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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

N,N-Diethylformamide Manufacturer/High quality/Best price/In stock

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Product description: Product name N,N-Diethylformamide CAS number 617-84-5 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Organic intermediate

N,N-Diethylformamide

Cas:617-84-5

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N,N-Diethylformamide

Cas:617-84-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

N,N-Diethylformamide with good quality and competitive price from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china an

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 617-84-5 with best price

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Antimex Chemical Limied

Antimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and Intermediates. food additives,water treatment chemicals. Fluori

N,N-DiethylforMaMide

Cas:617-84-5

Min.Order:100 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Formamide, N,N-diethyl- 617-84-5

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Ocean Chemical Co., Ltd.

N,N-Diethyl formamide (DEF) N, N-diethyl methylamine materialized properties Density: 0.908 g/mL at 25 degrees C (lit.) Boiling point: 176-177 degrees C (lit.) Melting point: 176-177 degrees C Flash point: 141 degrees F Refractive index: n20/D 1

N,N-Diethyl formamide (DEF)

Cas:617-84-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

N,N-Diethylformamide with CAS:617-84-5

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $14.0 / 20.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

N,N-Diethylformamide CAS:617-84-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm

N,N-Diethylformamide CAS:617-84-5

Cas:617-84-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Formamide, N,N-diethyl-

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 617-84-5 N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:617-84-5

Cas:617-84-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

BEST quality N,N-Diethylformamide 617-84-5

Cas:617-84-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:clear colorless to pale yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Appli

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

N,N-Diethylformamide

Cas:617-84-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

N,N-Diethylformamide

Cas:617-84-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply N,N-Diethylformamide

Cas:617-84-5

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products N,N-Diethylformamide

Cas:617-84-5

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

N,N-Diethylformamide

Cas:617-84-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

BEST quality N,N-Diethylformamide 617-84-5

Cas:617-84-5

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: N,N-Diethylformamide CAS No.: 617-84-5 Molecule Formula:C5H11NO Molecule Weight:101.15 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING IT

Lower Price N,N-Diethylformamide in stock

Cas:617-84-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Chemical Name: N,N-Diethylformamide Molecular Fomula:C5H11NO Appearance: Yellow Liquid Appearance:Colorless Clear to light yellow Liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25KG/Drum Application:Agroch

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best OfferN,N-Diethylformamide

Cas:617-84-5

Min.Order:0

Negotiable

Type:Trading Company

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

N,N-Diethylformamide Chemical Properties Melting point 176-177°C Boiling point 176-177 °C (lit.) density 0.908 g/mL at 25 °C (lit.) refractive index n20/D 1.434(lit.) Fp 141 °F storage temp. Store below +30&deg

N,N-Diethylformamide

Cas:617-84-5

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

BEST quality N,N-Diethylformamide 617-84-5

Cas:617-84-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Synthetic route

carbon dioxide
124-38-9

carbon dioxide

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With C21H24N2; phenylsilane In tetrahydrofuran at 20℃; under 750.075 - 2250.23 Torr; for 1.5h; Solvent; Concentration; Reagent/catalyst; Temperature; Time; Inert atmosphere; Glovebox;100%
With phenylsilane at 25℃; under 37503.8 Torr; for 12h; Pressure; Temperature; Autoclave;100%
With Zn(salen); phenylsilane; tetrabutylammomium bromide at 25℃; under 3750.38 Torr; for 15h; Reagent/catalyst; Autoclave;99%
formaldehyd
50-00-0

formaldehyd

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With potassium tetrachloroaurate(III); potassium carbonate In water; acetonitrile at 40℃; for 12h;98%
With sodium hydroxide In water at 25℃; for 6h;91%
With potassium iodide In water Ambient temperature; electrolysis;85%
N-<(trimethylsilyl)methyl>-N,N-diethylamine
10545-36-5

N-<(trimethylsilyl)methyl>-N,N-diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With copper(I) bromide In acetonitrile at 25℃; for 4h; chemoselective reaction;94%
formic acid
64-18-6

formic acid

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With Thiamine hydrochloride at 80℃; for 0.5h;90%
With sulfated polyborate In neat (no solvent) at 70℃; for 0.333333h;86%
With silica gel for 0.0236111h; microwave irradiation;80%
C10H20CuN2O2(1-)*Li(1+)

C10H20CuN2O2(1-)*Li(1+)

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With hydrogenchloride; diethyl ether In diethyl ether at -78℃; for 0.5h;85%
dihydroxyacetone
96-26-4

dihydroxyacetone

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With Cu/Al2O3; dihydrogen peroxide In water at 25℃; for 24h; Green chemistry;83%
4-tert-butyl-2-(2-nitrophenylazo)phenol
27959-42-8

4-tert-butyl-2-(2-nitrophenylazo)phenol

A

2-Methyl-1H-benzimidazole
615-15-6

2-Methyl-1H-benzimidazole

B

N-formyldiethylamine
617-84-5

N-formyldiethylamine

C

2-(5-tert-butyl-2-hydroxyphenyl)benzotriazole
3147-76-0

2-(5-tert-butyl-2-hydroxyphenyl)benzotriazole

D

2-nitro-aniline
88-74-4

2-nitro-aniline

Conditions
ConditionsYield
With carbon monoxide; triethylamine In 1,2-dichloro-benzene at 200℃; under 60800 Torr; for 8h; Further byproducts given;A n/a
B n/a
C 63%
D 82%
bis(diethylamin)nickeldibromid
14873-98-4

bis(diethylamin)nickeldibromid

diethylamine
109-89-7

diethylamine

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

N,N,N',N'-tetraethylurea
1187-03-7

N,N,N',N'-tetraethylurea

C

N,N,N',N'-tetraethyloxamide
14288-05-2

N,N,N',N'-tetraethyloxamide

D

diethylamine hydrobromide
6274-12-0

diethylamine hydrobromide

E

tetracarbonyl nickel
13463-39-3, 71564-36-8

tetracarbonyl nickel

Conditions
ConditionsYield
With carbon monoxide In tetrahydrofuran; diethyl ether reaction in THF/Et2O = 2/1 soln., room temp., under CO (1 bar);A 7%
B 0.5%
C 80%
D n/a
E n/a
triethylamine
121-44-8

triethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With manganese(IV) oxide; oxygen In chlorobenzene at 100℃; under 4500.45 Torr; for 4h; Autoclave; Green chemistry;80%
With Eosin Y In ethanol at 23℃; Irradiation;16%
With pyridine; copper(II) bis(trifluoromethanesulfonate) In acetonitrile at 130℃; under 7500.75 - 30003 Torr; Catalytic behavior; Reagent/catalyst; Pressure; Temperature; Autoclave;
N-formylformamide
18197-22-3

N-formylformamide

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
Ambient temperature;78%
N-formylbenzotriazole
72773-04-7

N-formylbenzotriazole

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 0.15h;78%
trimethylsilyl formate
18243-21-5

trimethylsilyl formate

(diethylamino)triethylsilane
6022-10-2

(diethylamino)triethylsilane

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

Hexamethyldisiloxane
107-46-0

Hexamethyldisiloxane

C

1,1,1-triethyl-3,3,3-trimethyl-disiloxane
2652-41-7

1,1,1-triethyl-3,3,3-trimethyl-disiloxane

D

hexaethyl disiloxane
994-49-0

hexaethyl disiloxane

Conditions
ConditionsYield
With N-Methylformamide at 20℃; for 2h;A 72.5%
B 13.6%
C n/a
D 23.8%
With N-Methylformamide at 20℃; for 2h; Product distribution; Mechanism; various amides as catalysts, other temperature, other time;A 72.5%
B 13.6%
C n/a
D 23.8%
trimethylsilyl formate
18243-21-5

trimethylsilyl formate

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

Hexamethyldisiloxane
107-46-0

Hexamethyldisiloxane

C

1,1,1-triethyl-3,3,3-trimethyl-disiloxane
2652-41-7

1,1,1-triethyl-3,3,3-trimethyl-disiloxane

D

hexaethyl disiloxane
994-49-0

hexaethyl disiloxane

Conditions
ConditionsYield
With N-Methylformamide; (diethylamino)triethylsilane at 20℃; for 2h;A 72.5%
B 13.6%
C n/a
D 23.8%
(diethylamino)triethylsilane
6022-10-2

(diethylamino)triethylsilane

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

Hexamethyldisiloxane
107-46-0

Hexamethyldisiloxane

C

1,1,1-triethyl-3,3,3-trimethyl-disiloxane
2652-41-7

1,1,1-triethyl-3,3,3-trimethyl-disiloxane

D

hexaethyl disiloxane
994-49-0

hexaethyl disiloxane

Conditions
ConditionsYield
With N-Methylformamide; trimethylsilyl formate at 20℃; for 2h;A 72.5%
B 13.6%
C n/a
D 23.8%
diethylamine
109-89-7

diethylamine

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With dioxo[bis(sulfato-κO)]molybdenum In ethanol for 5h; Reflux; Green chemistry;70%
diethylamine
109-89-7

diethylamine

2,2-Dichloro-3-oxo-butyraldehyde
160663-31-0

2,2-Dichloro-3-oxo-butyraldehyde

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

1,1-Dichloroacetone
513-88-2

1,1-Dichloroacetone

Conditions
ConditionsYield
In tetrachloromethane for 12h; Ambient temperature;A 68%
B 60%
carbon monoxide
201230-82-2

carbon monoxide

diethylamine
109-89-7

diethylamine

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

N,N,N',N'-tetraethylurea
1187-03-7

N,N,N',N'-tetraethylurea

C

N,N,N',N'-tetraethyloxamide
14288-05-2

N,N,N',N'-tetraethyloxamide

Conditions
ConditionsYield
With (Et2NH)2CuBr; (Et2NH)2NiBr In tetrahydrofuran under 15001.2 Torr; for 16h; Ambient temperature;A n/a
B n/a
C 66%
carbon monoxide
201230-82-2

carbon monoxide

diethylamine
109-89-7

diethylamine

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

N,N,N',N'-tetraethyloxamide
14288-05-2

N,N,N',N'-tetraethyloxamide

Conditions
ConditionsYield
With (Et2NH)2CuBr; (Et2NH)2NiBr In tetrahydrofuran under 15001.2 Torr; for 16h; Ambient temperature;A n/a
B 66%
2-aminopyridine
504-29-0

2-aminopyridine

triethylamine
121-44-8

triethylamine

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

imidazo[1,2-a]pyridine-3-carbaldehyde

imidazo[1,2-a]pyridine-3-carbaldehyde

Conditions
ConditionsYield
With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; oxygen In dimethyl sulfoxide at 100℃; for 24h; Sealed tube;A n/a
B 66%
chloroform
67-66-3

chloroform

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With sodium ethanolate at 50℃; Riemer-Tiemann reaction; Inert atmosphere;62%
With potassium tert-butylate; water; benzene
With sodium hydroxide
Hex-1-en-2-yl formate
134965-38-1

Hex-1-en-2-yl formate

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
In ethyl acetate for 1h; Ambient temperature;62%
sec.-butyllithium
598-30-1

sec.-butyllithium

N,N-diethylcarbamyl chloride
88-10-8

N,N-diethylcarbamyl chloride

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

2-methyl-butyric acid diethylamide
59002-07-2

2-methyl-butyric acid diethylamide

Conditions
ConditionsYield
Stage #1: sec.-butyllithium With CuCN In tetrahydrofuran at -30℃; for 0.5h;
Stage #2: N,N-diethylcarbamyl chloride In tetrahydrofuran at -30 - 0℃; for 2h;
A 11 % Chromat.
B 62%
N,N-diethylthioformamide
13839-14-0

N,N-diethylthioformamide

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With triphenyltin(IV) hydroxide In benzene-d6 at 90℃; for 8h;60%
carbon monoxide
201230-82-2

carbon monoxide

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
With tetracarbonyl nickel In toluene at 180℃; for 24h;55%
With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In methanol at 0 - 130℃; under 22502.3 Torr; for 36h; Autoclave;12.1%
In tetrahydrofuran under 760 Torr; for 24h; Product distribution; Mechanism; Ambient temperature; other conditions: other catalyst, other times, addition of complexing agents, addition of LiBr;
diethylamine
109-89-7

diethylamine

(1-phenyl-2-methyl-4-phenyl-1-azabuta-1,3-diene)tricarbonyliron(0)

(1-phenyl-2-methyl-4-phenyl-1-azabuta-1,3-diene)tricarbonyliron(0)

A

N-formyldiethylamine
617-84-5

N-formyldiethylamine

B

(1E,2E)-N,3-diphenylprop-2-en-1-imine
953-21-9

(1E,2E)-N,3-diphenylprop-2-en-1-imine

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran at 0℃; for 3h;A 50%
B n/a
carbon monoxide
201230-82-2

carbon monoxide

bis(diethylamin)nickel bromid

bis(diethylamin)nickel bromid

acetylene
74-86-2

acetylene

A

4-butanolide
96-48-0

4-butanolide

B

N-formyldiethylamine
617-84-5

N-formyldiethylamine

C

tetraethyl-butynediamide
25883-23-2

tetraethyl-butynediamide

D

N,N-diethylpropiolamide
51590-64-8

N,N-diethylpropiolamide

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether under 750.06 Torr; Ambient temperature;A 8.9 % Chromat.
B 2.4 % Chromat.
C 45%
D 11%
diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
12%
chloral
75-87-6

chloral

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

diethyl ether
60-29-7

diethyl ether

chloroacetylene
593-63-5

chloroacetylene

diethylamine
109-89-7

diethylamine

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Conditions
ConditionsYield
durch folgendes Erwaermen;
N-formyldiethylamine
617-84-5

N-formyldiethylamine

1,1-dichloromethyl-N,N-diethylamine
40416-60-2

1,1-dichloromethyl-N,N-diethylamine

Conditions
ConditionsYield
With thionyl chloride In dichloromethane at 20℃; for 2h; Inert atmosphere;100%
With (pentachloroethyl)phosphorimidic trichloride In benzene
N-formyldiethylamine
617-84-5

N-formyldiethylamine

(tert-butyldimethylsilyl)(phenyl)methanone
132868-67-8

(tert-butyldimethylsilyl)(phenyl)methanone

N-(p-methoxybenzylidene)diphenylphosphinamide
119701-95-0

N-(p-methoxybenzylidene)diphenylphosphinamide

N,N-diethyl-2-phenyl-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-phenyl-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(phenyl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
100%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

N-(p-methoxybenzylidene)diphenylphosphinamide
119701-95-0

N-(p-methoxybenzylidene)diphenylphosphinamide

tert-butyldimethylsilyl 4-fluorophenyl ketone

tert-butyldimethylsilyl 4-fluorophenyl ketone

N,N-diethyl-2-(4-fluorophenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-(4-fluorophenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; tert-butyldimethylsilyl 4-fluorophenyl ketone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
100%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

C17H28OSi

C17H28OSi

N-(p-methoxybenzylidene)diphenylphosphinamide
119701-95-0

N-(p-methoxybenzylidene)diphenylphosphinamide

N,N-diethyl-2-(4-tert-butylphenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-(4-tert-butylphenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; C17H28OSi With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
100%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

C15H24OSi

C15H24OSi

N-(p-methoxybenzylidene)diphenylphosphinamide
119701-95-0

N-(p-methoxybenzylidene)diphenylphosphinamide

N,N-diethyl-2-(3,4-dimethylphenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-(3,4-dimethylphenyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; C15H24OSi With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
100%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

ethyl acetoacetate
141-97-9

ethyl acetoacetate

3-diethylcarbamoyloxybut-2-enoic acid ethyl ester
1416425-91-6

3-diethylcarbamoyloxybut-2-enoic acid ethyl ester

Conditions
ConditionsYield
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry; stereoselective reaction;99%
With tert.-butylhydroperoxide; copper nanoparticles on black carbon In water; N,N-dimethyl-formamide at 80℃; for 5h; Inert atmosphere;80%
With tert.-butylhydroperoxide In water at 80℃; for 4h; Inert atmosphere; stereoselective reaction;70%
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction;68%
With tert.-butylhydroperoxide; copper(II) oxide In water at 20℃; for 4h; Sonication;
N-formyldiethylamine
617-84-5

N-formyldiethylamine

o-hydroxyacetophenone
118-93-4

o-hydroxyacetophenone

diethylcarbamic acid 2-acetylphenyl ester
211449-24-0

diethylcarbamic acid 2-acetylphenyl ester

Conditions
ConditionsYield
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry;99%
With tert.-butylhydroperoxide at 70℃; for 0.5h;95%
With tert.-butylhydroperoxide; copper diacetate In water at 80℃; for 3h;84%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

ethyl 3-oxo-3-phenylpropionate
94-02-0

ethyl 3-oxo-3-phenylpropionate

3-diethylcarbamoyloxy-3-phenylacrylic acid ethyl ester
1416425-90-5

3-diethylcarbamoyloxy-3-phenylacrylic acid ethyl ester

Conditions
ConditionsYield
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry; stereoselective reaction;99%
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction;80%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

acetoacetic acid methyl ester
105-45-3

acetoacetic acid methyl ester

3-diethylcarbamoyloxybut-2-enoic acid methyl ester
1416425-92-7

3-diethylcarbamoyloxybut-2-enoic acid methyl ester

Conditions
ConditionsYield
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.5h; Green chemistry; stereoselective reaction;99%
With tert.-butylhydroperoxide; copper nanoparticles on black carbon In water; N,N-dimethyl-formamide at 80℃; for 5h; Inert atmosphere;84%
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction;66%
With tert.-butylhydroperoxide; copper(II) oxide In water at 20℃; for 4h; Sonication;
N-formyldiethylamine
617-84-5

N-formyldiethylamine

1-Chloromethylnaphthalene
86-52-2

1-Chloromethylnaphthalene

1-<(N,N-diethylamino)methyl>naphthalene
35693-45-9

1-<(N,N-diethylamino)methyl>naphthalene

Conditions
ConditionsYield
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique;99%
With potassium hydroxide In water at 50℃; for 3h; Green chemistry;85%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

P,P-diphenyl-N-(phenylmethylene)phosphinic amide
98837-46-8, 67764-52-7

P,P-diphenyl-N-(phenylmethylene)phosphinic amide

(tert-butyldimethylsilyl)(phenyl)methanone
132868-67-8

(tert-butyldimethylsilyl)(phenyl)methanone

N,N-diethyl-2-phenyl-2-((tert-butyldimethylsilyl)oxyl)-3-phenyl-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-phenyl-2-((tert-butyldimethylsilyl)oxyl)-3-phenyl-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(phenyl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: P,P-diphenyl-N-(phenylmethylene)phosphinic amide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
99%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

toluene-4-sulfonamide
70-55-3

toluene-4-sulfonamide

(E)-N'-((4-methylphenyl)sulfonyl)-N,N-diethylformimidamide
29397-20-4

(E)-N'-((4-methylphenyl)sulfonyl)-N,N-diethylformimidamide

Conditions
ConditionsYield
With diazoacetic acid ethyl ester; zinc trifluoromethanesulfonate In cyclohexane for 12h; Reflux; stereoselective reaction;99%
With thionyl chloride In chloroform at 60℃; for 3h;96%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

4-chlorobenzo[d]thiazol-2-amine
19952-47-7

4-chlorobenzo[d]thiazol-2-amine

N,N-diethyl-N',N''-bis(4-chloro-2-benzothiazolyl)triaminomethane
112446-70-5

N,N-diethyl-N',N''-bis(4-chloro-2-benzothiazolyl)triaminomethane

Conditions
ConditionsYield
With benzenesulfonyl chloride In pyridine98%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

m-methoxybenzyl chloride
824-98-6

m-methoxybenzyl chloride

N,N-diethyl-3-(methoxyl)benzenemethanamine
27958-95-8

N,N-diethyl-3-(methoxyl)benzenemethanamine

Conditions
ConditionsYield
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique;98%
With potassium hydroxide In water at 50℃; for 3h; Green chemistry;92%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

diphenylcyclopropenone
886-38-4

diphenylcyclopropenone

5-(diethylamino)-3,4-diphenyl-2(5H)-furanone

5-(diethylamino)-3,4-diphenyl-2(5H)-furanone

Conditions
ConditionsYield
With silver trifluoromethanesulfonate at 130℃; for 2h; Inert atmosphere; Schlenk technique;98%
With silver hexafluoroantimonate In N,N-dimethyl-formamide at 80℃; for 20h; Inert atmosphere;86%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

phenylacetylene
536-74-3

phenylacetylene

1-ethyl-5-methyl-3-phenyl-1H-pyrrole-2-carbonitrile

1-ethyl-5-methyl-3-phenyl-1H-pyrrole-2-carbonitrile

Conditions
ConditionsYield
With ammonium iodide at 90℃; for 0.25h; Reagent/catalyst; Temperature; Time; Microwave irradiation;97%
With iodine In neat (no solvent) at 80℃; for 2h; Schlenk technique; Green chemistry;80%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

1-((5-phenylpent-1-en-2-yl)oxy)pyridin-1-ium bis((trifluoromethyl)sulfonyl)amide

1-((5-phenylpent-1-en-2-yl)oxy)pyridin-1-ium bis((trifluoromethyl)sulfonyl)amide

2-oxo-5-phenylpentyl formate

2-oxo-5-phenylpentyl formate

Conditions
ConditionsYield
With water In dichloromethane at 60℃; for 24h;97%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

2-(2-methylbenzyl)benzoic acid
80716-36-5

2-(2-methylbenzyl)benzoic acid

N,N-diethyl-2-(2-methylbenzyl)benzamide
80716-39-8

N,N-diethyl-2-(2-methylbenzyl)benzamide

Conditions
ConditionsYield
With thionyl chloride for 20h;96%
cobalt(II) trifluoromethanesulfonate

cobalt(II) trifluoromethanesulfonate

4,4'-benzene-1,4-diylbis(1H-pyrazole)
1036248-62-0

4,4'-benzene-1,4-diylbis(1H-pyrazole)

N-formyldiethylamine
617-84-5

N-formyldiethylamine

Co(1,4-benzenedi(4'-pyrazolyl)(2-))*2(N,N-diethylformamide)*H2O

Co(1,4-benzenedi(4'-pyrazolyl)(2-))*2(N,N-diethylformamide)*H2O

Conditions
ConditionsYield
In further solvent(s) mixt. Co(OTf)2, 1,4-benzenedipyridyl and HCONEt2 in sealed evacuated tube was heated at 150°C for 6 days; ppt. was filtered, washed with HCONEt2 and dried in vacuo for 30 min; elem. anal.;95%
In further solvent(s) react. in N,N-diethylformamide at 130°C;
N-formyldiethylamine
617-84-5

N-formyldiethylamine

indium(III) nitrate hydrate

indium(III) nitrate hydrate

benzene-1,3,5-tricarboxylic acid
554-95-0

benzene-1,3,5-tricarboxylic acid

tetraethylammonium bromide
71-91-0

tetraethylammonium bromide

(tetraethylammonium)3[In3(1,3,5-benzenetricarboxylate)4]*N,N-diethylformamide

(tetraethylammonium)3[In3(1,3,5-benzenetricarboxylate)4]*N,N-diethylformamide

Conditions
ConditionsYield
In further solvent(s) C6H3(COOH)3, (C2H5)4NBr, In(NO3)3*xH2O in N,N-diethylformamide was heated at 120°C for 4 days, cooled to room temp.; washed with ethanol; elem. anal.;95%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

Dimethylphenylsilane
766-77-8

Dimethylphenylsilane

phenyldimethylsilyloxymethyldiethylamine
1366432-35-0

phenyldimethylsilyloxymethyldiethylamine

Conditions
ConditionsYield
With CpMn(CO)3 for 16h; Irradiation;95%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

(tert-butyldimethylsilyl)(naphthalen-2-yl)methanone

(tert-butyldimethylsilyl)(naphthalen-2-yl)methanone

N-(p-methoxybenzylidene)diphenylphosphinamide
119701-95-0

N-(p-methoxybenzylidene)diphenylphosphinamide

N,N-diethyl-2-(2-naphthyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

N,N-diethyl-2-(2-naphthyl)-2-((tert-butyldimethylsilyl)oxyl)-3-(4-methoxyphenyl)-3-((N’-diphenylphosphinyl)amido)propionamide

Conditions
ConditionsYield
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(naphthalen-2-yl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique;
Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction;
95%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

cyclohexanone
108-94-1

cyclohexanone

N,N-diethyl-1-hydroxycyclohexanecarboxamide

N,N-diethyl-1-hydroxycyclohexanecarboxamide

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran at 25℃; for 0.0166667h;95%
1,3-Benzothiazole
95-16-9

1,3-Benzothiazole

N-formyldiethylamine
617-84-5

N-formyldiethylamine

N,N-diethylbenzo[d]thiazol-2-amine
24255-48-9

N,N-diethylbenzo[d]thiazol-2-amine

Conditions
ConditionsYield
With silver(I) acetate; sodium t-butanolate In neat (no solvent) at 120℃; for 5h; Inert atmosphere;95%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

N,N-diethyl-3-phenylpropanamide
18859-19-3

N,N-diethyl-3-phenylpropanamide

Conditions
ConditionsYield
With sulfur trioxide pyridine complex at 160℃; Schlenk technique; Inert atmosphere;95%
N-formyldiethylamine
617-84-5

N-formyldiethylamine

N-(1-phenyl)sulfamide
15959-53-2

N-(1-phenyl)sulfamide

(E)-N,N-diethyl-N'-(N-phenylsulfamoyl)formimidamide

(E)-N,N-diethyl-N'-(N-phenylsulfamoyl)formimidamide

Conditions
ConditionsYield
With trichlorophosphate In dichloromethane at 40℃; for 9h;95%
4,4'-bis-(1H-imidazol-1-yl)biphenyl
855766-92-6

4,4'-bis-(1H-imidazol-1-yl)biphenyl

N-formyldiethylamine
617-84-5

N-formyldiethylamine

cobalt(II) nitrate hexahydrate

cobalt(II) nitrate hexahydrate

2′,3′,5′,6′-tetramethyl(1,1′:4′,1″-terphenyl)-4,4″-dicarboxylic acid
1394899-62-7

2′,3′,5′,6′-tetramethyl(1,1′:4′,1″-terphenyl)-4,4″-dicarboxylic acid

2Co(2+)*2C24H20O4(2-)*2C5H11NO*C18H14N4

2Co(2+)*2C24H20O4(2-)*2C5H11NO*C18H14N4

Conditions
ConditionsYield
at 120℃; for 24h; Sealed tube;95%

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