CAS No.108-47-4,2,4-Lutidine Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

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Chemwill Asia Co., Ltd.

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Hebei yanxi chemical co.,LTD.

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Henan Tianfu Chemical Co., Ltd.

Henan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com

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Henan Sinotech Import&Export Corporation

Name 2,4-Lutidine CAS 108-47-4 MF C7H9N

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

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Hangzhou Lingrui Chemical Co.,Ltd.

108-47-4 C7H9N 2,4-LutidineAppearance:white powder Storage:Normal temperature Package:according to customers' requirements Application:Organics;Heterocyclic Compounds;Biochemistry;Reagents for Oligosaccharide Synthesis;Buildi

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HANGZHOU YUNUO CHEMICAL CO.,LTD

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Siwei Development Group Ltd.

Product name: 2,4-Lutidine CAS No.：108-47-4 Molecule Formula：C7H9N Molecule Weight：107.15 Purity: 99.0% Package: 25kg/drum Description：Yellowish-brown liquid Manufacture Standards：Enterprise Standard TESTING ITEMS

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)

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Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

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Hunan chemfish Pharmaceutical co.,Ltd

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SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

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Kono Chem Co.,Ltd

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Hangzhou Dingyan Chem Co., Ltd

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Henan Allgreen Chemical Co.,Ltd

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

108-47-4 Application:108-47-4

2,4-dimethylpyridine

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Changzhou Ansciep Chemical Co.,Ltd.

reagent grade ex stockAppearance:white or off-white crystalline powder Storage:Keep away of light，cool place Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:by Fedex, ship or plane

2,4-Dimethylpyridine

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

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Chemsigma International Co.,Ltd.

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Qingdao little fox Biological &Technology Co.,Ltd

108-47-4 C7H9N 2,4-LutidineAppearance:white powder Storage:Normal temperature Package:Woven bag Application:Organics;Heterocyclic Compounds;Biochemistry;Reagents for Oligosaccharide Synthesis;Building Blocks;C7;Chemical Synth

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Tocopharm Co., Ltd.

Product Name: 2,4-Lutidine Cas No: 108-47-4 Synonyms: 2,4-dimethyl-pyridin ;2,4-Lutidene;alpha,gamma-Dimethylpyridine;Pyridine,2,4-dimethyl- ;α,γ-dimethylpyridine ;2,4-DIMETHYLPYRIDINE;24L;2,4-LUTIDINE Structural Formula: 2

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Amadis Chemical Co., Ltd.

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HENAN SUNLAKE ENTERPRISE CORPORATION

2,4-Lutidine Basic information Product Name: 2,4-Lutidine S

108-47-4 C7H9N 2,4-Lutidine

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Changzhou Xuanming Chemical Co., Ltd.

Changzhou Xuanming Chemical Co., Ltd. is dedicated to the technology development, manufacturing, import and export chemicals, which are specialized in pharmaceutical intermediates, pesticide intermediate, industry of fine chemicals and custom synth

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Shaanxi Mingqi Chemical Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer a

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Synthetic route

: 1122-45-8
2,4-dimethylpyridine N-oxide

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With bis(triphenyl)oxodiphosphonium trifluoromethanesulfonate salt; potassium iodide In ethanol at 20℃; for 1.16667h;	93%
Multi-step reaction with 2 steps 1: 71 percent / CH2Cl2 / 1.5 h 2: aq. ammonium persulfate / 1 h / Heating View Scheme

: 108-89-4
picoline

: 71-23-8
propan-1-ol

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With Raney nickel at 180℃; for 0.5h; Concentration; Flow reactor; Green chemistry; regioselective reaction;	87%

: 41438-38-4
diethyl pyridine-2,4-dicarboxylate

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With sulfuric acid; titanium(IV) oxide at 20 - 30℃; for 10h; Electrochemical reaction;	75%

: 67-64-1
acetone

: 74-86-2
acetylene

A: 109-06-8
α-picoline

B: 108-48-5
2,6-dimethylpyridine

C: 108-75-8
2,4,6-trimethyl-pyridine

D: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With ammonia; MG-4 at 375℃; under 760 Torr;	A 6.3% B 7.3% C 58.3% D 5.9%
With ammonia; MG-4 at 375℃; under 760 Torr; Product distribution; other catalysts;	A 6.3% B 7.3% C 58.3% D 5.9%
With ammonia; MG-4 at 350℃; under 760 Torr;	A 6.2% B 15.6% C 36.4% D 6.8%

...Expand

: 108-89-4
picoline

A: 110-86-1
pyridine

B: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With hydrogen; aluminum oxide; nickel at 330℃; under 750.06 Torr; Product distribution;	A 0.6% B 35.2%

: 20451-53-0
Phenyl vinyl sulfoxide

: 77202-09-6
4,6-dimethyl-1,2,3-triazine

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
at 180℃; for 1h;	35%

: 20451-53-0
Phenyl vinyl sulfoxide

: 77202-09-6
4,6-dimethyl-1,2,3-triazine

A: 108-48-5
2,6-dimethylpyridine

B: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
at 180℃; 1-2.5 h;	A n/a B 35%

...Expand

: 50-00-0
formaldehyd

: 67-64-1
acetone

A: 1122-39-0
2,4,5-trimethylpyridine

B: 2233-29-6
2,3,4-lutidine

C: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With diammonium phosphate In ethanol; water at 234℃; for 1.08333h;	A 8.5% B 35% C 6%

...Expand

: 50-00-0
formaldehyd

: 67-64-1
acetone

A: 1122-39-0
2,4,5-trimethylpyridine

B: 108-47-4
2,4-lutidine

C: 2-ethyl-3,5-dimethylcyclopent-2-enone

Conditions

Conditions	Yield
With diammonium phosphate In ethanol; water at 234℃; for 1.08333h;	A 8.5% B 6% C 35%

...Expand

: 108-99-6
3-Methylpyridine

A: 110-86-1
pyridine

B: 109-06-8
α-picoline

C: 583-61-9
2,3-Lutidine

D: 108-47-4
2,4-lutidine

E: 589-93-5
2,5-dimethylpyridine

Conditions

Conditions	Yield
With hydrogen; aluminum oxide; nickel at 330℃; under 750.06 Torr; Product distribution;	A 0.3% B 0.5% C 5.3% D 8% E 30.9%

...Expand

: 109-06-8
α-picoline

: 67-56-1
methanol

A: 100-69-6
2-vinylpyridine

B: 108-48-5
2,6-dimethylpyridine

C: 100-71-0
2-Ethylpyridine

D: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
Cs exchanged zeolite at 450℃; Product distribution; investigation of the heterogeneous vapor-phase alkylation of α-picoline with methanol over Na+, K+, Rb+, or Cs+ exchanged X- or Y-type zeolite in an atmosphere of nitrogen;	A 3.1% B 7.3% C 30.2% D 3.6%

...Expand

: 108-89-4
picoline

: 67-56-1
methanol

A: 100-43-6
4-vinylpyridine

B: 536-75-4
4-Ethylpyridine

C: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
Cs exchanged zeolite at 450℃; Product distribution; investigation of the heterogeneous vapor-phase alkylation of γ-picoline with methanol over Na+, K+, Rb+, or Cs+ exchanged X- or Y-type zeolite in an atmosphere of nitrogen;	A 3.7% B 27.1% C 13.8%

...Expand

: 108-89-4
picoline

: 67-56-1
methanol

A: 536-75-4
4-Ethylpyridine

B: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
ammonium chloride at 335℃; for 12h;	A 25.5% B 9.5%
ammonium chloride at 335℃; for 12h; Product distribution; variation of reaction temperature, duration of heating, catalysts;	A 25.5% B 9.5%

...Expand

: 764-01-2
methyl propargyl alcohol

: 141-43-5
ethanolamine

A: 109-06-8
α-picoline

B: 108-75-8
2,4,6-trimethyl-pyridine

C: 108-47-4
2,4-lutidine

D: 75-05-8
acetonitrile

Conditions

Conditions	Yield
With aluminum(III) fluoride; aluminum oxide; chromium(III) oxide; zinc at 420℃; Further byproducts given;	A 14.4% B 13.3% C 23.9% D 21.2%

...Expand

: 764-01-2
methyl propargyl alcohol

: 141-43-5
ethanolamine

A: 108-89-4
picoline

B: 108-75-8
2,4,6-trimethyl-pyridine

C: 108-47-4
2,4-lutidine

D: 75-05-8
acetonitrile

Conditions

Conditions	Yield
With aluminum(III) fluoride; aluminum oxide; chromium(III) oxide; zinc at 420℃; Further byproducts given;	A 18.2% B 13.3% C 23.9% D 21.2%

...Expand

: 660867-80-1
2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 74-88-4
methyl iodide

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With C21H30ClNPPd; potassium tert-butylate In tert-Amyl alcohol at 65℃; for 18h; Sealed tube; Inert atmosphere; Glovebox;	21%

: 764-01-2
methyl propargyl alcohol

: 75-07-0
acetaldehyde

A: 109-06-8
α-picoline

B: 108-89-4
picoline

C: 108-75-8
2,4,6-trimethyl-pyridine

D: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With aluminum(III) fluoride; aluminum oxide; chromium(III) oxide; ammonia; zinc at 340℃; Further byproducts given;	A 15.8% B 5.5% C 1.5% D 7.7%

...Expand

: 108-89-4
picoline

: 67-56-1
methanol

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
nickel(II) nitrate for 8h; Ambient temperature; Irradiation;	11.5%
nickel(II) nitrate for 8h; Product distribution; Ambient temperature; Irradiation; Variation of reaction time and amount of catalyst and methanol;	11.5%
BaY; cation-exchanged zeolite at 400℃;	12.8 % Chromat.

: 30838-93-8
2-chloro-4,6-dimethyl-pyridine

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
bei der Zinkstaub-Destillation;

: 18088-10-3
4,6-dimethylpyridine-2-carboxylic acid

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With calcium oxide

: 2,4-dimethyl-pyridine-3,5-dicarboxylic acid

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
beim Destillieren;

: 690-94-8
dimethyl(vinylethynyl)carbinol

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With aluminum oxide; ammonia; cadmium(II) oxide at 360℃;
With chromium oxide-aluminium oxide-manganese oxide catalyst; ammonia at 420℃;

: 75-07-0
acetaldehyde

: 67-64-1
acetone

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With aluminum oxide; ammonia at 350℃;

: 75-05-8
acetonitrile

: 78-79-5
isoprene

: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
With aluminum oxide at 420℃;

: 110-86-1
pyridine

: 67-56-1
methanol

A: 109-06-8
α-picoline

B: 108-89-4
picoline

C: 108-48-5
2,6-dimethylpyridine

D: 108-99-6
3-Methylpyridine

E: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
BaY; cation-exchanged zeolite at 400℃; Product distribution; various H and alkaline or alkaline earth cation-exchanged X or Y type zeolite catalysts;	A 22.7 % Chromat. B 7.6 % Chromat. C 10.7 % Chromat. D 3.8 % Chromat. E 10.7 % Chromat.

...Expand

: 110-86-1
pyridine

: 67-56-1
methanol

A: 109-06-8
α-picoline

B: 108-89-4
picoline

C: 108-48-5
2,6-dimethylpyridine

D: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
BaY; cation-exchanged zeolite at 400℃; Further byproducts given;	A 22.7 % Chromat. B 7.6 % Chromat. C 10.7 % Chromat. D 10.7 % Chromat.
SrY; cation-exchanged zeolite at 400℃; Further byproducts given;	A 22.3 % Chromat. B 7.4 % Chromat. C 10.9 % Chromat. D 10.8 % Chromat.

...Expand

: 110-86-1
pyridine

: 67-56-1
methanol

A: 109-06-8
α-picoline

B: 108-89-4
picoline

C: 108-47-4
2,4-lutidine

D: 589-93-5
2,5-dimethylpyridine

Conditions

Conditions	Yield
SrY; cation-exchanged zeolite at 400℃;	A 22.3 % Chromat. B 7.4 % Chromat. C 10.8 % Chromat. D 10.9 % Chromat.

...Expand

: 109-06-8
α-picoline

: 67-56-1
methanol

A: 108-48-5
2,6-dimethylpyridine

B: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
cation-exchanged zeolite at 400℃;	A 8.8 % Chromat. B 5.2 % Chromat.

...Expand

: 109-06-8
α-picoline

: 67-56-1
methanol

A: 108-48-5
2,6-dimethylpyridine

B: 108-47-4
2,4-lutidine

C: 589-93-5
2,5-dimethylpyridine

Conditions

Conditions	Yield
cation-exchanged zeolite at 400℃; Product distribution; H and various alkaline or alkaline earth cation-exchanged Y type zeolite catalysts;

...Expand

: 108-89-4
picoline

: 67-56-1
methanol

A: 583-58-4
3,4-Lutidin

B: 108-47-4
2,4-lutidine

Conditions

Conditions	Yield
BaY; cation-exchanged zeolite at 400℃; Product distribution; H and various alkaline or alkaline earth cation-exchanged Y type zeolite catalysts;

...Expand

: 108-47-4
2,4-lutidine

: 1122-45-8
2,4-dimethylpyridine N-oxide

Conditions

Conditions	Yield
With 3-chloro-benzenecarboperoxoic acid In chloroform at 20℃; for 3h;	100%
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; Inert atmosphere;	100%
With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; acetonitrile In tert-butyl alcohol at 20℃; for 18h; Green chemistry; chemoselective reaction;	99%

: cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate

: 108-47-4
2,4-lutidine

: (C5H5)Ru((CH3)2C5NH3)(CH3CN)2(1+)*PF6(1-)={(C5H5)Ru((CH3)2C5NH3)(CH3CN)2}PF6

Conditions

Conditions	Yield
In dichloromethane 5 min, room temp.; adding Et2O, crystn. (-30°C); elem. anal.;	100%
In dichloromethane (Ar); reacted for 5 min with vigorous stirring; added diethyl ether; cooled to -30°C overnight; filtered; washed with diethyl ether; dried in vacuo;	100%

: tert-butyl (cyclohex-2-en-1-yl)carbonate

: 108-47-4
2,4-lutidine

: 1062229-34-8
(S)-2-(cyclohex-2-enylmethyl)-4-methylpyridine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In 1,4-dioxane for 0.5h; Inert atmosphere; Stage #2: tert-butyl (cyclohex-2-en-1-yl)carbonate With (η-C3H5-PdCl)2; (R,R)-ANDEN-phenyl Trost ligand; lithium hexamethyldisilazane In tetrahydrofuran; 1,4-dioxane for 10h; Inert atmosphere; optical yield given as %ee; enantioselective reaction;	100%

: 108-47-4
2,4-lutidine

: [Mo(N(2,6-diisopropylphenyl))(CHCMe2Ph)(2,5-dimethylpyrrolide)(tetrahydrofuran)2][B(3,5-(CF3)2C6H3)4]

: [Mo(N(2,6-diisopropylphenyl))(CHCMe2Ph)(η5-2,5-dimethylpyrrolide)(2,4-dimethylpyridine)][B(3,5-(CF3)2C6H3)4]

Conditions

Conditions	Yield
In dichloromethane byproducts: tetrahydrofuran; (N2); using Schlenk techniques; dissolving of Mo(N(2,6-diisopropylphenyl))(CHCMe2Ph)(2,5-dimethylpyrrolide)(THF)2(B(3,5-(CF3)2C6H3)4) in CH2Cl2;addn. of 2,4-dimethylpyridine (1.18 equiv.) via syringe; stirring at ro om temp. for 10 min; removal of volatiles in vac., addn. of pentane; stirring for 10 min; removal of volatiles in vac., drying in vac. for 2 h, elem. anal.;	99%

Yield

In dichloromethane byproducts: tetrahydrofuran; (N2); using Schlenk techniques; dissolving of Mo(N(2,6-diisopropylphenyl))(CHCMe2Ph)(2,5-dimethylpyrrolide)(THF)2(B(3,5-(CF3)2C6H3)4) in CH2Cl2;addn. of 2,4-dimethylpyridine (1.18 equiv.) via syringe; stirring at ro om temp. for 10 min; removal of volatiles in vac., addn. of pentane; stirring for 10 min; removal of volatiles in vac., drying in vac. for 2 h, elem. anal.;

99%

: 108-47-4
2,4-lutidine

: 256952-82-6
[(CH2Me2SiN(o-C6H4))2O]Zr(NMe2)2(dimethylamine)

: 256952-85-9
[(CH2Me2SiN(o-C6H4))2O]Zr(NMe2)2(2,4-lutidine)

Conditions

Conditions	Yield
In diethyl ether N2-atmosphere; excess of lutidine, stirring at room temp. for 6.5 h; removal of volatiles (vac.); elem. anal.;	98%

: 108-47-4
2,4-lutidine

: 66107-29-7
4-methoxyphenyl triflate

: 1334723-76-0
4-(4-methoxybenzyl)-2-methylpyridine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #3: 4-methoxyphenyl triflate With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;	98%

Yield

Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere;
Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #3: 4-methoxyphenyl triflate With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;

98%

: 108-47-4
2,4-lutidine

: 7646-85-7
zinc(II) chloride

: 14551-53-2
dichloro-bis(2,4-lutidine)-zinc

Conditions

Conditions	Yield
In methanol ZnCl2 and 2,4-lutidine dissolved in MeOH by heating; soln. cooled to ambient temp. and crystals formed within 15 min; XRD and IR spectrocopy;	97%
In acetone ZnCl2 and 2,4-lutidine dissolved in acetone by heating; soln. cooled to ambient temp. and crystals formed within 1 h; XRD and IR spectrocopy;	57%
In acetonitrile ZnCl2 and 2,4-lutidine dissolved in MeCN by heating; soln. cooled to ambient temp. and crystals formed over night; XRD and IR spectrocopy;	54%
In ethyl acetate ZnCl2 and 2,4-lutidine dissolved in ethyl acetate by heating; clear soln. transferred to new vessel and cooled to ambient temp. and crystals formed over night; XRD and IR spectrocopy;	53%

: 108-47-4
2,4-lutidine

: [(1,3-bis-(2,6-diisopropylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene)PdCl(μ-Cl)]2

: C34H45Cl2N3Pd

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 1h; Inert atmosphere;	96%

: 108-47-4
2,4-lutidine

: 544-77-4
1-iodohexadecane

: 78191-89-6
1-Hexadecyl-2,4-dimethyl-pyridinium; iodide

Conditions

Conditions	Yield
In acetic acid for 2h; Heating;	95%

: 108-47-4
2,4-lutidine

: 100-52-7
benzaldehyde

: 2-(2-methyl(4-pyridyl))-1-phenylethan-1-ol

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With lithium diethylamide In tetrahydrofuran; hexane at -50℃; for 0.166667h; Stage #2: benzaldehyde In tetrahydrofuran; hexane at -78℃; for 0.333333h; Further stages.;	95%
With N-ethyl-N,N-diisopropylamine; 9-BBN triflate 1) CH2Cl2, 2) CH2Cl2, RT; var. reag.: n-BuOTf and Et3N; Yield given. Multistep reaction;
With N-ethyl-N,N-diisopropylamine; 9-BBN triflate 1.) -78 deg C, 2.) CH2Cl2, RT, 17 h; Yield given. Multistep reaction;

: 108-47-4
2,4-lutidine

: 70-11-1
α-bromoacetophenone

: 26557-56-2
7-methyl-2-phenylindolicine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine; α-bromoacetophenone In acetone at 90℃; for 72h; Inert atmosphere; Stage #2: With potassium carbonate In water at 80℃; Inert atmosphere;	93%
Multi-step reaction with 2 steps 1: acetonitrile / Reflux 2: potassium carbonate / water View Scheme
Stage #1: 2,4-lutidine; α-bromoacetophenone In acetone at 60℃; for 5h; Stage #2: With potassium carbonate In water at 60℃;
Stage #1: 2,4-lutidine; α-bromoacetophenone In acetone at 60℃; for 5h; Stage #2: With potassium carbonate In water at 60℃; for 5h;

: 592-41-6
1-hexene

: 108-47-4
2,4-lutidine

: C13H21N

Conditions

Conditions	Yield
With triphenylcarbenium tetra(pentafluorophenyl)borate; C63H83N2O2ScSi2 In toluene at 40℃; for 72h; Schlenk technique; Inert atmosphere; enantioselective reaction;	93%

: 104-92-7
1-bromo-4-methoxy-benzene

: 108-47-4
2,4-lutidine

: 1334723-76-0
4-(4-methoxybenzyl)-2-methylpyridine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #3: 1-bromo-4-methoxy-benzene With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;	92%

Yield

Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere;
Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #3: 1-bromo-4-methoxy-benzene With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;

92%

: 108-47-4
2,4-lutidine

: 578-57-4
2-bromoanisole

: 1334723-78-2
4-(2-methoxybenzyl)-2-methylpyridine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #3: 2-bromoanisole With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;	92%

Yield

Stage #1: 2,4-lutidine With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere;
Stage #2: With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #3: 2-bromoanisole With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 50℃; for 2h; Inert atmosphere;

92%

: 292638-84-7
styrene

: 108-47-4
2,4-lutidine

: 79560-51-3
(phenyl-2' ethyl)-2 dimethyl-4,6 pyridine

Conditions

Conditions	Yield
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 7h; Inert atmosphere; Schlenk technique; Glovebox;	92%

: 108-47-4
2,4-lutidine

: nickel dichloride

: 24884-44-4
{NiCl2(α.γ-(CH3)2C5H3N)2}

Conditions

Conditions	Yield
In neat (no solvent) under N2; anhyd. NiCl2 suspended in 2,4-lutidine (neat); heated to 80°C for ca. 7 min; adapted from S. Buffagni, L. M. Vallarino, J. V. Quagliano, Inorg. Chem., 3 (1964) 480; soln. filtered hot through Celite; crystd.; crystals collected; wahsed with pentane;	91.8%
In ethanol mixing satd. soln. of H2O-free NiCl2 in ethanol with soln. of α.γ-lutidine in ethanol (excess);; washing with ether and drying in vac.;;
In neat (no solvent) heating NiCl2 for several hours with α.γ-lutidine, extg. with CH2Cl2 (several times), pptg. with ether;; recrystn. from α.γ-lutidine;;
In neat (no solvent) heating NiCl2 for several hours with α.γ-lutidine, extg. with CH2Cl2 (several times), pptg. with ether;; recrystn. from α.γ-lutidine;;
In ethanol mixing satd. soln. of H2O-free NiCl2 in ethanol with soln. of α.γ-lutidine in ethanol (excess);; washing with ether and drying in vac.;;

: 108-47-4
2,4-lutidine

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: dimethyl-[2-(2-methylpyridin-4-yl)vinyl]amine

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With n-butyllithium In tetrahydrofuran at -70 - -50℃; for 0.75h; Stage #2: With diethylamine In tetrahydrofuran for 0.5h; Stage #3: N,N-dimethyl-formamide In tetrahydrofuran for 1h;	91%
Stage #1: 2,4-lutidine With n-butyllithium; diethylamine In tetrahydrofuran; hexane at -50℃; for 0.416667h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexane at -50℃; for 1.16667h;

: 21384-43-0
1-(3-methylbenzoyl)-2-methylaziridine

: 108-47-4
2,4-lutidine

: 325770-44-3
1-(3-methylphenyl)-2-(2-methyl-4-pyridyl)ethanone

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine With lithium diisopropyl amide In tetrahydrofuran; hexane at -10℃; for 1h; Stage #2: 1-(3-methylbenzoyl)-2-methylaziridine In tetrahydrofuran; hexane at -78℃; for 2h;	91%

: 960604-20-0
1,3-bis-(5-bromo-pent-1-ynyl)-benzene

: 108-47-4
2,4-lutidine

: 1,3-bis-[5-(2,4-dimethyl-pyridinium)-pent-1-ynyl]-benzene dibromide

Conditions

Conditions	Yield
In water	91%
at 60 - 70℃; for 12h;	91%

: n-butyllithium hexane

: 21384-43-0
1-(3-methylbenzoyl)-2-methylaziridine

: 108-47-4
2,4-lutidine

: 325770-44-3
1-(3-methylphenyl)-2-(2-methyl-4-pyridyl)ethanone

Conditions

Conditions	Yield
With diisopropylamine In tetrahydrofuran; water	91%
With diisopropylamine In tetrahydrofuran; water	91%

...Expand

: 108-47-4
2,4-lutidine

: 17431-39-9, 131214-20-5, 13156-74-6
N,N-dimethyl-3-phenylacrylamide

: N,N-dimethyl-4-(2-methylpyridin-4-yl)-3-phenylbutanamide

Conditions

Conditions	Yield
With 18-crown-6 ether; potassium hexamethylsilazane In tetrahydrofuran at 0℃; for 18h; Inert atmosphere;	91%

: 108-47-4
2,4-lutidine

A: 4021-11-8
2-methylisonicotinic acid

B: 4021-08-3
4-methylpicolinic acid

Conditions

Conditions	Yield
at 30℃; for 16h; Pseudomonas putida ATCC 33015;	A 90% B 10%

: zinc trimethylacetate

: 108-47-4
2,4-lutidine

: 1307746-79-7
[zinc(II)(μ2-κ1O:κ1O'-O2C(t-Bu))2(2,4-lutidine)]2

Conditions

Conditions	Yield
In methanol soln. of C5H3NMe2 in MeOH added to soln. of Zn salt in MeOH, stirred at room temp. for 12 h; volatiles removed under vac., crystd. from MeOH at room temp. for 3 d; elem. anal.;	90%

: 108-47-4
2,4-lutidine

: 77287-34-4, 77287-35-5, 60100-09-6
formamide

: 72693-02-8
4,6-dimethylpicolinamide

Conditions

Conditions	Yield
With dipotassium peroxodisulfate; oxygen; sodium formate; silver nitrate In water at 80℃; for 4h; Schlenk technique; regioselective reaction;	90%
With dipotassium peroxodisulfate; oxygen; silver(I) acetate; sodium acetate In water at 80℃; for 4h; Green chemistry;	90%

: 108-47-4
2,4-lutidine

: 592-42-7
1,5-Hexadien

: C13H19N

Conditions

Conditions	Yield
With tris(pentafluorophenyl)borate; C42H51N3PSc In chlorobenzene at 100℃; for 10h; diastereoselective reaction;	90%

: 108-47-4
2,4-lutidine

: 105-36-2
ethyl bromoacetate

: 95047-62-4
1-(2-ethoxy-2-oxoethyl)-2,4-dimethylpyridin-1-ium bromide

Conditions

Conditions	Yield
In acetone for 72h; Ambient temperature;	89%
In ethyl acetate for 20h;	75%

: 108-47-4
2,4-lutidine

: 105-36-2
ethyl bromoacetate

: 1-carboxymethyl-2,4-dimethyl-pyridinium; bromide

Conditions

Conditions	Yield
Stage #1: 2,4-lutidine; ethyl bromoacetate With tetra-(n-butyl)ammonium iodide In toluene Heating; Stage #2: With hydrogen bromide at 100℃; for 1h;	89%

: 108-47-4
2,4-lutidine

: trimethylamine-iodoborane

: bis(2.4-lutidine)boronium iodide

Conditions

Conditions	Yield
In not given	89%

: 108-47-4
2,4-lutidine

: [1,3-bis(2,6-dimethylphenyl)-4,5-dihydroimidazol-2-ylidene]ruthenium(II)Cl2(benzylidene)PPh3

: [RuCl2(=CHPh)(1,3-bis(2,6-dimethylphenyl)-4,5-dihydroimidazol-2-ylidene)(2,4-dimethylpyride)]

Conditions

Conditions	Yield
In further solvent(s) byproducts: PPh3; 2,4-dimethylpyridine (17.2 mmol) added to Ru complex (0.17 mmol) in Schlenk flask; stirred (room temp., 2 h); hexane added (room temp.); ppt. filtered; washed with hexane; dried (vac., 6 h);	89%

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