CAS No.121-82-4,HEXAHYDRO-1,3,5-TRINITRO-1,3,5-TRIAZINE Suppliers,MSDS download

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Synthetic route

: 100-97-0
hexamethylenetetramine

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
Stage #1: hexamethylenetetramine With nitric acid at 20℃; for 0.666667h; Stage #2: With sodium nitrite at 20 - 70℃;	82%
With ammonium nitrate; Iron(III) nitrate nonahydrate; nitric acid; acetic anhydride	69%
With nitric acid

: 100-97-0
hexamethylenetetramine

: 108-24-7
acetic anhydride

: 141-43-5
ethanolamine

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With nitric acid In acetic acid at 50 - 60℃; for 1.5h;	A n/a B n/a C 75%

...Expand

: 100-97-0
hexamethylenetetramine

: 141-43-5
ethanolamine

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With nitric acid In acetic anhydride; acetic acid at 50 - 60℃; for 1.5h;	A n/a B n/a C 75%

...Expand

: diammonium 1,3,5,7-tetraazabicyclo[3.3.1]nonane-3,7-disulfonate sulfate

A: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

B: 2691-41-0
octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid In acetic anhydride; acetic acid at 70℃; for 0.333333h;	A 70% B 30%

: 30805-19-7
1,3,5-tripropionylperhydro-1,3,5-triazine

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid; trifluoroacetic anhydride In nitromethane at 0 - 20℃; for 4h;	63%

: 4719-04-4
1,3,5-tris(2-hydroxyethyl)-1,3,5-triazacyclohexane

: 108-24-7
acetic anhydride

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid In chloroform at 55 - 60℃; for 1h;	A 41.3% B n/a C 62%

...Expand

: 4719-04-4
1,3,5-tris(2-hydroxyethyl)-1,3,5-triazacyclohexane

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid In chloroform; acetic anhydride at 55 - 60℃; for 1h;	A 41.3% B n/a C 62%

...Expand

: 32516-05-5
3,7-diacetyl-1,3,5,7-tetraaza-bicyclo[3.3.1]nonane

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; copper(II) nitrate trihydrate; nitric acid; acetic anhydride at 65℃; for 4h; Molecular sieve;	62%

: 26028-46-6
1,3,5-tri-acetyl-1,3,5-triaza cyclohexane

A: 14168-42-4
1-acetyl-3,5-dinitrohexahydro-1,3,5-triazine

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; trifluoroacetic anhydride In nitromethane for 0.75h; Ambient temperature;	A 61% B 8%

: 108-24-7
acetic anhydride

: C5H11N3O7S2(2-)*2K(1+)

A: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

B: 1,3-dinitro-5-(2-nitro-ethyl)-[1,3,5]triazinane

C: C7H13N7O10

Conditions

Conditions	Yield
With nitric acid at 8 - 25℃; for 0.5h; Nitration; Acetoxylation;	A n/a B 41% C 48%

...Expand

: 108-24-7
acetic anhydride

: C6H13N3O7S2(2-)*2K(1+)

A: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

B: 1,3-dinitro-5-(3-nitro-propyl)-[1,3,5]triazinane

C: C8H15N7O10

Conditions

Conditions	Yield
With nitric acid at 8 - 25℃; for 0.5h; Nitration; Acetoxylation;	A n/a B 36% C 45%

...Expand

: 108-24-7
acetic anhydride

: dipotassium 1-methyl-1,3,5-triazacyclohexane-3,5-disulfonate

A: 14133-70-1
1-acetoxy-2,4,6-trinitro-2,4,6-triazaheptane

B: 98019-34-2
1-methyl-3,5-dinitro-1,3,5-triazacyclohexane

C: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

D: 1-acetoxy-2,4-dinitro-2,4-diazapentane

Conditions

Conditions	Yield
With nitric acid at 8 - 25℃; for 0.5h; Nitration; Acetoxylation;	A 39% B 4% C n/a D n/a

...Expand

: 108-24-7
acetic anhydride

: C5H11N3O6S2(2-)*2K(1+)

A: 117920-64-6
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-octane

B: 99512-95-5
1-ethyl-3,5-dinitro-hexahydro-[1,3,5]triazine

C: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid at 8 - 25℃; for 0.5h; Nitration; Acetoxylation;	A 38% B 30% C n/a

...Expand

: diammonium 1,3,5,7-tetraazabicyclo[3.3.1]nonane-3,7-disulfonate sulfate

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid at -40℃; for 1.5h;	38%

: 108-24-7
acetic anhydride

: C7H15N3O6S2(2-)*2K(1+)

A: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

B: 1-butyl-3,5-dinitro-[1,3,5]triazinane

C: C9H18N6O8

Conditions

Conditions	Yield
With nitric acid at 8 - 25℃; for 0.5h; Nitration; Acetoxylation;	A n/a B 25% C 35%

...Expand

: 66204-43-1
N,N'-methylene-bis(oxazolidine)

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid In acetic anhydride at 50 - 60℃; for 1.5h; Yield given;	A 27% B n/a C n/a

...Expand

: 66204-43-1
N,N'-methylene-bis(oxazolidine)

: 108-24-7
acetic anhydride

A: 71545-63-6
1-acetoxy-2-nitro-2-aza-4-nitroxybutabe

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

C: 76237-14-4
1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid at 50 - 60℃; for 1.5h; Yields of byproduct given;	A 27% B n/a C n/a
With ammonium nitrate; nitric acid at 50 - 60℃; for 1.5h; Yield given;	A 27% B n/a C n/a

...Expand

: 50-00-0
formaldehyd

: 14168-44-6
MEDINA

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; acetic anhydride; acetic acid

: 50-00-0
formaldehyd

: aminomethyl-nitro-(nitroamino-methyl)-amine; nitrate

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With acetic anhydride

: 50-00-0
formaldehyd

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; acetic anhydride

: 7020-51-1
2-thia-1,3,5,7-tetraaza-adamantane-2,2-dioxide

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid

: 13980-04-6
1,3,5-trinitroso-1,3,5-triazinane

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With dihydrogen peroxide; nitric acid at -40℃;

: 100-97-0
hexamethylenetetramine

: 79-05-0
Propionamid

A: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

B: 5755-28-2
1‑nitroso‑3,5,7‑trinitro‑1,3,5,7‑tetraazacyclooctane

Conditions

Conditions	Yield
With ammonium nitrate; nitric acid; acetic anhydride; acetic acid

...Expand

: 5755-27-1
1-nitroso-3,5-dinitro-1,3,5-triazacyclohexane

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With sulfuric acid; nitric acid
With dihydrogen peroxide; nitric acid at -40℃;

: 18423-20-6, 18423-21-7, 75853-48-4, 84376-11-4, 94388-82-6
hexamethylenetetramine; dinitrate

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; water; nitric acid; acetic anhydride

: 18423-20-6, 18423-21-7, 75853-48-4, 84376-11-4, 94388-82-6
hexamethylenetetramine; dinitrate

: 108-24-7
acetic anhydride

A: 1-acetoxy-2,4,6-trinitro-7-nitryloxy-2,4,6-triaza-heptane

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid

...Expand

: 55-21-0
benzamide

A: 1575-94-6
N,N'-methylenebisbenzamide

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With ammonium nitrate; hexamethylenetetramine; nitric acid at 65℃; weiteres Reagens: Acetanhydrid, Essigsaeure;

: 100-97-0
hexamethylenetetramine

A: 949-56-4
3,7-dinitro-1,3,5,7-tetraaza-bicyclo[3.3.1]nonane

B: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

Conditions

Conditions	Yield
With nitric acid at 0 - 10℃; Mechanism; isotope labelling experiments;
With nitric acid at 0 - 10℃;
With (2S)-N-methyl-1-phenylpropan-2-amine hydrate; nitric acid 1.) 0 - 10 deg C; Multistep reaction;

: 283-66-9
3,4,8,9,12,13-Hexaoxa-1,6-diaza-bicyclo[4.4.4]tetradecane

: 7697-37-2
nitric acid

NH4NO3: NH4NO3

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

...Expand

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

: 100-97-0
hexamethylenetetramine

Conditions

Conditions	Yield
With borohydride exchange resin; nickel diacetate In methanol for 3h;	100%

: 121-82-4
Hexahydro-1,3,5-trinitro-1,3,5-triazine

: N,N'-dinitromethylenediamine dipotassium salt

Conditions

Conditions	Yield
With potassium hydroxide In ethanol; acetone at 20 - 30℃; for 1h;	30%

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CADMIUM STANNATE

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CAS No.:121-82-4
Name:HEXAHYDRO-1,3,5-TRINITRO-1,3,5-TRIAZINE
Article Data:42
Molecular Structure:
Formula:C3H6 N6 O6
Molecular Weight:222.117
Synonyms:s-Triazine,hexahydro-1,3,5-trinitro- (8CI);1,3,5-Triaza-1,3,5-trinitrocyclohexane;1,3,5-Trinitro-1,3,5-triazacyclohexane;1,3,5-Trinitrohexahydro-1,3,5-triazine;1,3,5-Trinitrohexahydro-s-triazine;1,3,5-Trinitroperhydro-1,3,5-triazine;A 3;A 3 (explosive);A-IX 1;A-IX 2;CH 6 (explosive);CPX 301;CX 84A;Composition A 3;Cyclonite;Cyclotrimethylenenitramine;Cyclotrimethylenetrinitramine;Giekfol;Heksoflen;Hexahydro-1,3,5-trinitro-1,3,5-s-triazine;Hexahydro-1,3,5-trinitro-1,3,5-triazine;Hexahydro-1,3,5-trinitro-s-triazine;Hexogen;Hexogen (explosive);Hexogen 5W;NSC 312447;PBX 9407;PBX(AF) 108;PBX-B 2238;PBX-C 117;PBX-L 3;PBX-L 5;PBX-MC;PBX-MVF;PBX-W 108;PBXC 116;PBXN 107;PBXN 107A;PBXN 108;PBXN 201;PBXN 6;PBXN 8;PBXN(AF) 108;PBXW108(E);PE 4;PE 4 (explosive);PHX 34;PMW 8;RDX;T4;TS 1;TS 1(propellant);Trimethylenetrinitramine;V 29;V 29 (propellant);
EINECS:204-500-1
Density:1.89g/cm³
Melting Point:205 C
Boiling Point:747°Cat760mmHg
Flash Point:405.6°C
Solubility:insoluble
Appearance:
Hazard Symbols:High explosive, easily initiated by mercury fulminate. Toxic by inhalation and skin contact. TLV: 1.5 mg/m³.
Risk Codes11-23/24/25-36/37/38
Safety: Poison by ingestion, intraperitoneal, and intravenous routes. An experimental teratogen. Other experimental reproductive effects. A corrosive irritant to skin, eyes, and mucous membranes. Cases of epileptiform convulsions have been reported from exposure. It is one of the most powerful high explosives in use today. Has more shattering power than TNT and is often mixed with TNT as a bursting charge for aerial bombs, mines, and torpedoes. It is easily initiated by mercury fulminate, which may be used as a booster. When heated to decomposition it emits toxic fumes of NO_x. See also AMINES, NITRATES, and EXPLOSIVES, HIGH.
Transport Information:
PSA:147.18000
LogP:-0.26310

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