Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryCAS Number 2730-62-3 Product Name 2-chloro-3,3,3-trifluoroprop-1-ene Synonyms 2-chloro-3,3,3-trifluoro-1-propene; 2-chloro-3,3,3-trifluoroprop-1-ene; 1-propene, 2-chloro-3,3,3-trifluor
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:2730-62-3
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:2730-62-3
Min.Order:10 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:2730-62-3
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:2730-62-3
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inquiryProduct Name: 2-CHLORO-3,3,3-TRIFLUOROPROPENE Synonyms: HCFO-1233xf;2-CHLORO-3,3,3-TRIFLUOROPROP-1-ENE;2-CHLORO-3,3,3-TRIFLUOROPROPENE;2-Chloro-3,3,3-trifluoroprop-1-ene 98%;2-Chloro-3,3,3-trifluoroprop-1-ene98%;2-Chloro-3,3,3-trifluoro-1-propene
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inquiry2-CHLORO-3,3,3-TRIFLUOROPROPENE Basic information Product Name: 2-CHLORO-3,3,3-TRIFLUOROPROPENE Synonyms: 2-CHLORO-3,3,3-TRIFLUOROPROP-1-ENE;2-CHLORO-3,3,3-TRIFLUOROPROPENE;R-1233XF;2-Chloro-3,3,3-trifluoroprop-1-ene 98%;2-Chloro-3,3,3-trifluo
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:2730-62-3
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:2730-62-3
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:2730-62-3
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryHangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:2730-62-3
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Type:Lab/Research institutions
inquiryWe are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for
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inquiryFactory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
Cas:2730-62-3
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inquiry2-Chloro-3,3,3-trifluoropropene cas 2730-62-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryWuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Conditions | Yield |
---|---|
With potassium hydroxide; Aliquat 336 In water at 10 - 20℃; Product distribution / selectivity; | 97% |
With alkali | |
With potassium hydroxide In ethanol at -10℃; |
1,1,1,2,2-pentachloropropane
1,1,1,3,3-pentachloropropane
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride at 300℃; for 0.001h; Inert atmosphere; | 94.9% |
1,1,1,2,3-pentachloro-propane
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride In water at 400℃; under 750.075 Torr; for 8h; Inert atmosphere; | 94.3% |
With hydrogen fluoride; fluorinated Cr2O3 at 255℃; | |
With hydrogen fluoride; chromium(III) oxide at 255℃; under 915.2 Torr; for 0.00416667h; Industry scale; |
2,2-dichloro-3,3,3-trifluoropropyl acetate
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With zinc In ethanol Heating; | 73% |
1,1,2,3-Tetrachloropropene
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride; chlorine; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In 1,1,2-trichloro-2,2-difluoroethane at 132.1℃; under 6000.6 Torr; Product distribution / selectivity; | 72.6% |
With hydrogen fluoride; diisopropylamine; chromium(III) oxide at 200 - 300℃; under 760.051 Torr; for 0.000569444 - 0.00277778h; Product distribution / selectivity; | |
With methoxyhydroquinone; hydrogen fluoride; chromium(III) oxide at 243 - 254℃; under 760.051 Torr; for 66.75h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With fluorinated chromia at 200℃; Inert atmosphere; | A 40% B 60% |
1,1,1,2,2-pentachloropropane
1,1,1,3,3-pentachloropropane
A
2-chloro-1,1,1-trifluoropropene
B
trans-1,3,3,3-tetrafluoropropene
C
1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride at 300℃; for 0.001h; Time; Inert atmosphere; | A 29.6% B 6.6% C 60% |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-1,1,1,2-tetrafluoropropane
C
1,1,1,2,3-pentafluoropropane
D
2,3-dichloro-1,1,1-trifluoropropane
E
1-chloro-2,3,3,3-tetrafluoropropane
F
2-chloro-1,1,1,3-tetrafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 100 - 125℃; under 33082.7 - 39185.2 Torr; for 12h; Product distribution / selectivity; | A n/a B n/a C 53% D n/a E n/a F n/a |
1,1,1,2,2-pentachloropropane
1,1,1,3,3-pentachloropropane
A
2-chloro-1,1,1-trifluoropropene
B
1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride at 250℃; for 0.00277778h; Temperature; Time; Inert atmosphere; | A 50% B 49.8% |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-2,3,3-trifluoro-butane
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride; chlorine; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In 1,1,2-trichloro-2,2-difluoroethane at 133.2℃; under 6000.6 Torr; Product distribution / selectivity; | A 25.5% B 6.6% |
Conditions | Yield |
---|---|
With antimony dichloride trifluoride; antimony(III) fluoride | |
With antimonypentachloride; antimony(III) fluoride at 170℃; for 4h; |
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
3,3,3-trifluoroprop-1-yne
Conditions | Yield |
---|---|
With potassium hydroxide |
2,3,3,3-tetrachloropropene
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
With antimony dichloride trifluoride; antimony(III) fluoride |
6-chloro-5-trifluoromethyl-1,6-diazabicyclo<3.1.0>hexane
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
In Cyclohexane-d12 at 80℃; for 80h; Product distribution; Mechanism; |
2,3-dichloro-3,3-difluoroprop-1-ene
antimony(III) fluoride
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
at 30℃; |
2,3,3,3-tetrachloropropene
antimony(III) fluoride
1,2-dichloro-ethane
2-chloro-1,1,1-trifluoropropene
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
3,3,3-trifluoroprop-1-yne
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
(Z)-1-chloro-3,3,3-trifluoro-1-propene
C
2,3,3,3-tetrafluoro-propene
D
1,1,1,2,2-pentafluoropropane
E
1,1,1,3,3-Pentafluoropropane
F
trans-1,3,3,3-tetrafluoropropene
G
(Z)-1,3,3,3-tetrafluoropropene
H
trans-1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; 2percentCo2O3/Cr2O3, fluorided at 325 - 400℃; Product distribution / selectivity; |
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
2,3,3,3-tetrafluoro-propene
C
1,1,1,2,2-pentafluoropropane
D
1,1,1,3,3-Pentafluoropropane
E
trans-1,3,3,3-tetrafluoropropene
F
(Z)-1,3,3,3-tetrafluoropropene
G
2-chloro-1,1,1,3-tetrafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride; 2percentCo2O3/Cr2O3, fluorided at 275℃; Product distribution / selectivity; |
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
1,1,1-trifluoropropylene
C
2-chloro-1,1,1,3-tetrafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride at 140℃; Gas phase; | |
With hydrogen fluoride at 140℃; Inert atmosphere; |
1,1,1-trifluoropropylene
A
2-chloro-1,1,1-trifluoropropene
B
(Z)-1-chloro-3,3,3-trifluoro-1-propene
C
2,3,3,3-tetrafluoro-propene
D
(Z)-1,2-dichloro-3,3,3-trifluoropropene
E
1,1,1,2,2-pentafluoropropane
F
1,1,1,3,3-Pentafluoropropane
G
trans-1,3,3,3-tetrafluoropropene
H
trans-1,2-dichloro-3,3,3-trifluoropropene
I
(Z)-1,3,3,3-tetrafluoropropene
K
trans-1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; chlorine; 2percentCo2O3/Cr2O3, fluorided at 350 - 375℃; Product distribution / selectivity; |
1,1,1-trifluoropropylene
A
2-chloro-1,1,1-trifluoropropene
B
(Z)-1-chloro-3,3,3-trifluoro-1-propene
C
2,3,3,3-tetrafluoro-propene
D
(Z)-1,2-dichloro-3,3,3-trifluoropropene
E
1,1,1,2,2-pentafluoropropane
F
1,1,1,3,3-Pentafluoropropane
G
trans-1,3,3,3-tetrafluoropropene
H
trans-1,2-dichloro-3,3,3-trifluoropropene
I
(Z)-1,3,3,3-tetrafluoropropene
J
trans-1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; chlorine; 2percentCo2O3/Cr2O3, fluorided at 300℃; Product distribution / selectivity; |
1,1,1-trifluoropropylene
A
1,2,2-trichloro-3,3,3-trifluoropropane
B
2-chloro-1,1,1-trifluoropropene
C
2,3-dichloro-1,1,1-trifluoropropane
D
(Z)-1-chloro-3,3,3-trifluoro-1-propene
E
2,3,3,3-tetrafluoro-propene
F
(Z)-1,2-dichloro-3,3,3-trifluoropropene
G
trans-1,2-dichloro-3,3,3-trifluoropropene
H
2-chloro-1,1,1,3-tetrafluoropropane
I
trans-1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; chlorine at 140℃; Gas phase; |
1,1,1-trifluoropropylene
A
1,2,2-trichloro-3,3,3-trifluoropropane
B
2-chloro-1,1,1-trifluoropropene
C
2,3-dichloro-1,1,1-trifluoropropane
D
(Z)-1-chloro-3,3,3-trifluoro-1-propene
E
2,3,3,3-tetrafluoro-propene
F
2-chloro-1,1,1,3-tetrafluoropropane
G
trans-1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With hydrogen fluoride; chlorine at 140℃; Gas phase; |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
1,2-dichloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
Stage #1: 1,1,2,3-Tetrachloropropene With hydrogen fluoride; chromium(III) oxide at 350℃; under 2311.54 Torr; for 0.00177778h; Stage #2: FeCl3/C at 180℃; under 2311.54 Torr; for 0.00244444h; Product distribution / selectivity; | |
With fluorinated Cr2O3 at 260℃; for 0.005h; Inert atmosphere; Gas phase; | |
With hydrogen fluoride at 260℃; under 760.051 Torr; for 0.005h; Catalytic behavior; |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-1,1,1,2-tetrafluoropropane
C
1,2-dichloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
Stage #1: 1,1,2,3-Tetrachloropropene With hydrogen fluoride; 4-methoxy-phenol; chromium(III) oxide at 350℃; under 1794.37 Torr; for 0.00177778h; Stage #2: FeCl3/C at 180℃; under 1794.37 Torr; for 0.00244444h; Product distribution / selectivity; |
2-chloro-1,1,1,2-tetrafluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
2,3,3,3-tetrafluoro-propene
Conditions | Yield |
---|---|
magnesium fluoride at 450 - 530℃; under 760.051 Torr; for 1 - 14h; Product distribution / selectivity; | |
iron(III) trifluoride at 350 - 385℃; under 760.051 Torr; for 1 - 2h; Product distribution / selectivity; | |
chromium oxide, fluorinated at 250 - 317℃; under 760.051 Torr; for 1 - 2h; Product distribution / selectivity; |
1,1,2,3-Tetrachloropropene
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-1,1,1,2-tetrafluoropropane
C
2,3,3,3-tetrafluoro-propene
D
1,1,1,2,2-pentafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride at 100 - 120℃; under 16274.9 Torr; for 5h; Product distribution / selectivity; |
2,3-dichloro-1,1,1-trifluoropropane
A
2-chloro-1,1,1-trifluoropropene
B
2-chloro-1,1,1,2-tetrafluoropropane
Conditions | Yield |
---|---|
With hydrogen fluoride; activated by HF Zn/chromia catalyst at 100 - 340℃; | A 70 %Chromat. B 10 %Chromat. |
1,1,1-trifluoropropylene
A
2-chloro-1,1,1-trifluoropropene
B
1-chloro-3,3,3-trifluoropropene
Conditions | Yield |
---|---|
With chlorine; activated carbon catalyst at 250℃; under 760.051 Torr; Product distribution / selectivity; Inert atmosphere; | |
With chlorine; pyrographite at 250℃; under 760.051 Torr; Inert atmosphere; |
2-chloro-1,1,1-trifluoropropene
N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine
Conditions | Yield |
---|---|
With trifluoroacetic acid In tetrahydrofuran at 0℃; for 2h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 2,5-dichlorbenzenethiol With potassium hydroxide In isopropyl alcohol at 20℃; for 0.166667h; Stage #2: 2-chloro-1,1,1-trifluoropropene With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone In isopropyl alcohol at 50℃; for 4h; stereoselective reaction; | 97% |
2-chloro-1,1,1-trifluoropropene
4-methoxyphenylboronic acid
1-(1,1,1-trifluoroprop-2-en-2-yl)-4-methoxybenzene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Catalytic behavior; Reagent/catalyst; Solvent; Suzuki-Miyaura Coupling; Autoclave; | 95% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 93% |
2-chloro-1,1,1-trifluoropropene
[4-(benzyloxy)phenyl]boronic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 91% |
2-chloro-1,1,1-trifluoropropene
3,4-(methylenedioxy)-benzeneboronic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 89% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 89% |
2-chloro-1,1,1-trifluoropropene
3,4-Dimethoxyphenylboronic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 88% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 88% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 70 - 90℃; for 8h; | 87% |
4-methylpyridine-2-thiol
2-chloro-1,1,1-trifluoropropene
Conditions | Yield |
---|---|
Stage #1: 4-methylpyridine-2-thiol With potassium hydroxide In isopropyl alcohol at 20℃; for 0.166667h; Stage #2: 2-chloro-1,1,1-trifluoropropene With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone In isopropyl alcohol at 50℃; for 4h; stereoselective reaction; | 86% |
2-chloro-1,1,1-trifluoropropene
3-methoxyphenylboronic acid
1-methoxy-3-(1,1,1-trifluoroprop-2-en-2-yl)benzene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 85% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 85% |
2-chloro-1,1,1-trifluoropropene
[3-(methoxycarbonyl)phenyl]boronic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 84% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 84% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 84% |
2-chloro-1,1,1-trifluoropropene
4-biphenylboronic acid
4-(3,3,3-trifluoroprop-1-en-2-yl)-1,1’-biphenyl
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 83% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 83% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 83% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 83% |
Conditions | Yield |
---|---|
Stage #1: 4-Methoxybenzenethiol With potassium hydroxide In isopropyl alcohol at 20℃; for 0.166667h; Stage #2: 2-chloro-1,1,1-trifluoropropene With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone In isopropyl alcohol at 50℃; for 4h; stereoselective reaction; | A 83% B 13% |
2-chloro-1,1,1-trifluoropropene
4-formylphenylboronic acid,
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 82% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 82% |
2-chloro-1,1,1-trifluoropropene
(4-isopropylphenyl)boronic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In 1,4-dioxane; water at -100 - 100℃; for 5h; Suzuki-Miyaura Coupling; Autoclave; | 81% |
2-chloro-1,1,1-trifluoropropene
phenol
(Z)-((3,3,3-trifluoroprop-1-en-1-yl)oxy)benzene
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 81% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 81% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate In N,N-dimethyl-formamide at -100 - 100℃; for 5h; Autoclave; Sealed tube; | 80% |
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