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inquiryUnique advantages for Dimethylcarbamoyl chloride Cas 79-44-7 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless to yellowish transparent liquid Storage:N/A Package:25kg/dr
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inquiryDimethylcarbamoyl chloride Basic information Product Name: Dimethylcarbamoyl chloride Synonyms: (Dimethylamino)carbonyl chloride;(dimethylamino)carbonylchloride;Carbamicchloride,dimethyl
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Min.Order:1 Kilogram
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79-44-7 Dimethylcarbamoyl chloride Application:79-44-7 Dimethylcarbamoyl chloride
Dimethylcarbamoyl chloride cas 79-44-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryDimethylcarbamoyl chloride Basic information Product Name: Dimethylcarbamoyl chloride Synonyms: (Dimethylamino)carbonyl chloride;(dimethylamino)carbonylchloride;Carbamicchloride,dimethyl-;Carbamoyl chlori
Conditions | Yield |
---|---|
at 200℃; Temperature; | 96.2% |
at 275℃; | |
With benzene at 0℃; | |
With toluene | |
In 1,4-dioxane at 0 - 20℃; |
chloro(chlorosulfanyl)methanone
dimethyl amine
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
Stage #1: chloro(chlorosulfanyl)methanone; dimethyl amine In dichloromethane at 40℃; Inert atmosphere; Stage #2: With chlorine In dichloromethane at 20℃; | 88% |
bis(trichloromethyl) carbonate
dimethyl amine
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide for 0.0333333h; Neat (no solvent); | 88% |
With sodium hydrogencarbonate In dichloromethane at -10℃; | 50.4% |
With pyridine In dichloromethane at 0 - 5℃; |
Conditions | Yield |
---|---|
Stage #1: Thiram With chlorine In dichloromethane at 24 - 26℃; for 6.33333h; Cooling with ice; Stage #2: With water; sodium hydrogencarbonate In dichloromethane Cooling with ice; | 86.2% |
Thiram
A
N,N-Dimethylthiocarbamoyl chloride
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride In benzene at 50℃; for 6h; | A 83.2% B 3.1% |
With sulfuryl dichloride In benzene at 60℃; for 4h; | A 83.2% B 4.8% |
N-Methoxy-N-chloro-N',N'-dimethylurea
A
methyl N,N-dimethylcarbamate
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In tetrachloromethane at 20℃; for 600h; | A 63.3% B 70% |
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon at 55℃; under 750.075 Torr; for 2h; Reagent/catalyst; Temperature; | 56% |
Conditions | Yield |
---|---|
With trichlorophosphate In acetonitrile for 3.5h; Heating; | 46.6% |
diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | A 17% B n/a |
Conditions | Yield |
---|---|
at 17℃; Geschwindigkeit der Zersetzung; |
Conditions | Yield |
---|---|
je nach Bedingungen; |
phosgene
toluene
trimethylamine
A
methylene chloride
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
at 60 - 70℃; |
phosgene
trimethylamine
A
methylene chloride
B
N,N-Dimethylcarbamoyl chloride
C7H18ClN3O2P(1+)*Cl(1-)
A
N,N,N',N'-Tetramethylphosphorodiamidic chloride
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In diethyl ether; dichloromethane Product distribution; |
dimethyl amine
trichloromethyl chloroformate
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In 1,4-dioxane at 55 - 60℃; for 4h; |
N,N-dimethyl-formamide
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With trichlorophosphate at 0℃; for 0.25h; | |
With thionyl chloride | |
With oxalyl dichloride In dichloromethane at 20℃; for 16.5h; |
1-(benzyloxy)-2,4-pentanedione
3-imino-3-<<2-(diisopropylamino)ethyl>amino>propionate
A
N,N-dimethyl-N'-<6-<(benzyloxy)methyl>-4-methyl-2-pyridyl>-N'-<2-(diisopropylamino)ethyl>urea
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With potassium hydroxide; copper Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With toluene at 60 - 70℃; |
Conditions | Yield |
---|---|
In benzene |
Methanesulfenyl chloride
S-methyl dimethylthiocarbamate
A
Dimethyldisulphide
B
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In hexane at 20℃; for 1h; |
Conditions | Yield |
---|---|
With chlorine In hexane at 20 - 40℃; |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; |
Conditions | Yield |
---|---|
With thionyl chloride for 3h; Reflux; |
Conditions | Yield |
---|---|
Stage #1: 3-methyl-phenol With sodium hydride In N,N-dimethyl-formamide at 20℃; Stage #2: N,N-Dimethylcarbamoyl chloride In N,N-dimethyl-formamide at 20℃; for 0.5h; | 100% |
Stage #1: 3-methyl-phenol With pyridine; potassium carbonate In acetonitrile for 0.333333h; Stage #2: N,N-Dimethylcarbamoyl chloride In acetonitrile for 2h; | 85% |
With pyridine In benzene |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 3h; | 100% |
trimethylsilyl cyanide
N,N-Dimethylcarbamoyl chloride
6-cyanothieno<2,3-b>pyridine
Conditions | Yield |
---|---|
In dichloromethane | 100% |
trimethylsilyl cyanide
N,N-Dimethylcarbamoyl chloride
thieno<2,3-b>pyridine 7-oxide
6-cyanothieno<2,3-b>pyridine
Conditions | Yield |
---|---|
In dichloromethane | 100% |
4-chloropyridine N-oxide
N,N-Dimethylcarbamoyl chloride
4-chloro-pyridine-2-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane | 100% |
With potassium carbonate In dichloromethane | 100% |
trimethylsilyl cyanide
N,N-Dimethylcarbamoyl chloride
4-chloro-pyridine-2-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane | 100% |
trimethylsilyl cyanide
N,N-Dimethylcarbamoyl chloride
2-cyano-4-methoxylpyridine
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane | 100% |
4-carbethoxypiperidine
N,N-Dimethylcarbamoyl chloride
ethyl 1-(N,N-Dimethylcarbamoyl)-4-piperidinecarboxylate
Conditions | Yield |
---|---|
With triethylamine at 20℃; | 100% |
2-(N,N-dimethylcarbamoylthio)-4-phenyl-imidazole
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
In pyridine; chloroform; water | 100% |
2,3-dimethylbenzenethiol
N,N-Dimethylcarbamoyl chloride
dimethyl-thiocarbamic acid S-(2,3-dimethylphenyl) ester
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethylbenzenethiol; N,N-Dimethylcarbamoyl chloride With sodium hydride In tert-butyl methyl ether at 0 - 60℃; for 1.5h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water Stage #3: With sodium hydroxide In tert-butyl methyl ether; water Product distribution / selectivity; | 100% |
Stage #1: 2,3-dimethylbenzenethiol; N,N-Dimethylcarbamoyl chloride With potassium carbonate In tert-butyl methyl ether at 0 - 60℃; for 29h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 0℃; Stage #3: With sodium hydroxide In tert-butyl methyl ether; water Product distribution / selectivity; | 100% |
Niclosamide
N,N-Dimethylcarbamoyl chloride
4-chloro-2-((2-chloro-4-nitrophenyl)carbamoyl)phenyl dimethylcarbamate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran Reflux; | 100% |
With pyridine; dmap Reflux; |
2-deuterio-4-methylphenol
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With triethylamine In chloroform at 0 - 20℃; | 100% |
3,3-dimethyl-2-(3-methylamino-phenyl)-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester
N,N-Dimethylcarbamoyl chloride
3,3-dimethyl-2-[3-(trimethyl-ureido)-phenyl]-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 25℃; for 12h; | 100% |
With pyridine In dichloromethane at 0 - 25℃; for 12h; |
Conditions | Yield |
---|---|
With sodium hydroxide In ethyl acetate at 50℃; for 16h; Reagent/catalyst; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethyl acetate at 50℃; for 16h; Reagent/catalyst; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethyl acetate at 50℃; for 16h; Reagent/catalyst; | 100% |
N,N-Dimethylcarbamoyl chloride
methyl 2-bromo-6-hydroxy-4-methoxybenzoate
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 80℃; for 0.5h; | 100% |
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 2h; | 100% |
tert-butyl 1,4-diazepine-1-carboxylate
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 2h; | 100% |
dimethyl-pyrrolidin-3-yl-amine
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 2h; | 100% |
4-n-Propylphenol
N,N-Dimethylcarbamoyl chloride
4-propylphenyl dimethylcarbamate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 8h; Sealed tube; Reflux; | 100% |
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 8h; | 100% |
N,N-Dimethylcarbamoyl chloride
methyl salicylate
methyl 2-((dimethylcarbamoyl)oxy)benzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 60℃; for 18h; | 100% |
(-)-meptazinol
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
Stage #1: (-)-meptazinol With sodium hydride In tetrahydrofuran for 0.5h; Stage #2: N,N-Dimethylcarbamoyl chloride In tetrahydrofuran at 0 - 20℃; for 2h; | 100% |
N,N-Dimethylcarbamoyl chloride
Conditions | Yield |
---|---|
Stage #1: 2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride With triethylamine In dichloromethane Stage #2: N,N-Dimethylcarbamoyl chloride In dichloromethane | 100% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane for 24h; Reflux; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 12h; | 99.8% |
trimethylsilyl isocyanate
N,N-Dimethylcarbamoyl chloride
A
chloro-trimethyl-silane
B
dimethylcarbamoyl isocyanate
Conditions | Yield |
---|---|
With tin(IV) chloride at 100 - 120℃; for 5h; | A 99% B 90% |
6-hydroxy-2H-naphtho<1,8-b,c>furan-2-one
N,N-Dimethylcarbamoyl chloride
Dimethyl-carbamic acid 2-oxo-2H-naphtho[1,8-bc]furan-6-yl ester
Conditions | Yield |
---|---|
With pyridine for 16h; Heating; | 99% |
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane for 60h; Ambient temperature; | 99% |
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