As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:100-83-4
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct Description Product Name 3-Hydroxybenzaldehyde CAS No. 100-83-4 Appearance Yellowish crystalline powder Assay ≥99% Capacity 500mt/year Min.packing 100g
Cas:100-83-4
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:White or Light yellow power Package:1kg/foil bag; 1kg/tin
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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:100-83-4
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inquiry3-Hydroxybenzaldehyde CAS: 100-83-4 Molecular formula: C7H6O2 Molecular weight: 122.12 Physical properties Melting point: 101-105°C Boiling point: 191°C (50 mmHg) Water-soluble: SOLUBLE Uses: Hydroxybenzaldehyde is used as medicine
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:100-83-4
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiry
Cas:100-83-4
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inquiryName:3-Hydroxybenzaldehyde CAS:100-83-4 Grade:For chemical industry, scientific research and export Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without vulnerabili
Cas:100-83-4
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:100-83-4
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inquiryProduct Name: 3-Hydroxybenzaldehyde Synonyms: 3-FORMYLPHENOL;3-HYDROXYBENZALDEHYDE;MHB;M-HYDROXYBENZALDEHYDE;3-Hydroxydenzaldehyde;3-Hydroxybenzaldehyde m-Hydroxybenzaldehyde;3-Hydroxybenzaldehyde,99.5%;3-Hydroxybenzaldehyde, 98.50% CAS: 100-83-4
Cas:100-83-4
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:100-83-4
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:100-83-4
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inquiryChemical Name: 3-Hydroxybenzaldehyde CAS No.: 100-83-4 Molecular Fomula:C7H6O2 Chemical Structure: Molecular weight: 122.12 Appearance: white crystalline powder Assay: 99% min Appearance:White powder Storage:Store in cool and dry place, away fro
Cas:100-83-4
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inquiryAppearance:faintly yellow to light brown powder Storage:Inert atmosphere,2-8°C Package:25kg/drum Application:Intermediate for dyes, plastics, pharmaceuticals, and bactericides; color reagent for Schiff’s reagent, sensitizing agent in photographic
Cas:100-83-4
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inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:100-83-4
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryProduct Name: 3-Hydroxybenzaldehyde Synonyms: 3-hydroxy-benzaldehyd;Benzaldehyde, m-hydroxy-;hydroxybenzaldehyde;m-Aldehydophenol;m-Formylphenol;m-hydroxy-benzaldehyd;META-HYDROXY BENZALDEHYDE;HYDROXYBENZALDEHYDE-3 CAS: 100-83-4 MF: C7H6O
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inquiry3-Hydroxybenzaldehyde CAS: 100-83-4 .Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcin
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:100-83-4
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Conditions | Yield |
---|---|
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | 100% |
With manganese(IV) oxide; manganese(II) nitrate tetrahydrate; dibenzoyl peroxide In hexane at 70℃; under 760.051 Torr; for 0.0833333h; chemoselective reaction; | 99% |
In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation; | 99% |
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 100% |
Conditions | Yield |
---|---|
With iron(III) chloride on silica In neat (no solvent) at 80℃; for 0.5h; | 99% |
With magnesium iodide for 5h; neat (no solvent); | 93% |
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With lithium acetate In water; N,N-dimethyl-formamide at 25℃; for 8h; Inert atmosphere; | 96% |
With triethylamine N-oxide In methanol for 1h; | 91% |
In water; dimethyl sulfoxide at 90℃; for 8h; | 87% |
2-(3-hydroxyphenyl)-1,3-dithiolane
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With ammonium iodide; dihydrogen peroxide; sodium dodecyl-sulfate In water at 20℃; for 1h; micellar medium; | 96% |
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; dihydrogen peroxide In water; acetonitrile at 20℃; for 1h; | 94% |
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 3h; Micellar solution; | 90% |
2-(3-hydroxyphenyl)-1,3-dithiane
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.666667h; Micellar solution; | 95% |
With acetic acid at 25℃; for 15h; | 51% |
3-benzenesulfonyloxy-benzaldehyde
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide In toluene; tert-butyl alcohol at 100℃; for 0.5h; Inert atmosphere; | 95% |
3-Formylphenylboronic acid
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With C100H52N4O16Sn(6-)*2In(3+); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 3.5h; Irradiation; | 94% |
With C18H28Cl2CuN2O4 In water at 26℃; for 0.333333h; | 92% |
With 10-methylacridine-3(10H)-one; oxygen; N-ethyl-N,N-diisopropylamine In water at 20℃; for 20h; Irradiation; Green chemistry; | 90% |
3-allyloxy-benzaldehyde
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With bis(benzonitrile)palladium(II) dichloride In benzene for 20h; Heating; | 92% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol at 20℃; for 6h; | 82% |
3-((triisopropylsilyl)oxy)benzaldehyde
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium acetate In water; N,N-dimethyl-formamide at 25℃; for 13h; | 92% |
Conditions | Yield |
---|---|
With oxygen; potassium carbonate In N,N-dimethyl-formamide at 80℃; for 12h; | 92% |
3-hydroxybenzaldehyde oxime
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With N,N'-dichlorophenobarbital In acetonitrile at 20℃; | 92% |
With iodine at 45 - 60℃; for 0.2h; Reagent/catalyst; Microwave irradiation; | 83% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); t-BuBrettPhos; p-methylbenzaldehyde oxime; caesium carbonate In N,N-dimethyl-formamide at 90℃; for 2h; Inert atmosphere; | 92% |
With nickel(II) sulphate; water; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 12h; pH=8.8; UV-irradiation; Inert atmosphere; Glovebox; Enzymatic reaction; | 70 %Spectr. |
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With tribromo-isocyanuric acid In acetonitrile for 1.5h; Reflux; | 90% |
Conditions | Yield |
---|---|
With magnesium iodide for 5h; neat (no solvent); | 89% |
With 1-methyl-pyrrolidin-2-one; potassium carbonate at 190℃; for 0.5h; | 85% |
With 1-methyl-pyrrolidin-2-one; potassium carbonate; thiophenol for 0.5h; Heating; | 85% |
3-(4-Methoxybenzyloxy)benzaldehyde
A
p-methoxybenzyl acetate
B
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With acetic acid at 90℃; for 24h; | A n/a B 88% |
Acetic acid acetoxy-(3-hydroxy-phenyl)-methyl ester
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In acetonitrile at 70℃; for 5.5h; | 88% |
With formic acid; water; sodium dodecyl-sulfate for 4h; Heating; | 80% |
Conditions | Yield |
---|---|
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 2h; Sealed tube; | 88% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 88% |
N-(2,4-dinitrophenyl)-N'-(3'-hydroxybenzylidene)hydrazone
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With 1,4-dichloro-1,4-diazoniabicyclo[2,2,2]octane bischloride In water at 50℃; for 0.25h; pH=7; | 86% |
3-Hydroxybenzyl alcohol
A
(m-hydroxybenzyl) methyl ether
B
meta-hydroxybenzaldehyde
C
3-Carboxyphenol
Conditions | Yield |
---|---|
With sodium hydroxide; oxygen; platinum on activated charcoal; cerium(III) chloride; bismuth(III) sulfate In methanol; water at 50℃; for 2h; | A 5 % Chromat. B 83% C 1 % Chromat. |
With sodium hydroxide; oxygen; platinum on activated charcoal; bismuth(III) sulfate In methanol; water at 50℃; for 2h; | A 6 % Chromat. B 71 % Chromat. C 18 % Chromat. |
With sodium hydroxide; oxygen; platinum on activated charcoal; cerium(III) chloride; bismuth(III) sulfate In methanol; water at 50℃; for 2h; Product distribution; further solvent: water; further catalyst: 3percent Pt/C, Bi2(SO4)3; | A 6 % Chromat. B 71 % Chromat. C 18 % Chromat. |
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate; tris(2,2'-bipyridine)nickel(II) tetrafluoroborate In N,N-dimethyl-formamide electrochem. reaction; magnesium rod anode, nickel foam grid cathode; | 83% |
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With copper(II) nitrate hexahydrate In dichloromethane; water at 20℃; for 5h; | 83% |
Conditions | Yield |
---|---|
With poly(4-vinylpyridinium) hydrogen sulfate solid acid In methanol at 20℃; for 0.633333h; Irradiation; | 82% |
3-hydroxybenzoyl chloride
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen; triethylamine at 120℃; Autoclave; | 81.5% |
1α-H, 2α-H, 4α-H, 5α-H-3,9-Dioxatricyclo<3.3.1.02,4>nonan-7-on
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 0.25h; Ambient temperature; ice-cooling (adding); | 72% |
With lithium diisopropyl amide | 57% |
Sodium; hydroxy-(3-hydroxy-phenyl)-methanesulfonate
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With ammonium acetate for 0.0333333h; microwave irradiation; | 72% |
salicylaldoxime
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With aluminum oxide; ammonium chlorochromate at 35℃; for 2h; oxidative deoximation; | 70% |
(R,S)3-hydroxymandelic acid
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With Ag-Ag2S nanoparticles supported on cellulose In water at 80℃; for 0.05h; Microwave irradiation; Green chemistry; | 65% |
Conditions | Yield |
---|---|
Stage #1: 3-Bromophenol With n-butyllithium; isopropylmagnesium chloride In tetrahydrofuran; hexane at 0 - 5℃; for 1h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 1h; Further stages.; | 64% |
acetic anhydride
meta-hydroxybenzaldehyde
3-Acetoxy-1-(diacetoxymethyl)benzene
Conditions | Yield |
---|---|
With sulphated zirconia regioselective reaction; | 100% |
In neat (no solvent) at 20℃; for 0.1h; Green chemistry; chemoselective reaction; | 97% |
H6P2W18O62 at 20℃; for 0.5h; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 18h; Heating; | 100% |
With potassium carbonate; sodium iodide In ethanol for 3h; Reflux; | 100% |
With potassium carbonate In ethanol for 3h; Reflux; | 100% |
Conditions | Yield |
---|---|
In ethanol at 0 - 5℃; for 2h; | 100% |
at 20℃; for 12h; | 100% |
With benzene zuletzt unter Abdestillieren des gebildeten Wassers; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 70℃; | 90% |
In acetone | 88% |
Conditions | Yield |
---|---|
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 0.25h; | 100% |
With sodium tetrahydroborate In ethanol at 0℃; for 1h; Inert atmosphere; | 100% |
With sodium tetrahydroborate In ethanol at 0℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With bromine In dichloromethane | 100% |
With bromine In dichloromethane | 100% |
With 1,3-di-n-butyl-1H-imidazol-3-ium tribromide at 20℃; for 0.133333h; Neat (no solvent); regioselective reaction; | 95% |
3,5-dimethyl-4-nitroisoxazole
meta-hydroxybenzaldehyde
3-[(E)-2-(3-Methyl-4-nitro-isoxazol-5-yl)-vinyl]-phenol
Conditions | Yield |
---|---|
With pyrrolidine In neat (no solvent) at 20℃; for 0.116667h; Aldol Condensation; | 100% |
With base |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 12h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 23℃; for 3h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 14h; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol Heating; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 160℃; for 0.5h; | 90% |
Conditions | Yield |
---|---|
In di-isopropyl ether; water for 0.0416667h; Product distribution; Ambient temperature; separation of aldehyde; | 100% |
meta-hydroxybenzaldehyde
Sodium; hydroxy-(3-hydroxy-phenyl)-methanesulfonate
Conditions | Yield |
---|---|
With sodium hydrogensulfite In di-isopropyl ether; water for 0.0833333h; Product distribution; Ambient temperature; separation of aldehyde; | 100% |
With sodium hydrogensulfite at 50℃; for 1h; |
tert-butyldimethylsilyl chloride
meta-hydroxybenzaldehyde
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 25℃; for 16h; | 100% |
With triethylamine In dichloromethane at 20℃; for 2h; | 100% |
With 1H-imidazole In dichloromethane at 0 - 20℃; | 100% |
ethyl bromoacetate
meta-hydroxybenzaldehyde
ethyl 2-(3-formylphenoxy)acetate
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone Heating; | 100% |
With potassium carbonate In acetonitrile at 70℃; for 4h; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20 - 80℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; toluene at 25℃; for 16h; | 100% |
With 18-crown-6 ether; potassium carbonate In acetonitrile Inert atmosphere; Reflux; | 99% |
With tetrabutylammomium bromide; potassium carbonate In tetrahydrofuran; water at 50℃; for 4h; | 94% |
meta-hydroxybenzaldehyde
4-piperidyl N-(2-biphenyl)carbamate
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In dichloromethane for 3h; Ambient temperature; | 100% |
meta-hydroxybenzaldehyde
N-hexyl-2-cyanoacetylamide
Conditions | Yield |
---|---|
piperidine at 20℃; Knoevenagel condensation; solvent free; | 100% |
With piperidine In ethanol for 2h; Heating; | 57% |
meta-hydroxybenzaldehyde
1-bromo-3-propanol
3-(3-hydroxy-propoxy)-benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 3h; Reflux; | 100% |
Stage #1: meta-hydroxybenzaldehyde With potassium carbonate In DMF (N,N-dimethyl-formamide) for 0.166667h; Stage #2: 1-bromo-3-propanol In DMF (N,N-dimethyl-formamide) for 2h; Heating / reflux; | 95% |
With potassium carbonate In acetonitrile for 48h; Heating; | 90% |
With potassium carbonate In acetonitrile for 48h; Heating / reflux; | 90% |
With potassium carbonate In acetonitrile for 5h; Heating / reflux; |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In DMF (N,N-dimethyl-formamide) at 90℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 3h; |
Conditions | Yield |
---|---|
With sodium acetate; acetic acid In toluene for 4h; Reflux; Dean-Stark; | 100% |
In isopropyl alcohol at 80 - 90℃; for 2h; | 75% |
With piperidine; acetic acid for 0.333333h; Knoevenagel Condensation; Microwave irradiation; |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
meta-hydroxybenzaldehyde
3(S)-(tert-butoxycarbonylamino)pyrrolidine
tert-butyl N-[(3S)-1-[(3-hydroxyphenyl)methyl]pyrrolidin-3-yl]carbamate
Conditions | Yield |
---|---|
Stage #1: meta-hydroxybenzaldehyde; 3(S)-(tert-butoxycarbonylamino)pyrrolidine With acetic acid In dichloromethane at 20℃; for 1h; Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 4h; | 100% |
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 24h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With pyridine; copper(I) bromide dimethylsulfide complex; sodium carbonate In acetonitrile at 75℃; for 48h; Inert atmosphere; solid phase reaction; | 100% |
N-benzyl-2-amino-5-(pyrrolidin-1-yl)benzamide
meta-hydroxybenzaldehyde
2-(3-hydroxyphenyl)-3-benzyl-6-(pyrrolidin-1-yl)-1,2,3,4-tetrahydro-1H-quinazolin-4-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl acetamide at 20℃; for 2h; | 100% |
meta-hydroxybenzaldehyde
N-(3-hydroxy-benzylidene)-N'-(7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine
Conditions | Yield |
---|---|
Stage #1: (7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl)hydrazine trifluoroacetate; meta-hydroxybenzaldehyde In ethanol at 1 - 30℃; for 1h; Stage #2: With NH-silica gel In methanol; dichloromethane | 100% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 100% |
Conditions | Yield |
---|---|
Stage #1: meta-hydroxybenzaldehyde; aniline With acetic acid In dichloromethane at 20℃; for 24h; Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 24h; | 100% |
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; silver trifluoromethanesulfonate In dichloromethane at 20℃; for 1h; | 92% |
Stage #1: meta-hydroxybenzaldehyde; aniline In ethanol at 80℃; for 3h; Inert atmosphere; Stage #2: With methanol; sodium tetrahydroborate for 1h; | 36% |
With sodium tris(acetoxy)borohydride; acetic acid In methanol at 20℃; for 42h; Reagent/catalyst; Time; |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1.5h; | 85% |
meta-hydroxybenzaldehyde
3,4-dichlorobenzyl bromide
3-[(3,4-dichlorobenzyl)oxy]benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; Inert atmosphere; | 100% |
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