SICHUAN ZHONGBANG NEW MATERIAL CO., LTD
Appearance:white crystalline powder Storage:Stored in closed containers in dry cool conditions. Package:25kg/bag, Application:API Transportation:by air, by sea, by express
Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:281-23-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:281-23-2
Min.Order:0 Metric Ton
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Type:Manufacturers
inquiryJinan Finer Chemical Co., Ltd
Product description: Product name Adamantane CAS number 281-23-2 Assay ≥99% Appearance White crystalline powder Capacity 500mt/year Application Pharmaceutical intermediates,
LIDE PHARMACEUTICALS LIMITED
LIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:281-23-2
Min.Order:1 Kilogram
FOB Price: $0.9 / 1.0
Type:Lab/Research institutions
inquiryWuhan Fortuna Chemical Co.,Ltd
Unique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White to off-white powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:as intermediates Trans
Cas:281-23-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou Dingyan Chem Co., Ltd
Items Standard Result Appearance White crystalline powder Complies Assay 99.0%min
Cas:281-23-2
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Xi'an Xszo Chem Co., Ltd.
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:281-23-2
Min.Order:1 Gram
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inquiryCOLORCOM LTD.
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
TIANFUCHEM--281-23-2--Adamantane in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationships wit
Cas:281-23-2
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryLeader Biochemical Group
About Product Details Item Specification Test Results Appearance White crystalline powder Conform
Cas:281-23-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 5.0
Type:Lab/Research institutions
inquiryHebei Nengqian Chemical Import and Export Co., LTD
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Zhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:281-23-2
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHubei Langyou International Trading Co., Ltd
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White powder Storage:Store in sealed containers at cool & dr
Hangzhou Sartort Biopharma Co., Ltd
Appearance:White crystal Storage:Room temperature Package:25kg/drum Application:Pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:281-23-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryShanghai Upbio Tech Co.,Ltd
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:281-23-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryXi'an Faithful Biotech Co., Ltd.
We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:281-23-2
Min.Order:10 Gram
FOB Price: $3.5
Type:Trading Company
inquiryBaoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Qingdao Beluga Import and Export Co., LTD
Adamantane CAS:281-23-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, s
Cas:281-23-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Wuhan Wonda Pharm Limited
1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products wi
Cas:281-23-2
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Purestar Chem Enterprise Co.,Ltd
【Chemical Name】Adamantane 【Synonym】Tricyclo[3.3.1.1(3,7)]decane 【CAS No】281-23-2 【Molecular Formula】C10H16 【Molecular Weight】136.26 【Structural Formula】 【Properties】White crystalline powder; Density: 1.07g/cm3(20/20 deg C); Melting Point: 266.00 -
Xiamen Hisunny Chemical Co.,Ltd
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Triumph International Development Limilted
Appearance:White or off-white Solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Se
Afine Chemicals Limited
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:281-23-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 100000.0
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inquiryWuhan Han Sheng New Material Technology Co.，Ltd
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Synthetic route
| Conditions | Yield |
|---|---|
| With triethylsilane; dilauryl peroxide; 1-dodecylthiol at 70℃; for 1h; | 100% |
| With triethylsilane; dilauryl peroxide; 1-dodecylthiol In cyclohexane at 80℃; for 1h; | 100% |
| With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); cPS-SnBu2Cl In 1,2-dimethoxyethane at 80℃; for 0.5h; | 100% |
-
-
22110-53-8
1-adamantyl isocyanide
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With Perbenzoic acid; diphenylsilane In 1,4-dioxane for 1h; Heating; | 100% |
-
-
75480-69-2
1-(phenylseleno)tricyclo<3.3.1.13,7>decane
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile); 1,1,2,2-tetraphenyldisilane In ethyl acetate for 14h; Reduction; Heating; | 100% |
| With Perbenzoic acid; methyl phosphite In 1,4-dioxane for 5h; Heating; | 41 % Chromat. |
-
-
79057-62-8
O-(adamantan-1-yl) S-methyl carbonodithioate
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With sodium formate; (Bu4N)2S2O8 In N,N-dimethyl-formamide at 75℃; for 0.5h; Barton-McCombie deoxygenation; | 100% |
| With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane In toluene at 130℃; for 0.0833333h; Barton-McCombie deoxygenation; | 77% |
| With 1-ethyl-piperidine; 2,2'-azobis(isobutyronitrile); hypophosphorous acid In 1,4-dioxane for 1h; | 100 % Chromat. |
| With dibutylphosphine oxide; 1,1'-azobis(1-cyanocyclohexanenitrile) In 1,4-dioxane for 8h; Heating; | 90 % Chromat. |
| Conditions | Yield |
|---|---|
| With triisopropylborane; trifluorormethanesulfonic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane 1.) -30 deg C, 30 min 2.) room temp., 6 h; | A 99.9% B 0.1% |
| Conditions | Yield |
|---|---|
| With hydrogen; aluminum oxide; nickel at 180℃; | 99% |
| With indium(III) chloride; diphenylsilyl chloride In 1,2-dichloro-ethane at 80℃; for 3h; | 99% |
| With boron trifluoride diethyl etherate In water for 2h; Inert atmosphere; Reflux; | 29% |
| Conditions | Yield |
|---|---|
| With hydrogen; aluminum oxide; nickel at 170℃; | 99% |
| Multi-step reaction with 2 steps 1: 81 percent / NaI; HI / 48 h / 90 - 100 °C 2: 35 percent Chromat. / t-BuOK / dimethylsulfoxide / 3 h / Irradiation View Scheme | |
| Multi-step reaction with 2 steps 1: 81 percent / NaI; HI / 48 h / 90 - 100 °C 2: 20 percent Chromat. / t-BuOK / dimethylsulfoxide / 3 h / Irradiation View Scheme |
| Conditions | Yield |
|---|---|
| With tris(trifluoromethanesulfonyloxy)boron In 1,1,2-Trichloro-1,2,2-trifluoroethane at 0 - 20℃; for 0.5h; | 98% |
| With tris(trifluoromethanesulfonyloxy)boron In 1,1,2-Trichloro-1,2,2-trifluoroethane at 0 - 20℃; for 0.5h; Product distribution; sonication, other C(4n+6)H(4n+12), (n=1-3), other polycyclic hydrocarbon, other reactants, reaction condition; | 98% |
| With aluminium trichloride at 150 - 180℃; | |
| Mechanism; application of the "prinzip of minimal chemical distance"; |
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile); (C6F13CH2CH2)3SnH; sodium cyanoborohydride In tert-butyl alcohol at 90℃; for 3h; | 98% |
| With air; tributyl borane; water In benzene at 20℃; | 97% |
| With 1,3-bis(2,6-diiopropylphenyl)imidazol-2-ylidene borane In 1,2,3-trifluorobenzene at 140℃; for 12h; | 97% |
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile); tributyltin chloride; sodium cyanoborohydride; oxygen-18 In tert-butyl alcohol at 60℃; for 16h; Yields of byproduct given; | A n/a B 98% |
| Conditions | Yield |
|---|---|
| With hydrogen; aluminum oxide; nickel at 235℃; under 760 Torr; for 4h; | 97% |
-
-
6707-86-4, 62928-75-0
Octahydro-1,2,4-metheno-1H-cyclobutapentalene
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; trifluorormethanesulfonic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane at -78 - 20℃; for 18h; | 97% |
-
-
22635-62-7
1-acetyloxyadamantane
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With hafnium(IV) trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen In neat (no solvent) at 125℃; under 750.075 Torr; for 18h; Time; | 97% |
| With di-tert-butyl peroxide; (4-diphenylsilylphenyl)diphenylsilane at 140℃; for 15h; | 85% |
| Conditions | Yield |
|---|---|
| With sulfuric acid In ethanol; water for 44h; Heating; | 97% |
| Conditions | Yield |
|---|---|
| With triethylsilane; 2C2H3F3O*BF3 In dichloromethane at 20℃; for 3h; | 97% |
| With gallium(III) triflate; dimethylmonochlorosilane In dichloromethane at 20℃; for 0.5h; | 88% |
| With triethylsilane; 2C24BF20(1-)*C21H16N3P(2+) In dichloromethane at 120℃; for 13h; Inert atmosphere; | 94 %Spectr. |
-
-
768-90-1
1-Adamantyl bromide
-
-
1631-73-8
trimethylstannane
-
A
-
281-23-2
adamantane
-
B
-
1527-99-7
n-butyltrimethyltin
| Conditions | Yield |
|---|---|
| With n-butyllithium In hexane 1-bromoadamantane (1 equiv.) and TMTH (1 equiv.) in hexane cooled to 0°C under Ar, n-BuLi (1 equiv., 2.40 M in hexane) added, stirred for 15 min, quenched with water; analyzed by GC; | A 97% B 95% |
| Conditions | Yield |
|---|---|
| With hydrogen; aluminum oxide; nickel at 200℃; | 96% |
| With cerium(III) chloride; 9,10-diphenylanthracene; 1,2-bis(2,4,6-triisopropylphenyl)disulfane; tetrabutyl-ammonium chloride In acetonitrile for 24h; Irradiation; Inert atmosphere; | 95% |
-
-
77-73-6, 933-60-8, 1755-01-7
bi(cyclopentadiene)
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; trifluorormethanesulfonic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane at -78 - 20℃; for 18h; | 96% |
| With sodium tetrahydroborate; trifluoric acid In 1,1,2-Trichloro-1,2,2-trifluoroethane at -78 - 20℃; for 18h; Product distribution; other unsaturated polycyclics; | 96% |
-
-
91233-19-1
1-(adamantane-1-carbonyloxy)pyridine-2(1H)-thione
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With 9-borabicyclo[3.3.1]nonane dimer; tri-n-butyl-tin hydride In toluene at 0℃; | 96% |
| With thiophenol In tetrahydrofuran at -80℃; Product distribution; Mechanism; Irradiation; | |
| With 2,2'-azobis(isobutyronitrile); Tris(trimethylsilyl)methane In benzene at 80℃; | 89 % Chromat. |
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile); oxygen; tert-butyldibutyltin chloride; sodium cyanoborohydride In tert-butyl alcohol at 60℃; for 20h; Yields of byproduct given; | A n/a B 96% |
| With 2-(2-methoxyethoxy)ethyl alcohol; oxygen; sodium hydride In 1,4-dioxane at 20℃; for 24h; Schlenk technique; chemoselective reaction; | A 42% B n/a |
| Conditions | Yield |
|---|---|
| With [2-(di-tert-butylphosphinomethyl)-6-(diethylaminomethyl)pyridine]ruthenium(II) chlorocarbonyl hydride; isopropyl alcohol; sodium t-butanolate at 100℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | 95% |
| With air; diethylzinc; tri-n-butyl-tin hydride In benzene at 20℃; for 1h; | 90% |
| With water; zinc In acetonitrile at 80℃; for 41h; Inert atmosphere; Sealed tube; | 53% |
-
-
13380-94-4
octahydro-4,7-methano-inden-5-one
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; trifluorormethanesulfonic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane at -78 - 20℃; for 18h; | 95% |
| Conditions | Yield |
|---|---|
| With hydrogen; aluminum oxide; nickel at 180℃; Pd/SiO2, 330 deg C; | 95% |
| Multi-step reaction with 2 steps 1: DCC, DMAP 2: 93 percent / Bu3SnH, AIBN / benzene / 3 h / Heating View Scheme | |
| Multi-step reaction with 2 steps 1: 28 percent / 85percent H2O2 2: 3 percent Chromat. / cyclohexane / 81 °C View Scheme |
-
-
16104-50-0
1,3-dichloroadamantane
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium; N,N-diethyl-1,1,1-trimethylsilanamine In diethyl ether for 6h; Ambient temperature; | 95% |
| Conditions | Yield |
|---|---|
| With tetrabutylammonium tetrafluoroborate In acetonitrile at 20℃; Irradiation; | A 3% B n/a C 95% |
-
-
195874-42-1
C24H25NO2Se
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 3h; Heating; | 93% |
-
-
36712-30-8
adamantane-1-carboxylate
-
-
281-23-2
adamantane
| Conditions | Yield |
|---|---|
| With triethylsilane; C19H3BF14 In dichloromethane at 20℃; Inert atmosphere; Schlenk technique; | 93% |
-
-
98922-03-3
ethyl dispiro[1,3-dithiolane-2',2;4',2''-bis(adamantane)]-5'-carboxylate
-
A
-
281-23-2
adamantane
-
B
-
59210-87-6
(2-Adamantyl)essigsaeure-ethylester
| Conditions | Yield |
|---|---|
| nickel In methanol | A n/a B 92% |
| Conditions | Yield |
|---|---|
| With zirconocene dichloride; triethyl borane In tetrahydrofuran; hexane at 25℃; for 5h; | 92% |
| With iron(III) chloride; phenylsilane; sodium methylate In tetrahydrofuran for 12h; Schlenk technique; Inert atmosphere; | 89% |
| With Schwartz's reagent; triethyl borane In tetrahydrofuran at 25℃; for 17h; | 88% |
| Conditions | Yield |
|---|---|
| With azobisisobutyronitrile; sodium cyanoborohydride In α,α,α-trifluorotoluene; tert-butyl alcohol | 92% |
| With azobisisobutyronitrile; sodium cyanoborohydride In α,α,α-trifluorotoluene; tert-butyl alcohol | 92% |
| Conditions | Yield |
|---|---|
| In water-d2; d(4)-methanol at 19.84℃; for 0.0833333h; | 100% |
| Conditions | Yield |
|---|---|
| With iron(III)-acetylacetonate; carbon tetrabromide Reagent/catalyst; Sealed tube; Inert atmosphere; | A 99% B 23% |
| With bromine; iron at 0 - 50℃; for 3h; | A n/a B 93% |
| With iodine(I) bromide In tetrachloromethane for 3h; Heating; | A 75 % Chromat. B 25 % Chromat. |
| With iodine(I) bromide In tetrachloromethane for 3h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
| Conditions | Yield |
|---|---|
| With Fe(AAEMA)3; oxygen; isovaleraldehyde In 1,2-dichloro-ethane under 760 Torr; for 60h; Ambient temperature; | 99% |
| With oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate In dichloromethane; water at 0 - 25℃; under 3878.71 Torr; for 0.0222222h; Reagent/catalyst; Temperature; Solvent; | 99% |
| With water; bromine for 1h; Ambient temperature; | 95% |
-
-
281-23-2
adamantane
-
-
126683-99-6
1-(1-adamantyl)chlorophosphinoyladamantane
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride; phosphorus trichloride for 6.16667h; Reflux; | 99% |
| Stage #1: adamantane With aluminum (III) chloride; phosphorus trichloride Reflux; Stage #2: With water Cooling with ice; | 99% |
| With aluminium trichloride; phosphorus trichloride for 5h; Heating; | 95% |
| With aluminium trichloride; phosphorus trichloride for 5h; Heating; | 86.2% |
| With aluminium trichloride; water; phosphorus trichloride 1.) reflux, 6 h, 2.) chloroform; Yield given. Multistep reaction; |
-
-
281-23-2
adamantane
-
-
30470-60-1
adamantane-d16
| Conditions | Yield |
|---|---|
| With d8-isopropanol; 5% rhodium-on-charcoal; 10% Pt/activated carbon; water-d2 at 120℃; for 24h; Sealed tube; | 99% |
| Conditions | Yield |
|---|---|
| With bromine; Nitrogen dioxide In trifluoroacetic acid at 20℃; for 0.5h; | 98% |
| With water; bromine for 0.166667h; | 93% |
| With bromine at 85 - 110℃; Temperature; | 93% |
-
-
281-23-2
adamantane
-
-
16104-50-0
1,3-dichloroadamantane
| Conditions | Yield |
|---|---|
| With Iodine monochloride In tetrachloromethane for 5h; Heating; | 98% |
| With chlorosulfonic acid at 0 - 25℃; for 10h; | 98% |
| With chlorosulfonic acid at 0 - 25℃; for 8h; | 98% |
| Conditions | Yield |
|---|---|
| With oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate In dichloromethane; water at 0 - 25℃; under 3878.71 Torr; for 0.0222222h; | 98% |
| With potassium sulfate; sulfuric acid at 40 - 55℃; for 40h; Product distribution / selectivity; | 87% |
| With lithium sulfate; sulfuric acid at 40 - 55℃; for 40h; Product distribution / selectivity; | 87% |
| Conditions | Yield |
|---|---|
| With tetrachloromethane; manganese(III) acetylacetonate; acetonitrile at 200℃; for 1h; | 98% |
| With Iodine monochloride In tetrachloromethane for 0.25h; Ambient temperature; | 97% |
| With tetrachloromethane; ferrocene; ethanol at 160℃; for 6h; Sealed tube; | 93% |
| Conditions | Yield |
|---|---|
| With tetrachloromethane; K10 bentonite; iron(III) chloride for 40h; Heating; | A 2% B 98% |
| With tetrachloromethane; bis(acetylacetonate)oxovanadium; water at 160℃; for 6h; Sealed tube; | A 90% B n/a |
| With thionyl chloride; n-Butyl chloride; sulfuric acid at 30℃; for 30h; | A 73% B 10.5% |
-
-
281-23-2
adamantane
-
-
21336-43-6
1,3,5,7-tetrachloroadamanatane
| Conditions | Yield |
|---|---|
| With tetrachloromethane; aluminium trichloride for 1h; Heating; | 98% |
| With aluminum (III) chloride In tetrachloromethane Reflux; | 91% |
| Conditions | Yield |
|---|---|
| With Rh(PPh3)3Cl In dichloromethane at 150℃; for 3h; | 98% |
| Conditions | Yield |
|---|---|
| With bromine; iron In 1,1,2-Trichloro-1,2,2-trifluoroethane at 30℃; for 8h; | 97.3% |
| With bromine; iron at 20℃; for 2h; Cooling with ice; | 96% |
| With bromine at 0 - 25℃; | 85% |
| Conditions | Yield |
|---|---|
| With nitrosonium tetrafluoroborate for 4h; reflux; | 97% |
| With sulfuric acid at 3 - 25℃; for 5h; | 97% |
| With bromine for 0.666667h; Ambient temperature; | 96% |
| Conditions | Yield |
|---|---|
| With [2,2]bipyridinyl; Ba; trifluoroacetic acid In dichloromethane at 20℃; for 0.0333333h; Product distribution; | A n/a B 97% C n/a |
| With [2,2]bipyridinyl; Ba; trifluoroacetic acid In dichloromethane at 20℃; for 0.0333333h; Yields of byproduct given; | A n/a B 97% C n/a |
| With ammonium cerium(IV) nitrate; oxygen In acetonitrile for 5h; Ambient temperature; Irradiation; | A 5% B 85% C 5% |
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