1.high purity 2.consistent quality 3.competitive price 4.fast shipping Binbo Biological Products Co. Ltd., is a professional high-tech enterprise which engaged in Biological products and raw materials. Binbo is engaged in R&D with perfect eq
Cas:1135-24-6
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Type:Lab/Research institutions
inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Cas:1135-24-6
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inquiryFerulic acid CAS 1135-24-6 IN Stock 4-Hydroxy-3-methoxycinnamic acid CAS 1135-24-6 3-Methoxy-4-hydroxy-cinnamic acid Ferulic acid CAS 1135-24-6 IN Stock 4-Hydroxy-3-methoxycinnamic acid CAS 1135-24-6 Ferulic Acid COA TDS price MSDS F
Cas:1135-24-6
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Type:Manufacturers
inquiryZhonghe Fountain is striving for R&D,production and distribution cosmetic active ingredients for personal care industry. Zhonghe Fountain always maintains a keen insight into industry and focuses on the market demand trends to expand its invests
Cas:1135-24-6
Min.Order:1 Kilogram
FOB Price: $100.0
Type:Trading Company
inquiryFerulic Acid Quick Details Type: Herbal Extract Variety: Ferulic Acid Form: Powder Part: Rice bran Extraction Type: Solvent Extrac
Cas:1135-24-6
Min.Order:1 Kilogram
FOB Price: $45.0 / 50.0
Type:Trading Company
inquiryCartoon Ingredients Co.,Ltd.is located in NanJing, the capital of Jiangsu Province.with Convenient traffic As a manufacturer, the company mainly engaged in providing Food ingredients, Herbal extracts, Vitamins, APIs and Fine chemicals &a
Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica
Oryza Sativa Extract Specification: Name: Oryza Sativa Extract Identification Standardization Aspect brown
Cas:1135-24-6
Min.Order:1 Kilogram
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Type:Trading Company
inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:1135-24-6
Min.Order:1 Kilogram
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inquiryItems Standard Result Appearance Almost white crystalline powder Complies Melting Point 173
Cas:1135-24-6
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:1135-24-6
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Type:Manufacturers
inquiryProduct name:Ferulic acid CAS:1135-24-6 Quality: TOP Shelf life:2 years Purity:98%, 99% Company info KONO Chem Co., Ltd, is a leading producer of standardized herbal extracts, natural active ingredients and APIs for pharmaceutical,
Product description: Product name Ferulic acid CAS number 1135-24-6 Assay ≥99% Appearance White to yellowish powder Capacity 500mt/year Application Antioxidant, antiseptic, c
Cas:1135-24-6
Min.Order:100 Gram
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inquiryUnique advantages for Ferulic Acid Cas 1135-24-6 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Powder Storage:-20°C Freezer Package:1kg/foil bag, 25kg/drum or as y
Cas:1135-24-6
Min.Order:1 Kilogram
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inquiryComes from Natural Professional Factory We has a complete production and operating system, with an annual output capacity of 2000 tons. It can produce variety of content and proportion of extract according to the demand . Appearance:White fine po
Cas:1135-24-6
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inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Cas:1135-24-6
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Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:1135-24-6
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:1135-24-6
Min.Order:1 Gram
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Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:1135-24-6
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inquiryZorui combines R&D, production and sales into its operations, While continuously providing high-quality raw materials, we also provide and optimize technical solutions for customers to achieve mutual benefit. We adhere to the "quality, integ
Cas:1135-24-6
Min.Order:1 Kilogram
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Type:Other
inquiryWe are wholesaler established since 1987 and leading exporter of: Nutraceutical Ingredients and Botanical Extracts for Anti-aging, Immune Enhancement and Brain Health etc. Appearance:white powder Storage:Store in well-closed containers, in a
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Type:Trading Company
inquiryCHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
Cas:1135-24-6
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Type:Trading Company
inquiryName:Ferulic Acid Alias: Asafula extract English Name: Ferulic Acid Plant sources:A phenolic acid obtained from the resin of ferulic acid CAS No.1135-24-6 Molecular formula: C10H10O4 Molecular weight: 194.19 Packaging Specification: 25kg/d
Cas:1135-24-6
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryProduct Name: Ferulic Acid Synonyms: 4-HYDROXY-3-METHOXYCINNAMIC ACID;3-(4-HYDROXY-3-METHOXYPHENYL)ACRYLIC ACID;(2E)-3-(4-HYDROXY-3-METHOXYPHENYL)ACRYLIC ACID;AURORA 17401;BUTTPARK 121\04-54;(E)-3-(4-HYDROXY-3-METHOXY-PHENYL)-ACRYLIC ACID;LABOTEST
Cas:1135-24-6
Min.Order:1 Kilogram
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:1135-24-6
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Product name Ferulic Acid CAS 1135-24-6 Appearance white powder Melting point 168-172 °C(lit.) Appearance: white powder Storage:
Ferulic Acid Basic information Plant sources Physical and Chemical Properties History Lipid-Lowering effect Antimicrobial effect Food Industry Applications Pharmacological effects Synthetic method Uses Product Name:
Cas:1135-24-6
Min.Order:50 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryAppearance:slightly yellow powder Storage:R T Package:25kg/Barrel Application:Ferulic acid has many health care functions, such as scavenging free radicals, antithrombotic, antibacterial and anti-inflammatory, inhibiting tumors, preventing and treat
Cas:1135-24-6
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryethyl 4-hydroxy-3-methoxycinnamate
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water for 3h; Reflux; | 100% |
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 8h; | 98% |
With Sporotrichum thermophile type C feruloyl esterase; water Enzyme kinetics; | |
With recombinant Tan410 In aq. phosphate buffer at 35℃; for 0.75h; pH=7; Enzymatic reaction; |
Conditions | Yield |
---|---|
With piperidine; pyridine for 0.0833333h; microwave irradiation; | 94% |
With piperidine; p-toluidine In toluene at 80℃; for 3h; Knoevenagel Condensation; | 94% |
With bismuth(III) chloride for 0.0833333h; Doebner condensation; Microwave irradiation; Neat (no solvent); | 93% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
bismuth(lll) trifluoromethanesulfonate In tetrahydrofuran; water at 20℃; for 0.416667h; | 90% |
Conditions | Yield |
---|---|
With lithium hydroxide monohydrate In tetrahydrofuran; methanol; water at 20℃; for 18h; Inert atmosphere; Schlenk technique; Glovebox; | 89% |
With Sporotrichum thermophile type C feruloyl esterase; water Enzyme kinetics; |
malonic acid
3-methoxy-2-hydroxybenzaldehyde
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With 1-n-butyl-3-methylimidazolim bromide at 60℃; for 8h; Knoevenagel-Doebner condensation; | 83% |
curcumin
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
vanillin
Conditions | Yield |
---|---|
With 5,10,15,20-tetra(2',6'-dichlorophenyl)porphyrinatoiron(III) chloride; dihydrogen peroxide; acetylacetone In dichloromethane at 20℃; for 2.5h; | A 2.1% B 3.3% C 70% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With copper(I) oxide; 1-D-O-Methyl-chiro-inositol; sodium hydroxide In water at 120℃; for 6h; | 60% |
3-methyl-4-nitro-5-<2-(3-methoxy-4-hydroxyphenyl)ethenyl>isoxazole
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With sodium hydroxide for 2h; Heating; | 49.7% |
Conditions | Yield |
---|---|
O-methyltransferase pH 7; |
(E,E)-3-(4-hydroxy-3-methoxyphenyl)allyl 3-(4-hydroxy-3-methoxyphenyl)acrylate
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
coniferal alcohol
C
(E)-4-(3-methoxy-1-propenyl)-2-methoxyphenol
Conditions | Yield |
---|---|
Product distribution; hydrolysis by various reaction conditions to various product; |
(E)-3-(4-acetoxy-3-methoxyphenyl)acrylic acid
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With potassium hydroxide for 4h; Heating; |
6'-O-trans-feruloylnodakenin
A
D-Glucose
B
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
C
(+)-marmesin
Conditions | Yield |
---|---|
In sulfuric acid for 0.666667h; Heating; | |
With sulfuric acid for 0.666667h; Heating; |
di-(E)-feruloylspermidine
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 100℃; for 4h; |
(E)-N-(2-(1H-indol-3-yl)ethyl)-3-(4-hydroxy-3-methoxyphenyl)acrylamide
A
tryptamine
B
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
In sodium hydroxide |
N-trans-feruloyl-3-O-methyldopamine
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
3-Methoxytyramine
Conditions | Yield |
---|---|
With sodium hydroxide |
4-hydroxy-3-methoxycinnamic acid 4-O-β-D-glucopyranoside
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
D-glucose
Conditions | Yield |
---|---|
With sulfuric acid In ethanol for 3h; Heating; | A 21 mg B n/a |
demethoxycurcumin
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
p-Coumaric Acid
Conditions | Yield |
---|---|
With sodium hydroxide In water for 2h; Product distribution; Heating; |
A
D-xylose
B
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
C
L-arabinose
Conditions | Yield |
---|---|
With sodium hydroxide; Aspergillus niger "cellulase" Product distribution; |
scopoletin 7-O-(6-O-feruloyl-β-D-glucopyranoside)
A
D-Glucose
B
7-hydroxy-6-methoxy-2H-1-benzopyran-2-one
C
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With hydrogenchloride for 6h; Heating; water bath; |
scopoletin 7-O-(6-O-feruloyl-β-D-glucopyranoside)
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
scopolin
Conditions | Yield |
---|---|
With potassium hydroxide In water at 60℃; for 0.583333h; |
(2E)-3-(4-hydroxy-3-methoxyphenyl)-2-propenoic acid 2-(4-hydroxyphenyl)ethyl ester
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
2-phenylethanol
Conditions | Yield |
---|---|
With sodium hydroxide; ethanol for 0.166667h; | A 488 mg B 530 mg |
O-<5-O-(trans-feruloyl)-α-L-arabinofuranosyl>-(1<*>3)-O-β-D-xylopyranosyl-(1<*>4)-D-xylopyranose
A
D-Xylose
B
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
C
β-L-arabinopyranose
Conditions | Yield |
---|---|
With hydrolysis with cellulase or trifluoroacetic acid Product distribution; |
O-<5-O-(trans-feruloyl)-α-L-arabinofuranosyl>-(1<*>3)-O-β-D-xylopyranosyl-(1<*>4)-D-xylopyranose
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
α-L-arabinofuranosyl-(1→3)-β-D-xylopyranosyl-(1→4)-D-xylopyranose
Conditions | Yield |
---|---|
With sodium hydroxide for 24h; Ambient temperature; |
(E)-6-O-feruloylscandoside methyl ester
A
deacetylasperulosidic acid
B
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With barium dihydroxide Ambient temperature; Yields of byproduct given; |
Conditions | Yield |
---|---|
With hydrogenchloride for 3h; Heating; |
Conditions | Yield |
---|---|
With sodium hydroxide at 100℃; for 4h; Title compound not separated from byproducts; |
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
3-camphanol
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 24h; Heating; | A 30 mg B 10 mg |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 90℃; for 0.5h; |
A
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
B
angrendiol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol for 8h; Ambient temperature; | A 206 mg B 223 mg |
(E)-methyl 3-(3-methoxy-4-((methylsulfonyl)oxy)phenyl)acrylate
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water for 1h; Heating; |
Conditions | Yield |
---|---|
With Dowex 50 W x 8200-400 Heating; | 100% |
With thionyl chloride Ambient temperature; | 100% |
With sulfuric acid at 0℃; for 12h; Darkness; Reflux; | 99% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
ethanol
ethyl 4-hydroxy-3-methoxycinnamate
Conditions | Yield |
---|---|
With acetyl chloride at 20℃; | 100% |
With sulfuric acid at 88℃; under 1034.32 Torr; for 0.05h; Microwave irradiation; | 94% |
With sulfuric acid for 4h; Reflux; | 94% |
Conditions | Yield |
---|---|
With phosphate buffer; Catharanthus roseus at 25℃; for 72h; pH=6.0; | 100% |
With 4-methoxy-phenol In water; N,N-dimethyl-formamide at 150℃; for 4h; | 94% |
With sodium hydroxide In water at 30℃; for 3h; pH=8.5; Microbiological reaction; | 93.1% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
3-(4-hydroxy-3-methoxyphenyl)propionic acid
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate under 760 Torr; | 100% |
With hydrogen; palladium on activated charcoal In ethanol at 20℃; under 2068.59 Torr; | 100% |
With hydrogen; palladium on activated charcoal In methanol; ethyl acetate under 2068.59 Torr; for 5h; | 100% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
acetic anhydride
(E)-3-(4-acetoxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With pyridine at 37℃; Inert atmosphere; | 100% |
With chloro-trimethyl-silane; sodium iodide at 20℃; for 0.333333h; Reagent/catalyst; | 96% |
With sodium hydroxide In water at 20℃; for 1.5h; Cooling with ice; | 95.35% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
dimethyl sulfate
methyl (E)-3-(3,4-dimethoxyphenyl)acrylate
Conditions | Yield |
---|---|
With potassium carbonate In acetone Reflux; | 100% |
With potassium carbonate In acetone for 3h; Reflux; | 90% |
With potassium carbonate In acetone for 36h; | 4.2 g |
With potassium carbonate In acetone |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
benzyl bromide
(E)-3-(3-methoxy-4-benzyloxyphenyl)acrylic acid benzyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 48h; Esterification; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 4h; | 91% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
(E)-3-(3-Methoxy-4-trimethylsilanyloxy-phenyl)-acrylic acid
Conditions | Yield |
---|---|
100% |
3-(2-aminoethyl)-1H-indol-5-ol
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
(2E)-N-[2-(5-hydroxy-1H-indol-3-yl)ethyl]-3-(4-hydroxy-3-methoxyphenyl)-2-propenamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide | 99% |
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 3-(2-aminoethyl)-1H-indol-5-ol With triethylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 57% |
Stage #1: 3-(2-aminoethyl)-1H-indol-5-ol; (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With pyridine; dicyclohexyl-carbodiimide at 20℃; for 24h; Stage #2: With potassium hydroxide In methanol at 20℃; for 4h; |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With sodium In ethanol Reflux; Inert atmosphere; | 99% |
With sodium hydroxide In methanol | 82% |
With sodium hydroxide In water Heating; |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 0 - 20℃; Inert atmosphere; | 99% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
coniferal alcohol
Conditions | Yield |
---|---|
With ATP; NADPH; magnesium chloride In aq. phosphate buffer at 30℃; for 18h; pH=7.5; Green chemistry; Enzymatic reaction; | 98% |
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With chloroformic acid ethyl ester; triethylamine In 1,4-dioxane for 1h; Inert atmosphere; Stage #2: With sodium tetrahydroborate In 1,4-dioxane; N,N-dimethyl-formamide for 1h; Inert atmosphere; | 33% |
Multi-step reaction with 2 steps 1: 96 percent / HCl / 48 h / 20 °C 2: 87 percent / LiAlH4 / diethyl ether / 12 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With tricopper(II) bis(benzene-1,3,5-tricarboxylate) trihydrate; dihydrogen peroxide In ethanol; water; acetonitrile at 100℃; for 1h; | 98% |
With dihydrogen peroxide In ethanol; water; acetonitrile for 4h; Mechanism; Kinetics; Reflux; | 71% |
titanium(IV) oxide In water at 65℃; under 3.75038 Torr; Irradiation; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
at 85℃; for 0.05h; Microwave irradiation; | 98% |
(2-aminomethylpyridine)
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
(E)-3-(4-hydroxy-3-methoxyphenyl)-N-(pyridin-2-ylmethyl)acrylamide
Conditions | Yield |
---|---|
at 85℃; for 0.05h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
at 85℃; for 0.05h; Microwave irradiation; | 98% |
propan-1-ol
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
propyl (2E)-3-(4-hydroxy-3-methoxyphenyl)-prop-2-enoate
Conditions | Yield |
---|---|
With sulfuric acid for 6h; Reflux; | 97% |
With sulfuric acid at 107℃; under 1034.32 Torr; for 0.0666667h; Microwave irradiation; | 94% |
With acetyl chloride for 48h; | 90% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
aniline
3-(4-hydroxy-3-methoxyphenyl)-N-(4-phenyl)prop-(2E)-enamide
Conditions | Yield |
---|---|
at 125℃; for 0.0833333h; Microwave irradiation; | 97% |
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 8h; | 76% |
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 18h; | 44% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 25℃; Inert atmosphere; | 33% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
Trimethylenediamine
N,N'-(trimethylene)-bis[(E)-3-(4-hydroxy-3-methoxyphenyl)acrylamide]
Conditions | Yield |
---|---|
at 110℃; for 0.116667h; Microwave irradiation; | 97% |
Conditions | Yield |
---|---|
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide for 0.5h; Stage #2: 4-ethoxycarbonylpiperazine In N,N-dimethyl-formamide at 20℃; | 96.7% |
Conditions | Yield |
---|---|
With isopropyl alcohol; palladium on activated charcoal Product distribution; Heating; | 96% |
With isopropyl alcohol; palladium on activated charcoal Heating; | 96% |
Multi-step reaction with 2 steps 1: palladium/calcium carbonate; methanol / Hydrogenation 2: soda lime / 280 °C / 20 Torr View Scheme |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
allyl bromide
(E)-3-(4-(allyloxy)-3-methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid; allyl bromide With potassium carbonate In acetonitrile at 70℃; for 18h; Inert atmosphere; Stage #2: With potassium hydroxide In methanol; water; acetonitrile at 660℃; for 24h; Inert atmosphere; | 96% |
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With potassium carbonate In acetone at 20℃; for 0.5h; Stage #2: allyl bromide In acetone for 48h; Williamson ether synthesis; Reflux; Stage #3: With sodium hydroxide In ethanol for 2h; Reflux; | 84% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 3.5h; | 96% |
Conditions | Yield |
---|---|
at 85℃; for 0.05h; Microwave irradiation; | 96% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
(1S,2R,5S)-(+)-menthol
Conditions | Yield |
---|---|
With sulfuric acid-immobilized mesoporous silica catalyst at 70℃; for 1.5h; Green chemistry; | 96% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
(2E)-3-(4-hydroxy-3-methoxyphenyl)acrylohydrazide
Conditions | Yield |
---|---|
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 25℃; for 2h; Stage #2: With hydrazine hydrate In acetonitrile at 0 - 10℃; | 96% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
tert-butyldimethylsilyl chloride
(E)‐3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 25℃; for 14h; | 95% |
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With 1H-imidazole In N,N-dimethyl-formamide Stage #2: tert-butyldimethylsilyl chloride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #3: With potassium carbonate In tetrahydrofuran; methanol; water for 1h; | 93% |
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; | 67% |
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid
4-(2-aminoethyl)-1-(phenylmethyl)piperidine
Conditions | Yield |
---|---|
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 120℃; for 0.116667h; Microwave irradiation; Inert atmosphere; Sealed tube; Stage #2: 4-(2-aminoethyl)-1-(phenylmethyl)piperidine In tetrahydrofuran at 120℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Sealed tube; | 95% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 12h; | 75% |
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