As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-Amino-5-chlorobenzophenone CAS No.
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryFactory supply 2-Amino-5-chlorobenzophenone CAS 719-59-5 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, F
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryTIANFUCHEM--719-59-5--2-Amino-5-chlorobenzophenone factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable busine
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inquiryProduct Name: 2-Amino-5-chlorobenzophenone Alias: (2-amino-5-chlorophenyl)phenyl-methanon;2-Amino-5-chlorbenzophenon;2-Amino-5-chlorbenzophenone;2-Amino-5-chlorodiphenylone;2-Benzoyl-4-chloroaniline;Methanone, (2-amino-5-chlorophenyl)phenyl-;(2-AMIN
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inquiry2-Amino-5-chlorobenzophenone CAS:719-59-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
2-Amino-5-chlorobenzophenone CAS: 719-59-5 Specification Product Name 2-Amino-5-chlorobenzophenone CAS No. 719-59-5 Appearance Yellow needle crystal powder
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryConditions | Yield |
---|---|
With trimethylsilyl iodide; water In acetonitrile at 20℃; for 0.2h; | 98% |
Stage #1: 5-chloro-3-phenylanthranil With iron In ethanol for 0.5h; Reflux; Stage #2: With sulfuric acid In ethanol for 1h; Reflux; | 95.1% |
With aluminium trichloride; zinc In tetrahydrofuran for 6h; Ambient temperature; | 92% |
2-amino-5-chlorobenzonitrile
phenylboronic acid
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate; water In 2-methyltetrahydrofuran at 80℃; for 36h; Schlenk technique; | 96% |
With [2,2]bipyridinyl; methanesulfonic acid; palladium(II) trifluoroacetate In tetrahydrofuran; water at 80℃; for 36h; |
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With triethylene diamine nickel thiosulfate; water In chloroform at 20℃; for 0.166667h; Hydrolysis; | 92% |
2-amino-5-chlorobenzonitrile
sodium benzenesulfonate
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With p-nitrobenzenesulfonic acid; palladium diacetate In tetrahydrofuran; water at 80℃; for 48h; Inert atmosphere; Schlenk technique; | 92% |
Conditions | Yield |
---|---|
Stage #1: benzamide; 4-chloro-aniline With tin(ll) chloride at 123 - 250℃; for 4h; Stage #2: With potassium chloride at 95 - 130℃; for 4h; Stage #3: With phosphoric acid for 23h; Concentration; Temperature; Reflux; | 91% |
7-Chlor-2-methylthio-5-phenyl-3H-1,3,4-benzotriazepin
A
methylthiol
B
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With hydrogenchloride for 10h; | A n/a B 83.4% |
Conditions | Yield |
---|---|
With gallium(III) trichloride; boron trichloride In chlorobenzene at 100℃; for 20h; | 81% |
With gallium(III) trichloride; boron trichloride 1.) CH2Cl2, 1,1,2,2-tetrachloroethane, 0 deg C, 2.) 1,1,2,2-tetrachloroethane, 100 deg C, 5 h; Yield given. Multistep reaction; |
5-chloro-3-phenylanthranil
phenylboronic acid
A
2-Amino-5-chlorobenzophenone
B
(5-chloro-2-(phenylamino)phenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With potassium carbonate; copper dichloride In dimethyl sulfoxide at 100℃; for 6h; Reagent/catalyst; Solvent; Sealed tube; | A 17% B 81% |
Conditions | Yield |
---|---|
With antimony(III) oxide In dichloromethane at 15℃; for 2h; Temperature; | 78% |
Stage #1: 4-chloro-aniline; benzoyl chloride With antimony(III) trioxide In dichloromethane at 15℃; for 2h; Friedel-Crafts Acylation; Stage #2: With nitric acid In dichloromethane at 10 - 45℃; for 11.5h; Temperature; | 77% |
With dysprosium((III) oxide In tetrachloromethane at 15℃; for 2h; Temperature; | 76% |
7-chloro-9-phenyl-1,2-dihydrooxazolo<2,3-b>-1,3,4-benzotriazepine
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With sulfuric acid In ethanol at 40℃; for 1.16667h; | 75% |
carbon monoxide
p-chloro-o-iodoaniline
phenylboronic acid
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With potassium carbonate at 100℃; under 2250.23 Torr; for 8h; Catalytic behavior; Suzuki-Miyaura Coupling; Autoclave; | 75% |
5-chloro-2-[(phenylsulfonyl)amino]benzoic acid
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; triphenylphosphine In 1,4-dioxane at 25℃; for 8h; Schlenk technique; Inert atmosphere; Sealed tube; Irradiation; | 73% |
(2-amino-5-chlorophenyl)(phenyl)methanol
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; (R)-1,1'-binaphthyl-2,2'-diamine In toluene at 60℃; for 48h; | 61% |
With 1,4-diaza-bicyclo[2.2.2]octane; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; copper(l) chloride In toluene at 100℃; for 24h; | 58% |
With copper(II) chloride monohydrate; oxygen; potassium carbonate In N,N-dimethyl-formamide at 60℃; for 24h; | |
With copper(II) chloride monohydrate; potassium carbonate In N,N-dimethyl-formamide at 60℃; | |
With copper(II) chloride monohydrate; potassium carbonate In N,N-dimethyl-formamide at 60℃; for 24h; |
5-chloro-2-phenylindole
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With oxygen; caesium carbonate In dimethyl sulfoxide at 140℃; for 8h; | 59% |
7-chloro-3-methyl-2-(methyl-thio)-5-phenyl-3H-1,3,4-benzotriazepine
A
methylthiol
B
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With hydrogenchloride for 10h; | A n/a B 57.7% |
propylamine
5-chloro-2-trichloroacetylaminobenzophenone
A
2-Amino-5-chlorobenzophenone
B
syn-5-chloro-2-trichloroacetamidobenzophenone n-propylimine
C
6-chloro-3,4-dihydro-4-phenyl-3-(n-propyl)-4-trichloromethyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In ethanol at 60℃; for 3h; | A 16% B 57% C 13% |
(2-amino-5-chlorophenyl)(phenyl)methanol
C
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-1,1'-binaphthyl-2,2'-diamine In toluene at 60℃; for 24h; optical yield given as %ee; | A n/a B n/a C 57% |
(2-amino-5-chlorophenyl)(phenyl)methanol
B
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-1,1'-binaphthyl-2,2'-diamine In toluene at 80℃; for 11h; optical yield given as %ee; | A n/a B 57% |
5-chloro-2-trichloroacetylaminobenzophenone
ethanolamine
A
2-Amino-5-chlorobenzophenone
B
9-chloro-10b-phenyl-2,3,6,19b-tetrahydro-5H-oxazolo<3,2-c>quinazolin-5-one
C
6-chloro-3,4-dihydro-3-(2-hydroxyethyl)-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In ethanol for 3h; Heating; | A 17% B 43% C 38% |
3-Amino-6-chlor-4-hydroxy-4-phenyl-2-thioxo-1,2,3,4-tetrahydrochinazolin
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With hydrogenchloride for 10h; Heating; | 41.5% |
Multi-step reaction with 2 steps 1: 1) CH3ONa, 2) HCl (g) / 1) acetone, 7 d, RT, 2) benzene 2: 5 M HCl / Heating; hydrolysis View Scheme |
3-Amino-6-chlor-4-hydroxy-2-methylthio-4-phenyl-3,4-dihydrochinazolinhydrochlorid
A
methylthiol
B
2-Amino-5-chlorobenzophenone
C
3-Amino-6-chlor-4-hydroxy-2-oxo-4-phenyltetrahydrochinazolin
D
N-(2-Benzoyl-4-chlorphenyl)monothiocarbamidsaeure-S-methylester
Conditions | Yield |
---|---|
With hydrogenchloride for 0.5h; Heating; reflux; | A n/a B 37% C n/a D n/a |
With hydrogenchloride Product distribution; Heating; hydrolysis; |
5-chloro-2-trichloroacetylaminobenzophenone
3-amino-2-propanol
A
2-Amino-5-chlorobenzophenone
B
9-chloro-2-methyl-10b-phenyl-2,3,6,10b-tetrahydro-5H-oxazolo<3,2-c>quinazolin-5-one
C
6-chloro-3,4-dihydro-3-(2-hydroxypropyl)-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In propan-1-ol for 8h; Heating; | A 28% B 31% C 36% |
2'-Benzoyl-4'-chloro-N-(N-phthaloyl-DL-alanyl)sarcosinanilide
A
2-Amino-5-chlorobenzophenone
B
2'-Benzoyl-4'-chloro-N-(DL-alanyl)sarcosinanilide
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol; chloroform for 15h; Ambient temperature; | A 29% B 36% |
5-chloro-2-trichloroacetylaminobenzophenone
isopropylamine
A
2-Amino-5-chlorobenzophenone
B
1-(2-benzoyl-4-chlorophenyl)-3-isopropylurea
C
6-chloro-3,4-dihydro-3-isopropyl-4-hydroxy-4-phenyl-2(1H)-quinazolinone
D
6-chloro-3,4-dihydro-3-isopropyl-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 5h; | A 5% B 12% C 35% D 7% |
5-chloro-2-trichloroacetylaminobenzophenone
cyclohexylamine
A
5-chloro-2-dichloroacetamidobenzophenone
B
1-(2-benzoyl-4-chlorophenyl)-3-cyclohexylurea
C
2-Amino-5-chlorobenzophenone
D
6-chloro-3-cyclohexyl-3,4-dihydro-4-hydroxy-4-phenyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 7h; Further byproducts given; | A 5% B 31% C 8% D 28% |
5-chloro-2-trichloroacetylaminobenzophenone
cyclohexylamine
A
1-(2-benzoyl-4-chlorophenyl)-3-cyclohexylurea
B
2-Amino-5-chlorobenzophenone
C
6-chloro-3-cyclohexyl-3,4-dihydro-4-hydroxy-4-phenyl-2(1H)-quinazolinone
D
6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 7h; Further byproducts given; | A 31% B 8% C 28% D 3% |
Conditions | Yield |
---|---|
With aluminium trichloride for 5h; Heating; | 31% |
N-(2-benzoyl-4-chlorophenyl)acetamide
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With hydrogenchloride |
N-Benzoyl-2-amino-5-chlorobenzophenone
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With sulfuric acid | |
With sodium hydroxide In methanol for 4h; Heating; | 1.96 g |
2-Amino-5-chlorobenzophenone
allyl bromide
2-Allylamino-5-chlor-benzophenon
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide In tetrahydrofuran at 60℃; for 0.5h; | 100% |
2-Amino-5-chlorobenzophenone
dimethyl sulfate
5-chloro-2-(methylamino)benzophenone
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide In tetrahydrofuran at 60℃; for 1h; | 100% |
With sodium hydroxide; tetrabutylammomium bromide; potassium carbonate In tetrahydrofuran at 30 - 35℃; for 2.5h; | 96% |
Conditions | Yield |
---|---|
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis; | 100% |
With sulfuric acid; silica gel at 100℃; for 2h; Friedlaender synthesis; | 99% |
KAl(SO4)2*12H2O/SiO2 at 30℃; for 1.5h; Friedlaender synthesis; | 99% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 153℃; for 19h; Sealed tube; | 100% |
at 160℃; for 4h; Time; | 93% |
With Amberlite Na sr1L at 115℃; for 0.0666667h; Microwave irradiation; Neat (no solvent); | 92% |
m-bromobenzoic aldehyde
2-Amino-5-chlorobenzophenone
2-(3-bromophenyl)-6-chloro-4-phenylquinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate In ethanol at 60℃; for 1h; | 94% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 0.5h; | 92% |
4-chlorobenzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-2(4-chloro-phenyl)-4-phenyl-quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate In ethanol at 60℃; for 1h; Catalytic behavior; Solvent; Temperature; Time; | 96% |
With ammonium acetate; iodine In neat (no solvent) at 40℃; for 2.5h; Green chemistry; | 95% |
benzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-2,4-diphenyl-quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III); ammonium acetate In neat (no solvent) at 40℃; for 2.5h; Green chemistry; | 95% |
With ammonium acetate In ethanol at 60℃; for 1h; | 95% |
4-methoxy-benzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-2-(4-methoxyphenyl)-4-phenylquinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate In ethanol at 60℃; for 1h; | 95% |
With Maltose; N,N'-Dimethylurea; ammonium acetate; ammonium chloride at 90℃; for 2.5h; | 91% |
salicylaldehyde
2-Amino-5-chlorobenzophenone
2-(6-chloro-4-phenylquinazoline-2-yl)phenol
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III); ammonium acetate In neat (no solvent) at 40℃; for 2.5h; Green chemistry; | 91% |
With ammonium acetate In neat (no solvent) at 60℃; Catalytic behavior; Green chemistry; | 91% |
With Maltose; N,N'-Dimethylurea; ammonium acetate; ammonium chloride at 90℃; for 2.5h; | 88% |
With ammonium acetate; 1-methyl-1H-imidazolium trifluoroacetate at 80℃; for 2h; Ionic liquid; aerobic oxidation; | 87% |
2,4-dichlorobenzaldeyhde
2-Amino-5-chlorobenzophenone
6-chloro-2-(2,4-dichlorophenyl)-4-phenylquinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate; 1-methyl-1H-imidazolium trifluoroacetate at 80℃; for 2h; Ionic liquid; aerobic oxidation; | 92% |
With ammonium acetate In ethanol at 60℃; for 1h; | 90% |
2-Amino-5-chlorobenzophenone
2-nitro-benzaldehyde
6-chloro-2(2-nitro-phenyl)-4-phenyl-quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate; iodine In neat (no solvent) at 40℃; for 2.5h; Green chemistry; | 93% |
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III); ammonium acetate In neat (no solvent) at 40℃; for 2.5h; Green chemistry; | 91% |
4-Trifluoromethylbenzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-4-phenyl-2-(4-(trifluoromethyl)phenyl)quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With Maltose; N,N'-Dimethylurea; ammonium acetate; ammonium chloride at 90℃; for 2.33333h; | 93% |
3-Trifluoromethylbenzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-4-phenyl-2-(3-(trifluoromethyl)phenyl)quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With Maltose; N,N'-Dimethylurea; ammonium acetate; ammonium chloride at 90℃; for 3.33333h; | 91% |
4-methyl-benzaldehyde
2-Amino-5-chlorobenzophenone
6-chloro-4-phenyl-2-(p-tolyl)-quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With ammonium acetate; iodine In neat (no solvent) at 40℃; for 0.5h; Green chemistry; | 97% |
With ammonium acetate In toluene at 110℃; for 4h; Reflux; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1.5h; | 85% |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1h; | 90% |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1.5h; | 86% |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1.5h; | 84% |
3-nitro-benzaldehyde
2-Amino-5-chlorobenzophenone
6-Chloro-2-(3-nitro-phenyl)-4-phenyl-quinazoline
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium acetate In ethanol for 4h; Reflux; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol; ammonium acetate at 55℃; for 1.16667h; | 90% |
2-Amino-5-chlorobenzophenone
(2-amino-5-chlorophenyl)(phenyl)methanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In isopropyl alcohol at 60℃; for 3.5h; | 99% |
With sodium tetrahydroborate In methanol at 50℃; for 1h; | 98% |
With sodium tetrahydroborate In ethanol | 98% |
Conditions | Yield |
---|---|
sulfuric acid for 0.116667h; Friedlaender quinoline synthesis; microwave irradiation; | 99% |
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis; | 99% |
With phosphoric acid triphenyl ester at 130℃; for 4h; | 97% |
2-Amino-5-chlorobenzophenone
acetylacetone
1-(6-chloro-2-methyl-4-phenylquinolin-3-yl)ethanone
Conditions | Yield |
---|---|
With sulfuric acid; silica gel at 100℃; for 0.75h; Friedlaender synthesis; | 99% |
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis; | 99% |
With tin(ll) chloride at 20℃; for 0.5h; | 98% |
2-Amino-5-chlorobenzophenone
trifluoroacetic anhydride
N-(2-benzoyl-4-chlorophenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 12h; | 99% |
With triethylamine In dichloromethane at -78 - 20℃; for 0.166667h; |
cyclohexanone
2-Amino-5-chlorobenzophenone
6-chloro-10-phenyl-1,2,3,4-tetrahydroacridine
Conditions | Yield |
---|---|
With CuBTC metal-organic-framework at 89.84℃; for 5h; Friedlaender reaction; Neat (no solvent); | 99% |
With 1-butylimidazolium tetrafluoroborate at 100℃; for 3h; Friedlaender reaction; | 98% |
With tin(ll) chloride at 20℃; for 2.33333h; | 96% |
ethyl acetoacetate
2-Amino-5-chlorobenzophenone
ethyl 6-chloro-2-methyl-4-phenylquinoline-3-carboxylate
Conditions | Yield |
---|---|
With magnesium(II) perchlorate In ethanol at 60℃; for 18h; Friedlaender synthesis; | 99% |
scandium tris(dodecyl sulfate) In water at 40℃; Friedlaender annulation; | 99% |
With cuprous triflate at 20℃; for 2h; Friedlaender synthesis; neat (no solvent); | 99% |
2-Amino-5-chlorobenzophenone
dimethyl acetylenedicarboxylate
dimethyl 4-phenyl-6-chloroquinoline-2,3-dicarboxylate
Conditions | Yield |
---|---|
With propylphosphonium tetrachloroindate ionic liquid supported on nanosilica In neat (no solvent) at 110℃; for 0.5h; Reagent/catalyst; Temperature; | 99% |
With indium(III) chloride at 80℃; for 0.833333h; regioselective reaction; | 96% |
Stage #1: dimethyl acetylenedicarboxylate With pyridine at 0 - 10℃; for 0.25h; Stage #2: 5-chloro-2-aminobenzophenone at 20℃; for 12h; | 89% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; iodine In ISOPROPYLAMIDE; water at 80℃; for 4h; Sealed tube; | 99% |
2-Amino-5-chlorobenzophenone
diphenyl acetylene
6-chloro-2,3,4-triphenylquinoline
Conditions | Yield |
---|---|
With 18-crown-6 ether; trifluorormethanesulfonic acid; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane In toluene; acetonitrile at 100℃; for 12h; Reagent/catalyst; Solvent; Sealed tube; | 98.1% |
With propylphosphonium tetrachloroindate ionic liquid supported on nanosilica In neat (no solvent) at 110℃; for 1h; | 67% |
With acetic acid; palladium(II) bromide In benzonitrile; 1,2-dichloro-ethane at 130℃; for 18h; Sealed tube; | 51% |
Conditions | Yield |
---|---|
In pyridine; hydrogenchloride | 98% |
39% |
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