As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquirysuperior quality moderate price & quick delivery Appearance:pink or beige to brown crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request.
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry3-Hydroxybenzyl alcoholAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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3-Hydroxybenzyl alcohol cas 620-24-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:pink or beige to brown crystalline powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Conditions | Yield |
---|---|
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 0.25h; | 100% |
With sodium tetrahydroborate In ethanol at 0℃; for 1h; Inert atmosphere; | 100% |
With sodium tetrahydroborate In ethanol at 0℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; Trimethyl borate; dimethyl sulfate In tetrahydrofuran at 20℃; for 4.5h; | 97% |
Stage #1: 3-Carboxyphenol With 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane at 20℃; for 11h; Inert atmosphere; Stage #2: With silica gel In methanol at 50℃; for 3h; | 92% |
In sulfuric acid; water at 50℃; Product distribution; electroreduction; further reduction potentials, temperatures, electrolytes, cathodes; | 90% |
Conditions | Yield |
---|---|
With aluminum (III) chloride; sodium tetrahydroborate In tetrahydrofuran at 70℃; for 12h; Reagent/catalyst; Inert atmosphere; | 91% |
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol for 12h; Heating; | 90% |
methyl 3-hydroxybenzoate
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In 2-methyltetrahydrofuran at -15 - 20℃; for 24.16h; | 86% |
With sodium tetrahydroborate In water for 24h; Ambient temperature; | 60% |
A
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol at 20℃; for 2h; | A 5% B 85% |
3-iodobenzylalcohol
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
Stage #1: 3-iodobenzylalcohol With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide In water; dimethyl sulfoxide at 20 - 100℃; Inert atmosphere; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide at 20℃; Inert atmosphere; | 84% |
With copper(l) iodide; 8-quinolinol; potassium hydroxide In water; dimethyl sulfoxide; tert-butyl alcohol at 100℃; for 48h; Inert atmosphere; | 63% |
(3-Bromophenyl)methanol
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
Stage #1: (3-Bromophenyl)methanol With copper(l) iodide; cesium hydroxide; 5-bromo-2-(1H-imidazol-2-yl)pyridine In water; dimethyl sulfoxide; tert-butyl alcohol at 120℃; for 36h; Inert atmosphere; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide; tert-butyl alcohol pH=1 - 2; Inert atmosphere; | 83% |
(3-hydroxyphenyl)methyl 2-nitrobenzenesulfenate
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With piperidine In acetonitrile for 2h; Ambient temperature; | 74% |
Conditions | Yield |
---|---|
With sodium carbonate; bis(dibenzylideneacetone)-palladium(0); ruphos In 1,4-dioxane; water for 36h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Reflux; | 61.8% |
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; methanol; water at 50℃; for 1h; Inert atmosphere; Glovebox; Schlenk technique; | 43% |
Conditions | Yield |
---|---|
at 50 - 60℃; |
Conditions | Yield |
---|---|
With sodium hydroxide at 50 - 60℃; |
Conditions | Yield |
---|---|
at 70℃; bei der elektrolytischen Reduktion; |
hydrogenchloride
water
3-Carboxyphenol
A
3-Hydroxybenzyl alcohol
B
meta-hydroxybenzaldehyde
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate at 20 - 30℃; |
benzyl alcohol
B
salicylic alcohol
C
3-Hydroxybenzyl alcohol
D
benzaldehyde
Conditions | Yield |
---|---|
With water; dinitrogen monoxide at 20℃; pH=6; Kinetics; Radiolysis; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SnCl2; hydrochloric acid / ueber mehrerer Stufen 2: sodium amalgam View Scheme |
3-acetoxybenzyl acetate
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With methanol; sulfuric acid for 4h; Heating / reflux; |
Conditions | Yield |
---|---|
With triethylsilane; palladium dichloride In ethanol for 0.5h; Inert atmosphere; | A 6.5 %Chromat. B 92.0 %Chromat. |
benzyl alcohol
A
(4-hydroxyphenyl)methanol
B
salicylic alcohol
C
3-Hydroxybenzyl alcohol
D
benzaldehyde
E
4-hydroxy-benzaldehyde
F
salicylaldehyde
G
meta-hydroxybenzaldehyde
H
benzoic acid
Conditions | Yield |
---|---|
With water; oxygen at 24.84℃; under 760.051 Torr; for 5h; Sonication; Irradiation; |
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol at 240℃; for 2h; Autoclave; Inert atmosphere; | A 14 %Chromat. B 65 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: 3-methyl-phenol With 4-methylphenyl phosphate synthase; ATP; magnesium chloride; manganese(ll) chloride In aq. buffer at 30℃; for 2h; pH=8; Enzymatic reaction; Stage #2: With ferredoxin reductase; ferredoxin; P450 monooxygenase; NADPH In aq. buffer at 30℃; for 2h; pH=8; Enzymatic reaction; Stage #3: With phosphohydrolase In aq. buffer at 30℃; for 2h; pH=8; Enzymatic reaction; | A 29.8 %Chromat. B 5.3 %Chromat. |
benzyl alcohol-d7
benzyl alcohol
A
(4-hydroxyphenyl)methanol
B
salicylic alcohol
C
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With water; oxygen; titanium(IV) oxide at 25℃; for 2h; Catalytic behavior; Reagent/catalyst; Irradiation; |
3-hydroxy-trans-cinnamic acid
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With whole cells of recombinant strain VA1 In aq. phosphate buffer at 30℃; for 24h; pH=7.4; Microbiological reaction; |
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With lipase from Candida antarctica B In aq. buffer at 20℃; for 24h; pH=7; Enzymatic reaction; |
Conditions | Yield |
---|---|
With Candida cylindracea lipase In hexane for 4h; | 100% |
Y5(OiPr)13O at 20℃; for 18h; Acetylation; transesterification; | 93% |
With Pseudomonas cepacia PS lipase In di-isopropyl ether at 25℃; for 0.5h; |
Conditions | Yield |
---|---|
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | 100% |
With manganese(IV) oxide; manganese(II) nitrate tetrahydrate; dibenzoyl peroxide In hexane at 70℃; under 760.051 Torr; for 0.0833333h; chemoselective reaction; | 99% |
In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 7h; Reflux; Inert atmosphere; | 100% |
With potassium carbonate In acetone for 4h; Heating; | 95% |
With potassium carbonate In acetone at 45℃; for 12h; Williamson Ether Synthesis; | 89% |
3-Hydroxybenzyl alcohol
2-chloro-5-trifluoromethylpyridine
[3-[[5-(trifluoromethyl)-2-pyridyl]oxy]phenyl]methanol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 95 - 105℃; for 5h; Product distribution / selectivity; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 90 - 95℃; for 16h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 95℃; for 16h; Product distribution / selectivity; | 53% |
With potassium carbonate In N,N-dimethyl-formamide at 95℃; for 16h; | 53% |
With potassium carbonate In N,N-dimethyl-formamide at 95℃; for 16h; | 53% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 12h; | 99.8% |
3-Hydroxybenzyl alcohol
3-hydroxybenzyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; triethylamine In benzene at 0 - 20℃; for 6h; | 99% |
With 1-pyrrolidinecarboxaldehyde; 1,3,5-trichloro-2,4,6-triazine In 1,4-dioxane at 40℃; for 12h; Sealed tube; Green chemistry; | 82% |
With thionyl chloride In chloroform at 20℃; for 1h; | 78% |
6-chloronicotinonitrile
3-Hydroxybenzyl alcohol
Conditions | Yield |
---|---|
With potassium carbonate In ISOPROPYLAMIDE at 100℃; for 4h; | 99% |
With potassium carbonate In N,N-dimethyl acetamide at 100℃; |
Conditions | Yield |
---|---|
In tetrahydrofuran at 25 - 67℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 2h; | 98% |
With pyridine at 0 - 20℃; for 3h; Inert atmosphere; | 98% |
3-Hydroxybenzyl alcohol
ethyl bromoacetate
3-hydroxymethyl-1-ethoxycarbonylmethoxybenzene
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 12h; Heating / reflux; | 97% |
With potassium carbonate In acetone at 60℃; for 18h; Inert atmosphere; | 73% |
With potassium carbonate In N,N-dimethyl-formamide | |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 10 g |
With potassium carbonate In acetone for 12h; Reflux; |
3-Hydroxybenzyl alcohol
4-chlorobenzaldehyde
1-(4'-chlorophenyl)-1.3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.0333333h; oxa-Pictet-Spengler reaction; Microwave irradiation; | 97% |
With toluene-4-sulfonic acid In methanol at 38℃; for 48h; Pictet-Spengler cyclisation; Inert atmosphere; | 56% |
3-Hydroxybenzyl alcohol
vanillin
1-(4'-hydroxy-3'-methoxyphenyl)-1.3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.025h; oxa-Pictet-Spengler reaction; Microwave irradiation; | 97% |
With toluene-4-sulfonic acid In methanol at 38℃; for 48h; Pictet-Spengler cyclisation; Inert atmosphere; | 55% |
3-Hydroxybenzyl alcohol
m-hydroxybenzyl bromide
Conditions | Yield |
---|---|
With phosphorus tribromide In chloroform for 2h; Ambient temperature; | 96% |
With phosphorus tribromide In dichloromethane at 0 - 20℃; for 1h; | 86.3% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; for 1.5h; | 82% |
1-bromomethylpyrene
3-Hydroxybenzyl alcohol
3-(1-pyrenylmethyloxy)benzyl alcohol
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In acetone for 22h; Heating; | 96% |
3,5-di(o-carboranylmethoxy)benzylbromide
3-Hydroxybenzyl alcohol
3-[3,5-di(o-carboranylmethoxy)benzyloxy]benzylalcohol
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone for 24h; Heating / reflux; | 96% |
With potassium carbonate; potassium iodide In acetone for 24h; Heating / reflux; | 96% |
3-Hydroxybenzyl alcohol
benzaldehyde
1-phenyl-1,3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.0333333h; oxa-Pictet-Spengler reaction; Microwave irradiation; | 96% |
With toluene-4-sulfonic acid In methanol at 38℃; for 48h; Pictet-Spengler cyclisation; Inert atmosphere; | 60% |
3-Hydroxybenzyl alcohol
4-methoxy-benzaldehyde
1-(4'-methoxyphenyl)-1.3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.5h; oxa-Pictet-Spengler reaction; | 96% |
With toluene-4-sulfonic acid In methanol at 38℃; for 48h; Pictet-Spengler cyclisation; Inert atmosphere; | 62% |
oxa-Pictet-Spengler cyclisation; |
3-Hydroxybenzyl alcohol
propargyl bromide
(3-(prop-2-yn-1-yloxy)phenyl)methanol
Conditions | Yield |
---|---|
With sodium hydroxide In water for 24h; | 95% |
With sodium hydroxide In water at 10 - 35℃; for 24h; | 31% |
With sodium hydroxide In tetrahydrofuran; water; xylene for 6h; Heating / reflux; |
3-Hydroxybenzyl alcohol
ethyl 3-(N-chloroacetylamino)propionate
Ethyl 3-(2-(3-(hydroxymethyl)phenoxy)acetamido)propanoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 12h; Heating / reflux; | 95% |
3-Hydroxybenzyl alcohol
4-bromo-benzaldehyde
1-(4-bromophenyl)-1,3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.0333333h; oxa-Pictet-Spengler reaction; Microwave irradiation; | 95% |
3-Hydroxybenzyl alcohol
2,2,2-trichloroacetophenone
3-hydroxybenzenemethanol benzoate
Conditions | Yield |
---|---|
With N,N,N',N'',N'''-pentamethyldiethylenetriamine In acetonitrile at 20 - 25℃; for 16h; | 95% |
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 95% |
3-Hydroxybenzyl alcohol
triphenylphosphine hydrogen iodide
Conditions | Yield |
---|---|
In acetonitrile at 90℃; for 12h; | 95% |
3-Hydroxybenzyl alcohol
3,4-dimethoxy-benzaldehyde
1-(3'.4'-dimethoxyphenyl)-1.3-dihydroisobenzofuran-5-ol
Conditions | Yield |
---|---|
With nanosilica supported sulfuric acid In ethanol at 80℃; for 0.025h; oxa-Pictet-Spengler reaction; Microwave irradiation; | 94% |
With toluene-4-sulfonic acid In methanol at 38℃; for 48h; Pictet-Spengler cyclisation; Inert atmosphere; | 55% |
3-Hydroxybenzyl alcohol
ethyl acetoacetate
2,6-dimethyl-3,5-diethoxycarbonyl-4-(3-hydroxyphenyl)-1,4-dihydropyridine
Conditions | Yield |
---|---|
With ammonium hydroxide; hydrogen bromide; dimethyl sulfoxide In water at 75℃; for 2.53333h; | 94% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In chloroform; water; N,N-dimethyl-formamide | 93.1% |
3-Hydroxybenzyl alcohol
tert-butyldimethylsilyl chloride
tert-butyl((3-((tert-butyldimethylsilyl)oxy)benzyl)oxy)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide Ambient temperature; | 93% |
With 1H-imidazole In tetrahydrofuran at 25℃; for 3h; | |
With lipase from Candida antarctica B In hexane at 20℃; for 24h; Enzymatic reaction; |
3-Hydroxybenzyl alcohol
triethylene glycol di-(p-toluenesulfonate)
[ethane-1,2-diylbis(oxyethane-2,1-diyloxy-3,1-phenylene)]dimethanol
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 22h; Heating; | 93% |
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