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inquiryProduct name: Dimethylthiocarbamoyl Chloride CAS No.:16420-13-6 Molecule Formula:C3H6ClNS Molecule Weight:123.60 Purity: 98.0% Package: 25kg/drum Description:Light yellow crystalline powder Manufacture Standards:Enterprise Standard
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inquiryDimethylthiocarbamoyl chloride Basic information Product Name: Dimethylthiocarbamoyl chloride Synonyms: N,N-Dimethylcarbamothioic chloride, tech;DiMethylthiocarbaMoyl Chloride (DMTCC);DiMethylthiocarbaMoyl chloride, 99% 100GR;N,N-Dimethylamino
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Thiram
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride In dichloromethane for 0.25h; Ambient temperature; | 97% |
With sulfuryl dichloride In tetrachloromethane 1) room temp., 10 min; 2) reflux, 20 min; | 94% |
With thionyl chloride In tetrachloromethane at 20℃; for 0.5h; | 92% |
Thiram
A
N,N-Dimethylthiocarbamoyl chloride
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride In benzene at 50℃; for 6h; | A 83.2% B 3.1% |
With sulfuryl dichloride In benzene at 60℃; for 4h; | A 83.2% B 4.8% |
3,5-dibromo-4-hydroxyphenylacetic acid ethyl ester
B
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
A 62% B n/a |
μ-tetrasulfido-1,2-dithio-dicarbonic acid bis-dimethylamide
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine | |
With tetrachloromethane; chlorine |
bis(dimethylthiocarbamoyl)sulfide
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine | |
With tetrachloromethane; chlorine |
N,N-dimethylthioformamide
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With pyridine; disulfur dichloride In dichloromethane | |
With chlorine In tetrachloromethane |
dichloromethylenedimethyliminium chloride
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With LiAlHSH at 0℃; for 1.5h; |
N,N-Dimethylthiocarbamoyl chloride
dichloromethylenedimethyliminium chloride
Conditions | Yield |
---|---|
With chlorine under 750.06 Torr; for 10h; Ambient temperature; | 100% |
With phosphorus pentachloride In tetrachloromethane for 1h; Heating; | 90% |
3-(trimethylsilyl)phenol
N,N-Dimethylthiocarbamoyl chloride
O-(3-trimethylsilylphenyl)-N,N-dimethylaminothiocarbamate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 85℃; | 100% |
4-(trimethylsilyl)phenol
N,N-Dimethylthiocarbamoyl chloride
O-(4-trimethylsilylphenyl)-N,N-dimethylaminothiocarbamate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 85℃; | 100% |
With sodium hydride In N,N-dimethyl-formamide at 85℃; for 6h; | 100% |
N,N-Dimethylthiocarbamoyl chloride
methyl (4-hydroxy-2-methylphenoxy)acetate
(4-dimethylthiocarbamoyloxy-2-methyl-phenoxy)-acetic acid methyl ester
Conditions | Yield |
---|---|
With dmap; triethylamine In 1,4-dioxane for 16h; Heating; | 100% |
p-hexylphenol
N,N-Dimethylthiocarbamoyl chloride
O-p-hexylphenyl N,N-dimethylthiocarbamate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 85℃; for 15h; | 100% |
p-heptylphenol
N,N-Dimethylthiocarbamoyl chloride
O-p-heptylphenyl N,N-dimethylthiocarbamate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 85℃; | 100% |
rac-6-bromo-3-nitro-2'-phenyl-[1,1'-binaphthalen]-2-ol
N,N-Dimethylthiocarbamoyl chloride
rac-O-(6-bromo-3-nitro-2'-phenyl-[1,1'-binaphthalen]-2-yl) dimethylthiocarbamate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 23℃; for 24h; | 100% |
4-bromo-2-hydroxyphenylcyclopentyl ketone
N,N-Dimethylthiocarbamoyl chloride
dimethylthiocarbamic acid O-(5-bromo-2-cyclopentanecarbonylphenyl) ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
methyl 5-methoxy-2-hydroxybenzoate
N,N-Dimethylthiocarbamoyl chloride
methyl 2-((dimethylcarbamothioyl)oxy)-5-methoxybenzoate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 20 - 60℃; for 4h; Inert atmosphere; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 55℃; for 3h; | 78% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil for 3h; Inert atmosphere; | 65% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 50℃; for 19h; Inert atmosphere; | 57% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 20℃; |
2-(5-hydroxyindane-2-yl)isoindole-1,3-dione
N,N-Dimethylthiocarbamoyl chloride
dimethylthiocarbamic acid O-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yl)indan-5-yl] ester
Conditions | Yield |
---|---|
Stage #1: 2-(5-hydroxyindane-2-yl)isoindole-1,3-dione; N,N-Dimethylthiocarbamoyl chloride With 1,4-diaza-bicyclo[2.2.2]octane In DMF (N,N-dimethyl-formamide) at 20℃; for 16h; Stage #2: With water at 0 - 20℃; for 18h; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 20℃; for 16h; | 70% |
1,4-diaza-bicyclo[2.2.2]octane
2-(5-hydroxyindane-2-yl)isoindole-1,3-dione
N,N-Dimethylthiocarbamoyl chloride
dimethylthiocarbamic acid O-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yl)indan-5-yl] ester
Conditions | Yield |
---|---|
In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 18h; | 100% |
N,N-Dimethylthiocarbamoyl chloride
ethyl 2-ethoxy-3-(4-hydroxy-phenyl)-propionate
3-(4-dimethylthiocarbamoyloxy-phenyl)-2-ethoxy-propionic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine; dmap In 1,4-dioxane at 100℃; for 10h; Heating / reflux; | 100% |
With dmap; triethylamine In 1,4-dioxane; dichloromethane | 140.1 g (~100%) |
6-bromo-naphthalen-2-ol
N,N-Dimethylthiocarbamoyl chloride
O-(6-bromonaphthalene-2-yl) dimethylcarbamothioate
Conditions | Yield |
---|---|
Stage #1: 6-bromo-naphthalen-2-ol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide; mineral oil at 20 - 80℃; for 17h; | 100% |
With sodium hydride In N,N-dimethyl-formamide at 80℃; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 20℃; for 48h; Inert atmosphere; | 82% |
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; potassium hydroxide In water; acetone | 100% |
N,N-Dimethylthiocarbamoyl chloride
4-bromo-2,3-dichlorophenol
dimethyl-thiocarbamic acid O-(4-bromo-2,3-dichloro-phenyl) ester
Conditions | Yield |
---|---|
Stage #1: 4-bromo-2,3-dichlorophenol With sodium hydride In DMF (N,N-dimethyl-formamide) at 0℃; for 0.5h; Stage #2: N,N-Dimethylthiocarbamoyl chloride In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide | 100% |
p-[4-(trifluoromethyl)phenoxy]phenol
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
Stage #1: p-[4-(trifluoromethyl)phenoxy]phenol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.25h; Inert atmosphere; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 100% |
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
With dmap; triethylamine In 1,4-dioxane at 80℃; for 15h; | 100% |
4-nitro-phenol
N,N-Dimethylthiocarbamoyl chloride
O-(4-nitrophenyl) N,N-dimethylcarbamothioate
Conditions | Yield |
---|---|
Stage #1: 4-nitro-phenol With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; Stage #2: N,N-Dimethylthiocarbamoyl chloride In 1-methyl-pyrrolidin-2-one at 50℃; for 2.5h; | 99% |
Stage #1: 4-nitro-phenol With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; Stage #2: N,N-Dimethylthiocarbamoyl chloride In 1-methyl-pyrrolidin-2-one at 50℃; for 2h; | 92% |
With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; for 2.5h; | 91% |
N,N-Dimethylthiocarbamoyl chloride
7-(tert-butyldimethylsilyloxy)heptan-1-ol
1-(tert-butyldimethylsilanyloxy)-7-(dimethylthiocarbamoyloxy)heptane
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In tetrahydrofuran at 20℃; for 10h; | 99% |
N,N-Dimethylthiocarbamoyl chloride
6α,9α-difluoro-17α-[(2-furylcarbonyl)oxy]-11β-hydroxy-16α-methyl-3-oxoandrost-1,4-dien-17β-thiocarboxylic acid S-N,N-dimethylcarbamoyl ester
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; triethylamine In tetrahydrofuran at 10 - 20℃; for 4h; | 99% |
With tetra-(n-butyl)ammonium iodide; triethylamine In tetrahydrofuran at 10 - 20℃; for 4h; | 99% |
Stage #1: GW694301X With triethylamine In butanone at 10 - 20℃; for 0.166667h; Stage #2: N,N-Dimethylthiocarbamoyl chloride In butanone for 0.166667h; Stage #3: With sodium iodide In water; butanone at 15 - 20℃; for 5h; | 87% |
With triethylamine; sodium iodide In butanone at 70 - 75℃; for 2h; |
methyl 2-hydroxy-5-nitrobenzoate
N,N-Dimethylthiocarbamoyl chloride
2-dimethylthiocarbamoyloxy-5-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 20℃; for 48h; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide for 3h; Inert atmosphere; | 68% |
5-bromo-2-hydroxy-3-nitrobenzoic acid ethyl ester
N,N-Dimethylthiocarbamoyl chloride
5-bromo-2-dimethylthiocarbamoyloxy-3-nitrobenzoic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 5-bromo-2-hydroxy-3-nitrobenzoic acid ethyl ester With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.166667h; Inert atmosphere; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃; Inert atmosphere; | 99% |
2,6-dibromo-4-(trifluoromethyl)phenol
N,N-Dimethylthiocarbamoyl chloride
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-(trifluoromethyl)phenol With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Stage #2: N,N-Dimethylthiocarbamoyl chloride In tetrahydrofuran at 0 - 60℃; for 20h; | 99% |
N,N-Dimethylthiocarbamoyl chloride
(aR)-2,2'-dihydroxy-6,6'-dimethoxy-1,1'-binaphthyl
Conditions | Yield |
---|---|
Stage #1: (aR)-2,2'-dihydroxy-6,6'-dimethoxy-1,1'-binaphthyl With sodium hydride In N,N-dimethyl-formamide at 15℃; for 2h; Inert atmosphere; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide at 80℃; for 2h; | 99% |
N,N-Dimethylthiocarbamoyl chloride
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 25℃; for 1h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: C66H66N2O5 With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 1h; Cooling with ice; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃; for 3h; Cooling with ice; | 99% |
7-hydroxy-2,2-dimethyl-chroman-4-one
N,N-Dimethylthiocarbamoyl chloride
2,2-Dimethyl-7-((N,N-dimethylthiocarbamoyl)oxy)-4-chromanone
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide for 2h; Ambient temperature; | 98% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide for 2h; Ambient temperature; | 98% |
methyl 4-hydroxylbenzoate
N,N-Dimethylthiocarbamoyl chloride
O-(4-carbomethoxyphenyl) N,N-dimethylthiocarbamate
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina In acetonitrile for 16h; Ambient temperature; | 98% |
With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; for 78h; | 92% |
With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; for 3h; | 92% |
3,5-dihydroxyphenol
N,N-Dimethylthiocarbamoyl chloride
Dimethyl-thiocarbamic acid O-(3,5-bis-dimethylthiocarbamoyloxy-phenyl) ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 0℃; for 3h; | 98% |
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