2-Bromo-4'-methoxyacetophenone
Cas:2632-13-5
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:2632-13-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:2632-13-5
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:2632-13-5
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:2632-13-5
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:2632-13-5
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Trading Company
inquiryCAS No.2632-13-5 /2-Bromo-4'-methoxyacetophenone Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships wit
Cas:2632-13-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:2632-13-5
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:2632-13-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry2-Bromo-4'-methoxyacetophenone CAS:2632-13-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
Cas:2632-13-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:2632-13-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:2632-13-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:2632-13-5
Min.Order:1 Kilogram
FOB Price: $40.0 / 50.0
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:2632-13-5
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:2632-13-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:2632-13-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:2632-13-5
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:2632-13-5
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:2632-13-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:2632-13-5
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryProduct Name: 2-Bromo-4'-methoxyacetophenone Synonyms: ALPHA-BROMO-4'-METHOXYACETOPHENONE;ALPHA-BROMO-4-METHOXYACETOPHENONE;AKOS BBS-00000817;Bromomethyl 4-methoxyphenyl ketone;4-(BROMOACETYL)ANISOLE;4-methoxy phenecyl bromide;4-METHOXY
Cas:2632-13-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:2632-13-5
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:2632-13-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:2632-13-5
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:2632-13-5
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:2632-13-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is
Cas:2632-13-5
Min.Order:100 Kilogram
FOB Price: $100.0 / 150.0
Type:Other
inquiryConditions | Yield |
---|---|
With bromine In 1,4-dioxane; diethyl ether for 0.5h; Ambient temperature; | 100% |
With N-Bromosuccinimide; toluene-4-sulfonic acid In chloroform at 20℃; for 12h; | 98.7% |
With bis(dimethylacetamide)hydrogen tribromide In methanol at 20 - 45℃; for 0.25h; | 96% |
1-bromo-2-(4-methoxyphenyl)acetylene
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With tetrafluoroboric acid; water In 2,2,2-trifluoroethanol at 80℃; for 2h; | 93% |
With indium(III) triflate; water In acetic acid at 100℃; Sealed tube; | 92% |
With cerium(IV) sulphate; sulfuric acid; water In dichloromethane at 80℃; for 12h; Sealed tube; regioselective reaction; | 90% |
Conditions | Yield |
---|---|
With N,N'-ethylenethiourea; 1,3-dibromo-5,5-dimethylhydantoin; water In acetone at 45℃; | 87% |
Stage #1: 4-methoxyphenylacetylen With methanol; gold(III) chloride; silver(I) triflimide In 1,4-dioxane at 45℃; Stage #2: With N-Bromosuccinimide In 1,4-dioxane regioselective reaction; | 75% |
Multi-step reaction with 2 steps 1: diethyl ether / Umsetzen der entstandenen Magnesiumverbindung mit Bromcyan 2: sulfuric acid View Scheme | |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide; silver nitrate / acetone / 20 °C 2: water; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide / 1,2-dichloro-ethane / 14 h / 20 °C View Scheme |
2,2-dibromo-1-(4-methoxyphenyl)ethanone
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium dichloride; 1,5-dimethoxynaphthalene; ascorbic acid In methanol; water for 2h; Inert atmosphere; Irradiation; | 70% |
Conditions | Yield |
---|---|
With ferric(III) bromide; oxygen; toluene-4-sulfonic acid; potassium bromide In tert-butyl methyl ether at 20℃; Irradiation; Green chemistry; | 65% |
With dipotassium peroxodisulfate; potassium bromide In water at 60℃; for 12h; Green chemistry; | 24% |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide / acetonitrile; water / 4 h / 25 - 30 °C 2: 2-iodo-3,4,5,6-tetramethylbenzoic acid; oxone / acetonitrile; water / 10 h / 25 - 30 °C View Scheme | |
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water In acetone at 70℃; for 0.138833h; |
1-(4-methoxyphenyl)ethanone
A
2,2-dibromo-1-(4-methoxyphenyl)ethanone
B
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With N-Bromosuccinimide; silica gel In methanol for 0.216667h; Reflux; chemoselective reaction; | A n/a B 64% |
With 1-methyl-3-(4-sulfonylbutyl)-1H-imidazol-3-ium trifluoromethanesulfonate; N-Bromosuccinimide at 55℃; for 0.333333h; Green chemistry; | A 20% B 62% |
With potassium permanganate; hydrogen bromide In acetonitrile at 60℃; | A 6% B 56% |
4-methoxy-α-bromoacetophenone oxime
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With oxygen; sodium nitrite In dichloromethane; water at 25℃; under 760.051 Torr; for 6h; Sealed system; | 52% |
2-(4-methoxyphenyl)-2-methyI-1,3-dioxolane
A
2-bromomethyl-2-(4-methoxyphenyl)-1,3-dioxolane
B
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With phenyltrimethylammonium tribromide In tetrahydrofuran at 25℃; for 2.15h; | A 50% B 50 % Chromat. |
1-bromo-2-(4-methoxyphenyl)acetylene
acetic acid
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
methanol
A
2,2-dibromo-1-(4-methoxyphenyl)ethanone
B
methyl 4-methoxybenzoate
C
4-methoxyphenylglyoxylate methyl ester
D
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With oxygen at 10℃; for 2h; Irradiation; | A 5.8 % Chromat. B 4.4 % Chromat. C 61.9 % Chromat. D 1 % Chromat. |
2-(4-methoxyphenyl)-2-methyI-1,3-dioxolane
A
2,2-dibromo-1-(4-methoxyphenyl)ethanone
B
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With tribromure de triphenylmethylphosphonium In dichloromethane at 25℃; for 3h; | A 15 % Chromat. B 70 % Chromat. |
3-Bromomethyl-3-(4-methoxy-phenyl)-4,4-dimethyl-[1,2]dioxetane
A
acetone
B
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In xylene at 60℃; Thermodynamic data; Rate constant; Ea; other solvents and temp., var. 1,2-dioxetanes; |
4-methoxy-α-bromoacetophenone methyl hemiacetal
A
methanol
B
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With hydrogen cation In water at 25℃; Rate constant; | |
With hydroxide In water at 25℃; Rate constant; | |
With water at 25℃; Rate constant; | |
With acetate In water at 25℃; Rate constant; |
Conditions | Yield |
---|---|
With n-butyllithium; lithium diisopropyl amide Yield given. Multistep reaction; |
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With sulfuric acid Ambient temperature; Yield given; |
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With diethyl ether; hydrogen bromide |
1-((4-methoxy)phenyl)-1,2-dibromoethane
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 1-((4-methoxy)phenyl)-1,2-dibromoethane With water at 100℃; for 3h; Stage #2: With dihydrogen peroxide In 1,4-dioxane; water at 25℃; for 3h; | 41 %Chromat. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tris(2,2'-bipyridyl)ruthenium dichloride; 1,5-dimethoxynaphthalene; ascorbic acid / methanol; water / 15 h / Inert atmosphere; Irradiation 2: bromine / chloroform / 0 - 65 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetone / 0.25 h / Reflux 1.2: 3 h / Reflux 2.1: bromine; acetic acid / 50 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 2 h / Reflux 2: hydrogenchloride; bromine / methanol / 3 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetone / 0.25 h / Reflux 1.2: 3 h / Reflux 2.1: bromine; acetic acid / 50 °C View Scheme |
Conditions | Yield |
---|---|
With copper(ll) bromide In ethanol for 2h; Reflux; |
2-bromo-1-(4-methoxyphenyl)ethanol
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With oxone; 2-iodo-3,4,5,6-tetramethylbenzoic acid In water; acetonitrile at 25 - 30℃; for 10h; | 139 mg |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper(l) iodide; potassium carbonate / N,N-dimethyl-formamide / Reflux 2: copper(ll) bromide / ethyl acetate; chloroform / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 °C / Inert atmosphere 2.1: 1 h / 0 °C 2.2: 0.33 h / 0 °C View Scheme |
diazomethane
4-methoxy-benzoyl chloride
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: diazomethane; 4-methoxy-benzoyl chloride at 0℃; for 1h; Stage #2: With hydrogen bromide at 0℃; for 0.333333h; |
N-Bromosuccinimide
1-(4-methoxyphenyl)ethanone
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 60 - 80℃; |
thioacetamide
2-Bromo-4'-methoxyacetophenone
methyl 4-(2-methyl-1,3-thiazol-4-yl)phenyl ether
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; | 100% |
In ethylene glycol at 20℃; for 0.0833333h; | 97% |
With 1,3-di-n-butyl-imidazolium tetrafluoroborate at 20℃; for 0.25h; | 96% |
tris<(trimethylsiloxy)methyl>phosphine
2-Bromo-4'-methoxyacetophenone
[2-(4-Methoxy-phenyl)-2-oxo-ethyl]-tris-trimethylsilanyloxymethyl-phosphonium; bromide
Conditions | Yield |
---|---|
at 20℃; for 5h; | 100% |
Conditions | Yield |
---|---|
With AcrH2 In acetonitrile at 298℃; for 19h; Irradiation; | 100% |
With AcrH2 In acetonitrile at 298℃; for 19h; Irradiation; | 100% |
With decaborane; palladium on activated charcoal In methanol at 20℃; for 2h; | 99% |
sodium 4-methylbenzenesulfinate
2-Bromo-4'-methoxyacetophenone
1-(4-methoxyphenyl)-2-tosylethanone
Conditions | Yield |
---|---|
In 1,4-dioxane; water Reflux; | 100% |
In ethanol for 1.5h; Heating; | 90% |
In ethanol Heating; |
thiourea
2-Bromo-4'-methoxyacetophenone
4-(4-methoxyphenyl)-1,3-thiazol-2-amine
Conditions | Yield |
---|---|
In ethanol at 45℃; for 0.333333h; Sonication; | 100% |
In ethanol for 2h; Reflux; | 100% |
In ethanol for 1h; Reflux; | 99% |
2-Bromo-4'-methoxyacetophenone
dimethyl 3,4-bis(4-(benzyloxy)phenyl)-1H-pyrrole-2,5-dicarboxylate
dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 1h; | 100% |
2-Bromo-4'-methoxyacetophenone
1-(4-Methoxy-phenyl)-2-nitrooxy-ethanone
Conditions | Yield |
---|---|
With silver nitrate In acetonitrile at 20℃; for 10h; | 100% |
With silver nitrate In acetonitrile at 20℃; for 48h; |
2-Iodophenol
2-Bromo-4'-methoxyacetophenone
2-(2-iodophenoxy)-1-(4-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 80℃; for 4h; | 100% |
With potassium carbonate In acetone Reflux; | 90% |
With potassium carbonate | 80% |
6,7-dimethoxy-1-(2',2'-diphenyl-1'-ethenyl)-3,4-dihydroisoquinoline
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In diethyl ether | 100% |
Conditions | Yield |
---|---|
In acetonitrile Heating; | 100% |
In acetonitrile Heating; |
Conditions | Yield |
---|---|
With dimethyl sulfoxide In water at 50℃; for 2.5h; | 100% |
Multi-step reaction with 2 steps 1: AgNO3 / acetonitrile / 48 h / 20 °C 2: 1.69 g / NaOAc / dimethylsulfoxide / 16 h / 20 °C View Scheme | |
In dimethyl sulfoxide |
Conditions | Yield |
---|---|
In acetone at 20℃; | 100% |
Conditions | Yield |
---|---|
With sodium carbonate decahydrate In ethanol Reflux; | 100% |
phenylglyoxylic acid potassium salt
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; | 100% |
potassium 2-(4-methoxyphenyl)-2-oxoacetate
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; | 100% |
2-Bromo-4'-methoxyacetophenone
4-methyl-N-{2-(phenylethynyl)phenyl}benzenesulfonamide
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-{2-(phenylethynyl)phenyl}benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
Stage #1: 4-methyl-N-{2-(phenylethynyl)phenyl}benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 90% |
4-methyl-N-(4-methyl-2-(phenylethynyl)phenyl)benzenesulfonamide
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-(4-methyl-2-phenylethynyl-phenyl)-benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
4-methyl-N-(4-fluoro-2-phenylethynyl-phenyl)-benzenesulfonamide
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-(4-fluoro-2-phenylethynyl-phenyl)-benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
4-methyl-N-(4-chloro-2-phenylethynyl-phenyl)-benzenesulfonamide
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-(4-chloro-2-phenylethynyl-phenyl)-benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
4-methyl-N-(2-(p-tolylethynyl)phenyl)benzenesulfonamide
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 4-methyl-N-(2-(p-tolylethynyl)phenyl)benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 4-bromo-N-(2-(phenylethynyl)phenyl)benzenesulfonamide With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 2-Bromo-4'-methoxyacetophenone In N,N-dimethyl-formamide at 20℃; | 100% |
p-cresol
2-Bromo-4'-methoxyacetophenone
1-(4-methoxyphenyl)-2-(p-tolyloxy)ethan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 4h; Reflux; | 100% |
With potassium carbonate In acetone at 20℃; for 16h; Inert atmosphere; Schlenk technique; |
α-picoline
2-Bromo-4'-methoxyacetophenone
2-(4-methoxyphenyl)-indolizine
Conditions | Yield |
---|---|
Stage #1: α-picoline; 2-Bromo-4'-methoxyacetophenone In acetone for 1h; Heating; Stage #2: With potassium carbonate for 5h; | 99% |
2-aminopyridine
2-Bromo-4'-methoxyacetophenone
2-(4-methoxyphenyl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In neat (no solvent) at 25 - 30℃; Milling; Green chemistry; | 99% |
at 20℃; for 0.166667h; grinding; neat (no solvent); | 95% |
In water; isopropyl alcohol at 75℃; Microwave irradiation; Green chemistry; | 95% |
2-Amino-4-methylpyridine
2-Bromo-4'-methoxyacetophenone
2-(4-methoxyphenyl)-7-methyl-imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
In neat (no solvent) at 25 - 30℃; Milling; Green chemistry; | 99% |
In water; isopropyl alcohol at 75℃; Microwave irradiation; Green chemistry; | 96% |
In neat (no solvent) at 65℃; under 750.075 Torr; for 0.3h; Microwave irradiation; Green chemistry; | 83% |
benzylamine
2-Bromo-4'-methoxyacetophenone
2-(benzylamino)-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether at -78 - 20℃; for 3h; Inert atmosphere; | 99% |
4-amino-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In ethanol at 95℃; for 0.5h; Microwave irradiation; | 99% |
Stage #1: 4-amino-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol; 2-Bromo-4'-methoxyacetophenone In ethanol for 2h; Reflux; Stage #2: With ammonium hydroxide In ethanol at 20℃; | 78% |
In ethanol for 24h; Heating; | 62% |
potassium cyanamide salt
2-Bromo-4'-methoxyacetophenone
(4-Amino-2-ethoxy-thiazol-5-yl)-(4-methoxy-phenyl)-methanone
Conditions | Yield |
---|---|
With triethylamine In acetone for 2h; Ambient temperature; | 99% |
4-amino-5-(4-bromophenyl)-3-mercapto-1,2,4-triazole
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
In ethanol at 95℃; for 0.5h; Microwave irradiation; | 99% |
In ethanol for 24h; Heating; | 82% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View