DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:623-03-0
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 4-Chlorobenzonitrile CAS number 623-03-0 Assay ≥99% Appearance White crystal Capacity 200mt/year Application Dye/pharmaceutical intermediate
Cas:623-03-0
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inquiryUnique advantages for 4-Chlorobenzonitrile Cas 623-03-0 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Powder Storage:Store below +30°C Package:25kg/drum Application:Interme
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inquiryTechnology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure that our technology
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 4-Chlorobenzonitrile CAS 623-03-0 PCBN IN Stock p-Chlorobenzonitrile 623-03-0 623-03-0 CAS 623-03-0 highly quality and immedaite
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct: 4-Chlorobenzonitrile Synonym: PCBN CAS no: 623-03-0 Molecular formula: C7H4ClN Molecular Weight: 137.56 Melting point: 91-94°C Appearance: white needle crystals Package: 25kg, or 50kg/drum Spec: ≥99.0% Usage: Int
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inquiryAppearance:White crystals Storage:ln stock Package:25kg/Barrel Application:Used as dyes and pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in China
Cas:623-03-0
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiry4-Chlorobenzonitrile CAS:623-03-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:623-03-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiryCHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
Cas:623-03-0
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inquiryProduct name: 4-Chlorobenzonitrile CAS No.:623-03-0 Molecule Formula:C7H4ClN Molecule Weight:137.57 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:623-03-0
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:623-03-0
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide at 20℃; for 4h; Beckmann rearrangement; | 100% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; 4 A molecular sieve In acetonitrile at 80℃; for 0.166667h; | 89% |
With carbon disulfide; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In benzene for 0.5h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 130℃; under 3750.38 Torr; for 24h; | 100% |
Stage #1: para-Chlorobenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
With ammonia; oxygen In tert-Amyl alcohol; water at 100℃; under 3750.38 Torr; for 5h; Autoclave; High pressure; | 99% |
Conditions | Yield |
---|---|
With ammonia; iodine In tetrahydrofuran; water at 20℃; for 0.666667h; | 99% |
With Nitroethane; pyridine hydrochloride for 1h; Heating; | 98% |
With hydroxylamine hydrochloride; pyrographite; methanesulfonyl chloride at 100℃; for 2h; | 98% |
Conditions | Yield |
---|---|
With N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; copper(l) chloride In toluene at 100℃; for 24h; | 99% |
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide for 2h; Product distribution; Ambient temperature; also in (C2H5O)3PO, other temperature, other time; | 96% |
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide for 2h; Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; for 3h; | 99% |
With pyrographite; methanesulfonyl chloride at 100℃; for 0.166667h; | 98% |
With thionyl chloride; sodium sulfite at 0℃; for 0.0833333h; | 98% |
Conditions | Yield |
---|---|
With oxygen In acetone at 20℃; for 3.2h; Electrochemical reaction; | 99% |
With potassium hydroxide; nickel copper formate; (Bu4N)2S2O8 In 1,2-dichloro-ethane at 20℃; for 13h; Oxidation; | 95% |
With [hydroxy(tosyloxy)iodo]benzene; ammonium acetate In water; acetonitrile at 80℃; for 3h; | 92% |
4-chlorobenzoyl cyanide
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 12h; | 98% |
4-chlorobenzaldehyde N,N-dimethylhydrazone
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In acetone at 0℃; for 0.05h; | 98% |
With magnesium monoperoxyphthalate hexahydrate In methanol at 0℃; for 0.0833333h; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 98% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Catalytic behavior; | 96% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; | 96% |
2-(4-chlorophenyl)-1,3,4-oxadiazole
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With sodium t-butanolate In N,N-dimethyl-formamide at 20℃; for 4h; | 98% |
1-Chloro-4-iodobenzene
tert-butylisonitrile
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With copper (II) trifluoroacetate hydrate; palladium diacetate In dimethyl sulfoxide at 130℃; for 6h; Sealed tube; Inert atmosphere; | 98% |
4-cyanophenylboronic acid
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With N-chloro-succinimide In acetonitrile at 80℃; for 12h; | 98% |
4-chloro-benzaldehyde-(O-benzoyl oxime )
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With iron(II) sulfate In 1,2-dichloro-ethane; 1,3,5-trimethyl-benzene at 20℃; for 0.25h; | 98% |
With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In toluene at 20℃; for 0.0833333h; Schlenk technique; | 85% |
Conditions | Yield |
---|---|
With polystyrene-bound diaryl telluroxide In dichloromethane for 1h; Ambient temperature; | 97% |
With tellurium tetrachloride; triethylamine In chloroform for 3h; Ambient temperature; | 96% |
With p-methoxybenzenetellurinic acid anhydride In dichloromethane for 0.5h; Ambient temperature; | 91% |
(acetyloxy)(4-chlorophenyl)methyl acetate
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With trimethylsilylazide; titanium tetrachloride In dichloromethane for 2h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine In toluene at 110℃; for 1h; Schlenk technique; Inert atmosphere; | 96% |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 120℃; for 24h; Glovebox; Inert atmosphere; Sealed tube; | 53% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; Ambient temperature; | 95% |
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 25℃; for 1h; | 95% |
With triethylamine at 20℃; for 0.333333h; Milling; | 0.161 g |
Conditions | Yield |
---|---|
With calcium dihydride; tri-tert-butyl phosphine; [Pd2(dba)5] In tetrahydrofuran; acetonitrile at 70℃; for 2h; | 95% |
3-{[(4-chlorophenyl)methylene]amino}-2-phenylquinazolin-4(3H)-one
A
4-Cyanochlorobenzene
B
2-phenyl-4(3H)-quinazolinone
Conditions | Yield |
---|---|
at 200 - 240℃; under 1 Torr; | A 94% B n/a |
Conditions | Yield |
---|---|
With 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium tert-butylate; triethylamine; bis(dibenzylideneacetone)-palladium(0) In dichloromethane; water; acetonitrile at 50℃; for 24h; Inert atmosphere; | 94% |
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; tetrabutylammomium bromide; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.0833333h; Microwave irradiation; chemoselective reaction; | 93% |
With tris-(dibenzylideneacetone)dipalladium(0); tris(2-morpholinophenyl)phosphine; potassium carbonate In water; tert-butyl alcohol at 85℃; for 10h; Schlenk technique; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With [Pd{C6H3(CH2CH2NH2)-4-OMe-5-κ2-C,N}(μ-Br)]2; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.0666667h; Microwave irradiation; chemoselective reaction; | 94% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Catalytic behavior; | 92% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; | 92% |
Conditions | Yield |
---|---|
With copper diacetate; Triphenylphosphine oxide; silver(l) oxide at 125℃; for 72h; | 94% |
Conditions | Yield |
---|---|
With Aloe vera mediated silver nanoparticles In water at 50℃; for 0.5h; Green chemistry; | 94% |
4-Chlorophenylboronic acid
A
4-Cyanochlorobenzene
B
4-nitro-N-(4-chlorophenyl)benzenesulfonamide
Conditions | Yield |
---|---|
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 10h; Catalytic behavior; Reflux; | A 94% B n/a |
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene In various solvent(s) at 60℃; for 2h; | 93% |
(4-chlorphenyl)magnesium bromide
pyridin-2-yl cyanate
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 0.166667h; | 93% |
5-(tert-butyl)-3-((p-chloro)phenyl)-5H-1,2,4-oxathiazole
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With benzylamine In chloroform at 20℃; for 12h; | 93% |
Conditions | Yield |
---|---|
With sodium carbonate; potassium ferrocyanide In N,N-dimethyl-formamide at 120℃; for 5h; | 93% |
4-Cyanochlorobenzene
5-(4-chlorophenyl)-1H-tetrazole
Conditions | Yield |
---|---|
With sodium azide; copper(II) sulfate In dimethyl sulfoxide at 140℃; for 0.5h; | 100% |
With sodium azide In dimethyl sulfoxide at 140℃; for 0.833333h; | 100% |
With sodium azide In dimethyl sulfoxide at 120℃; for 0.166667h; Green chemistry; | 100% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium In methanol | 100% |
With hydroxylamine In ethanol; water for 8h; Reflux; | 100% |
With potassium fluoride; hydroxylamine hydrochloride at 100℃; for 1h; | 98% |
Conditions | Yield |
---|---|
With C18H57O3P6Ru2(1+)*C6H5O(1-)*C6H6O; water In 1,4-dioxane for 6h; Time; Sealed tube; Inert atmosphere; Schlenk technique; | 100% |
With water; tricyclohexylphosphine; {Rh(OMe)(cod)}2 In isopropyl alcohol at 25℃; for 24h; | 99% |
With manganese(IV) oxide In dichloromethane at 40℃; under 760.051 Torr; for 2h; Molecular sieve; | 99% |
Conditions | Yield |
---|---|
With potassium tert-butylate; N,N-dimethyl-formamide at 35℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation; | 100% |
With C60H48BP3Pd; potassium formate; [2.2.2]cryptande In tetrahydrofuran at 60℃; for 72h; Schlenk technique; Inert atmosphere; | 99% |
With formic acid; Cyclohexanethiol; 10-phenyl-10H-phenothiazine; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; under 2625.26 Torr; for 0.05h; Catalytic behavior; Reagent/catalyst; Time; Wavelength; Irradiation; Flow reactor; | 96% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel(0); lithium tert-butoxide In toluene at 110℃; for 16h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 100% |
With C45H39BrNiOP2; lithium tert-butoxide; phenylboronic acid In toluene at 110℃; for 16h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube; | 99% |
With C34H45ClNiO6P2; lithium tert-butoxide at 65℃; | 91% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); Py2NPtBu2; sodium t-butanolate In tetrahydrofuran at 60℃; for 24h; Suzuki coupling; | 100% |
With caesium carbonate; polymer-supp. 11-(2-[Pd(OAc)2]-1-Mes-imidazol-3-yl)undecanol In 1,4-dioxane at 80℃; for 0.5h; Suzuki-Miyaura coupling; | 100% |
With C38H53Cl2N2O2PPd*CH2Cl2; tetrabutylammomium bromide; potassium hydroxide In water at 80℃; for 6h; Suzuki-Miyaura Coupling; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
With 2-(dicyclohexylphosphino)-4'-(N,N-dimethylamino)-1,1'-biphenyl at 20℃; | 100% |
With potassium hydroxide; XPhos; palladium diacetate In water; toluene at 100℃; for 0.5h; Buchwald-Hartwig amination; microwave irradiation; | 99% |
With tris(dibenzylideneacetone)dipalladium (0); (-)-2-(dicyclohexylphosphino)-2'-(dimethylamino)-1,1'-binaphthyl; sodium t-butanolate In 1,2-dimethoxyethane Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate In 1-methyl-pyrrolidin-2-one at 100℃; for 12h; | 100% |
styrene
4-Cyanochlorobenzene
A
(E)-1-cyano-4-styryl-benzene
B
1-(4-cyanophenyl)-1-phenylethylene
Conditions | Yield |
---|---|
With C28H24FN2O3PPd; tetrabutylammomium bromide; sodium acetate at 140℃; for 12h; Catalytic behavior; Inert atmosphere; Schlenk technique; regioselective reaction; | A 100% B n/a |
With C27H21F3N6OPd; tetrabutylammomium bromide; sodium acetate at 140℃; for 2h; Heck reaction; Inert atmosphere; |
4-Cyanochlorobenzene
2,6-dimethylbenzene boronic acid
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate In tetrahydrofuran for 24h; Suzuki coupling; Inert atmosphere; Reflux; | 100% |
With C51H40ClN3O5P2Pd; sodium hydroxide In water at 80℃; for 9h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Suzuki-Miyaura Coupling; | 90% |
4-Cyanochlorobenzene
(S)-valinol
(-)-(4S)-2-(4'-chlorophenyl)-4,5-dihydro-4-isopropyloxazole
Conditions | Yield |
---|---|
In neat (no solvent) at 240℃; for 1.66667h; Temperature; Microwave irradiation; | 100% |
Conditions | Yield |
---|---|
With C28H24FN2O3PPd; tetrabutylammomium bromide; sodium acetate at 140℃; for 12h; Catalytic behavior; Inert atmosphere; Schlenk technique; regioselective reaction; | 100% |
4-Cyanochlorobenzene
tetrapentylammonium bromide
acrylic acid methyl ester
Conditions | Yield |
---|---|
With C32H27N4O2Pd(1+)*BF4(1-); sodium acetate at 140℃; for 12h; Inert atmosphere; Schlenk technique; Green chemistry; | 100% |
Conditions | Yield |
---|---|
With ammonia; lanthanum(lll) triflate at 200℃; for 24h; in a stainless steel pressure vessel; | 99% |
With zinc(II) chloride at 300℃; for 60h; | 71% |
With chlorosulphuric acid |
Conditions | Yield |
---|---|
With [Ru(H)(BH4)(CO)(PPh3)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2 yl)methyl)propylamine)]; hydrogen In isopropyl alcohol at 70℃; for 3h; Inert atmosphere; Autoclave; | 99% |
With ammonia; hydrogen In water; isopropyl alcohol at 80℃; under 15001.5 Torr; for 24h; Autoclave; | 98% |
With C19H34Cl2CoN2P; hydrogen; sodium ethanolate; sodium triethylborohydride In benzene at 135℃; under 22502.3 Torr; for 36h; Autoclave; | 93% |
4-Cyanochlorobenzene
(4-chlorophenyl)methanamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 4-Cyanochlorobenzene With [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]triethylphosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; diethylphenylsilane at 20℃; for 18h; Glovebox; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether at 20℃; for 1h; Glovebox; Inert atmosphere; | 99% |
Stage #1: 4-Cyanochlorobenzene With fac-[Mn(1,2-bis(di-n-propylphosphino)ethane)(CO)3(CH3)]; hydrogen In toluene at 100℃; under 37503.8 Torr; for 18h; Autoclave; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 96% |
Stage #1: 4-Cyanochlorobenzene With 1,1,3,3-Tetramethyldisiloxane; 1,2,3-trimethoxy glycerol ether; copper(II) bis(trifluoromethanesulfonate) at 100℃; for 24h; Inert atmosphere; Sealed tube; Green chemistry; Stage #2: With hydrogenchloride In diethyl ether at 20℃; for 0.0833333h; Green chemistry; | 94% |
4-Cyanochlorobenzene
4-chloroselenobenzamide
Conditions | Yield |
---|---|
With selenium; carbon monoxide; water; triethylamine In tetrahydrofuran at 100℃; under 3800 Torr; for 5h; | 99% |
Stage #1: 4-Cyanochlorobenzene With woollins’ reagent In toluene for 4h; Heating; Stage #2: With water In toluene for 1h; | 95% |
With pyridine; hydrogenchloride; sodium hydrogen selenide In ethanol for 3.5h; Heating; | 93% |
Conditions | Yield |
---|---|
With tetrakis[μ-1-[(3-methoxyphenyl)methyl]-2-phenyl-3-[2-oxo-2-[(2-phenolato-kO)aminokN]ethyl]-1H-imidazoliumato-kC4]tetrapalladium; tetrabutylammomium bromide; sodium acetate at 140℃; for 2h; Heck Reaction; | 99% |
With tetrabutylammomium bromide; sodium acetate; C84H60N12O8Pd4 at 140℃; for 2h; Heck Reaction; Inert atmosphere; Schlenk technique; | 99% |
With tetrabutylammonium acetate; palladium diacetate; DavePhos In 1,4-dioxane at 80℃; for 24h; Heck reaction; Inert atmosphere; Sealed tube; | 98% |
4-Cyanochlorobenzene
4-methylphenylboronic acid
p-(p-tolyl)benzonitrile
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; potassium carbonate In water at 100℃; for 22h; Suzuki-Miyaura coupling; | 99% |
With tetrabutylammomium bromide; nickel; sodium carbonate; triphenylphosphine In ethanol at 80℃; for 6h; Suzuki-Miyaura reaction; | 95% |
With potassium carbonate In water at 80 - 90℃; for 12h; Suzuki-Miyaura cross-coupling; | 95% |
styrene
4-Cyanochlorobenzene
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium acetate; C27H21FN4O2Pd at 140℃; for 2h; Heck Reaction; Schlenk technique; Inert atmosphere; | 99% |
With potassium tert-butylate In water at 100℃; for 16h; Catalytic behavior; Reagent/catalyst; Solvent; Heck Reaction; Green chemistry; | 95% |
With [Pd(O(C(O)CH)2)(CN(CH2C(O)NHC6H5)CHCHNCH2C6H5)2]; sodium acetate at 140℃; for 2h; Heck coupling; Ionic liquid; Inert atmosphere; regioselective reaction; | 90% |
4-Cyanochlorobenzene
2-Methylphenylboronic acid
4-cyano-2'-methyl-1,1'-biphenyl
Conditions | Yield |
---|---|
With caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 100℃; for 2.8h; Suzuki-Miyaura reaction; | 99% |
With C84H64Cl3N3Pd; potassium carbonate In ethanol at 80℃; for 2h; Suzuki-Miyaura Coupling; | 98% |
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In ethanol; water at 80℃; for 4h; Suzuki-Miyaura Coupling; Sealed tube; Green chemistry; | 97% |
4-Cyanochlorobenzene
(S)-4-Benzyl-2-oxazolidinone
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); caesium carbonate; johnphos In toluene at 115℃; for 15h; | 99% |
With potassium phosphate; [(π-allyl)Pd(tBuBrettPhos)]OTf In tert-butyl alcohol at 110℃; for 3h; Schlenk technique; Inert atmosphere; Sealed tube; | 95% |
With (PAd2-DalPhos)NiCl(o-tol); caesium carbonate In 1,4-dioxane at 90℃; for 18h; Inert atmosphere; Glovebox; Sealed tube; | 64% |
4-Cyanochlorobenzene
(p-hydroxyphenyl)boronic acid
4-Cyano-4'-hydroxybiphenyl
Conditions | Yield |
---|---|
With potassium phosphate; catacxium A; palladium diacetate In toluene at 100℃; for 20h; Suzuki cross-coupling reaction; | 99% |
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