97% |
In isopropyl alcohol; acetone for 3h; Reflux; | 97.1% |
Conditions | Yield |
---|---|
In isopropyl alcohol at 20 - 80℃; Product distribution / selectivity; Reflux; | 99.6% |
In methanol at 50 - 55℃; for 2.5h; Solvent; Temperature; | 95% |
In methanol at -10 - 0℃; for 0.333333h; Product distribution / selectivity; | 58% |
imatinib
6-methyl-1-N-(4-(pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid at 20℃; Reflux; | 97% |
Conditions | Yield |
---|---|
In methanol; 5,5-dimethyl-1,3-cyclohexadiene at 25 - 80℃; for 18h; | 94% |
In methanol; 5,5-dimethyl-1,3-cyclohexadiene at 25 - 80℃; for 18h; | 94% |
camphor-10-sulfonic acid
imatinib
4-[(4-methyl-1-piperazinyl)methyl]-N-[4-methyl-3-[[4-(3-pyridyl)-2-pyrimidinyl]amino]phenyl]-benzamide D,L-(+/-)-camphorsulphonate
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Product distribution / selectivity; Heating / reflux; | 93.8% |
Stage #1: camphor-10-sulfonic acid; imatinib In methanol at 20℃; for 1h; Activated carbon; Stage #2: In isopropyl alcohol at 20℃; for 1h; Product distribution / selectivity; | 91.1% |
methanesulfonic acid
imatinib
Conditions | Yield |
---|---|
In water; isopropyl alcohol at 20℃; | 91% |
In ethanol at 20 - 70℃; for 3.33h; Product distribution / selectivity; Heating / reflux; | |
In isopropyl alcohol at 65 - 70℃; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In methanol; 5,5-dimethyl-1,3-cyclohexadiene at 25 - 80℃; for 18h; | 90% |
Conditions | Yield |
---|---|
In methanol; 5,5-dimethyl-1,3-cyclohexadiene at 25 - 80℃; for 18h; | 90% |
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