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inquiryBromotrichloromethane CAS:75-62-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
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Min.Order:1 Gram
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inquiryBromotrichloromethane Basic information Product Name: Bromotrichloromethane Synonyms: bromotrichloro-methan;Carbon bromotrichloride;Carbon trichlorobromide;Carbonbromidetrichloride(CBrCl3);carbonbromotrichloride;carbontrichlorobromide;CCl3Br;h
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Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryConditions | Yield |
---|---|
With bromine at 59℃; Temperature; Wavelength; Reagent/catalyst; Irradiation; Inert atmosphere; | 99% |
With bromine im Licht; | |
With bromine at 225 - 275℃; im Rohr; |
tetrachloromethane
A
Bromotrichloromethane
B
dibromodichloromethane
C
chlorotribromomethane
Conditions | Yield |
---|---|
With aluminum tri-bromide for 8h; Heating; | A n/a B n/a C 12% |
Conditions | Yield |
---|---|
With aluminum tri-bromide | |
With aluminum tri-bromide | |
With aluminium trichloride; hydrogen bromide |
Conditions | Yield |
---|---|
With dibenzoyl peroxide | |
In neat (no solvent) formation on heating with CBr4 in presence of dibenzoylperoxide;; | |
In neat (no solvent) formation on heating with CBr4 in presence of dibenzoylperoxide;; |
Conditions | Yield |
---|---|
at 400℃; in Glasrohr; |
tetrachloromethane
A
Bromotrichloromethane
B
dibromodichloromethane
C
chlorotribromomethane
D
carbon tetrabromide
Conditions | Yield |
---|---|
With Bromoform; tetranormalbutyl ammonium fluoride for 0.166667h; Product distribution; Mechanism; Ambient temperature; equilibrium; products determined by GC-MS; |
Conditions | Yield |
---|---|
With bromine at 26.9℃; Rate constant; Kinetics; Thermodynamic data; other temp.: 358, 399, 456, 532 deg K; | |
With bromine at 26.85℃; under 990.079 Torr; Kinetics; Further Variations:; Temperatures; Pressures; |
Conditions | Yield |
---|---|
With bromine; chlorine In trichlorofluoromethane at 10℃; for 0.25h; Irradiation; Yield given; | |
With bromine; chlorine In trichlorofluoromethane at 10℃; for 0.25h; Irradiation; Yield given; |
dibromodichloromethane
A
tetrachloromethane
B
Bromotrichloromethane
C
chlorotribromomethane
D
carbon tetrabromide
Conditions | Yield |
---|---|
With acidic acceptor; tetranormalbutyl ammonium fluoride for 0.166667h; Product distribution; Mechanism; Ambient temperature; equilibrium; products determined by GC-MS; |
chlorotribromomethane
A
tetrachloromethane
B
Bromotrichloromethane
C
dibromodichloromethane
D
carbon tetrabromide
Conditions | Yield |
---|---|
With acidic acceptor; tetranormalbutyl ammonium fluoride for 0.166667h; Product distribution; Mechanism; Ambient temperature; equilibrium; products determined by GC-MS; |
carbon tetrabromide
A
tetrachloromethane
B
Bromotrichloromethane
C
dibromodichloromethane
D
chlorotribromomethane
Conditions | Yield |
---|---|
With chloroform; tetranormalbutyl ammonium fluoride for 0.166667h; Product distribution; Mechanism; Ambient temperature; equilibrium; products determined by GC-MS; |
tetrachloromethane
carbon tetrabromide
A
Bromotrichloromethane
B
dibromodichloromethane
C
chlorotribromomethane
Conditions | Yield |
---|---|
With sodium hydroxide In various solvent(s) Mechanism; Ambient temperature; effects of additives: p-dinitrobenzene and di-tert-butyl nitroxide; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium carbonate In phosphate buffer haloform reaction; Enzymatic reaction; |
Conditions | Yield |
---|---|
With bromide Mechanism; other halocarbons, other halide ions; |
Conditions | Yield |
---|---|
bei Siedetemperatur im Licht; | |
In neat (no solvent) byproducts: HBr; equilibrium;; enthalpy of reaction;; | |
In neat (no solvent) Irradiation (UV/VIS); formation by light;; |
Bromotrichloromethane
Conditions | Yield |
---|---|
With ethanol at 100℃; |
Bromotrichloromethane
Conditions | Yield |
---|---|
With bromine at 120℃; |
chloroform
bromine
A
Bromotrichloromethane
B
dibromodichloromethane
C
chlorotribromomethane
Conditions | Yield |
---|---|
at 225 - 275℃; im Licht; |
Conditions | Yield |
---|---|
at 250℃; beim Leiten im Licht durch ein Quarzrohr im Stickstoffstrom; |
Conditions | Yield |
---|---|
at 400℃; |
Conditions | Yield |
---|---|
at 100 - 110℃; |
bromine
trichloro-acetic acid ; potassium-compound
A
Bromotrichloromethane
B
methylammonium carbonate
Conditions | Yield |
---|---|
at 120℃; |
tetrachloromethane
bromine
A
1,1,2,2-tetrachloroethylene
B
Bromotrichloromethane
C
dibromodichloromethane
D
hexachloroethane
E
bromine chloride
Conditions | Yield |
---|---|
In tetrachloromethane other Radiation; γ-radiation of Br2 soln. in CCl4 (free from air) at 25°C; mechanism discussed;; |
tetrachloromethane
bromine
A
Bromotrichloromethane
B
hexachloroethane
C
bromine chloride
Conditions | Yield |
---|---|
In tetrachloromethane other Radiation; γ-radiation of Br2 soln. in CCl4 (free from air); yield depends on temp.;; |
tetrachloromethane
bromine
A
Bromotrichloromethane
B
dibromodichloromethane
Conditions | Yield |
---|---|
In tetrachloromethane reaction of activated in CCl4 dissolved Br2, formation of radioactive CCl3Br, CCl2Br2 and higher boiling compounds;; yields depend on Br2 concn., given as diagram;; | |
In tetrachloromethane reaction of activated in CCl4 dissolved Br2, formation of radioactive CCl3Br, CCl2Br2 and higher boiling compounds;; yields depend on Br2 concn., given as diagram;; |
tetrachloromethane
A
trichloromethyl radical
B
Bromotrichloromethane
C
hexachloroethane
Conditions | Yield |
---|---|
In neat (no solvent) reaction at 600°C on passing CCl4-gas over AgBr; mechanism discussed;; condensation of the reaction mixture to -190°C; determination by IR;; | |
In neat (no solvent) reaction at 600°C on passing CCl4-gas over AgBr; mechanism discussed;; condensation of the reaction mixture to -190°C; determination by IR;; |
Conditions | Yield |
---|---|
In neat (no solvent) formation on heating CCl3CO2K with Br2 to 120°C;; | |
In neat (no solvent) formation on heating CCl3CO2K with Br2 to 120°C;; |
4-benzoyloxycyclohexanone
Bromotrichloromethane
Benzoic acid 4-dichloromethylene-cyclohexyl ester
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile at 20℃; for 1h; | 100% |
Bromotrichloromethane
N,N,N',N'-Tetraisopropyl-P-methylphosphonous diamide
A
chloroform
B
P-(bromomethyl)-N,N,N',N'-tetraisopropylphosphonous diamide
Conditions | Yield |
---|---|
In diethyl ether for 0.25h; Ambient temperature; | A 100% B 45% |
In diethyl ether for 0.25h; Ambient temperature; or P-ethyl-N,N,N',N'-tetraisopropylphosphonous diamide; | A n/a B 45% |
Bromotrichloromethane
P-ethyl-N,N,N',N'-tetraisopropylphosphonous diamide
A
chloroform
B
P-(1-bromoethyl)-N,N,N',N'-tetraisopropylphosphonous diamide
Conditions | Yield |
---|---|
In diethyl ether for 0.25h; Ambient temperature; | A 100% B 45% |
Conditions | Yield |
---|---|
With air; triethyl borane In ethanol; water at 25℃; for 2h; Product distribution; Further Variations:; Solvents; | 99% |
With iron In N,N-dimethyl-formamide at 60℃; for 5h; | 96% |
With potassium acetate; manganese(II) acetate; acetic acid; methyl 2-cyanoacetate at 40℃; anodic oxidation; | 95% |
Bromotrichloromethane
Allyl ether
3-(bromomethyl)-4-(2,2,2-trichloroethyl)tetrahydrofuran
Conditions | Yield |
---|---|
With sodium hydroxide; dimanganese decacarbonyl In dichloromethane Irradiation; | 99% |
With sodium hydroxide; Mn(CO)10; N-benzyl-N,N,N-triethylammonium chloride In dichloromethane; water for 2h; Irradiation; | 99% |
With Benzoylformic acid In Petroleum ether for 18h; Sealed tube; Irradiation; Green chemistry; | 79% |
Conditions | Yield |
---|---|
With sodium hydroxide; BrMn(CO)5 In dichloromethane Irradiation; | 99% |
With sodium hydroxide; dimanganese decacarbonyl; N-benzyl-N,N,N-triethylammonium chloride In dichloromethane; water for 2h; Irradiation; | 99% |
With Benzoylformic acid In Petroleum ether for 18h; Sealed tube; Irradiation; Green chemistry; | 82% |
Bromotrichloromethane
methacrylic acid methyl ester
methyl 2-bromo-2-methyl-4,4,4-trichlorobutanoate
Conditions | Yield |
---|---|
With tetralin; C15H17ClNRu at 135℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 99% |
With C28H41N3O4Pd In acetonitrile at 20℃; for 16h; Inert atmosphere; Schlenk technique; Glovebox; | 75% |
With (Me3tacn)PdCl2 at 65℃; for 18h; Kharasch reaction; | 97.5 %Spectr. |
Bromotrichloromethane
(S)-4-benzyl-3-hexanoyl-5,5-dimethyloxazolidin-2-one
C19H24Cl3NO3
Conditions | Yield |
---|---|
Stage #1: (S)-4-benzyl-3-hexanoyl-5,5-dimethyloxazolidin-2-one With titanium tetrachloride In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 0.666667h; Inert atmosphere; Stage #3: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane at 45℃; for 12h; Inert atmosphere; Sealed vial; optical yield given as %de; | 99% |
Bromotrichloromethane
Conditions | Yield |
---|---|
Stage #1: Bromotrichloromethane; 2-(1-adamantylsulfanyl)-3-bromo-6-iodobenzaldehyde With triphenylphosphine In acetonitrile at 50℃; Corey-Fuchs Alkyne Synthesis; Stage #2: With potassium tert-butylate In tetrahydrofuran at -78℃; for 1.5h; | 99% |
Conditions | Yield |
---|---|
With tetralin; C15H17ClNRu at 80℃; for 6h; Kinetics; Reagent/catalyst; Inert atmosphere; | 98% |
With diethylamine; copper(l) chloride for 4h; | 95.8% |
With dilauryl peroxide | 81% |
Conditions | Yield |
---|---|
With Benzoylformic acid In Petroleum ether for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Sealed tube; Irradiation; Green chemistry; | 98% |
With potassium carbonate; palladium diacetate; triphenylphosphine In benzene at 100℃; for 3.5h; | 90% |
With C62H44N6Ru(2+)*2Cl(1-) In dimethyl sulfoxide for 24h; Sealed tube; Irradiation; | 90% |
With disodium tetracarbonylferrate In tetrahydrofuran at 25℃; for 16h; Catalytic behavior; Reagent/catalyst; Glovebox; Inert atmosphere; | 83% |
With potassium carbonate; Pd(PPh3)(OAc)2 at 40℃; for 5h; | 88 % Chromat. |
Bromotrichloromethane
Allyl acetate
2-bromo-4,4,4-trichlorobutyl acetate
Conditions | Yield |
---|---|
With iron In N,N-dimethyl-formamide at 60℃; for 5h; | 98% |
for 8h; Irradiation; | 89% |
With potassium carbonate; palladium diacetate; triphenylphosphine In benzene at 80℃; for 7h; CO atmosphere; | 83% |
With potassium carbonate; Pd(PPh3)(OAc)2 at 80℃; for 7h; | 83% |
With triethyl borane In methanol; water | 70% |
Conditions | Yield |
---|---|
With iron In N,N-dimethyl-formamide at 60℃; for 5h; | 98% |
Bromotrichloromethane
(S)-4-benzyl-5,5-dimethyl-3-propanoyl-1,3-oxazolidin-2-one
(S)-4-benzyl-5,5-dimethyl-3-((S)-3,3,3-trichloro-2-methylpropanoyl)-oxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: (S)-4-benzyl-5,5-dimethyl-3-propanoyl-1,3-oxazolidin-2-one With titanium tetrachloride In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 0.666667h; Inert atmosphere; Stage #3: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane at 45℃; for 12h; Inert atmosphere; Sealed vial; optical yield given as %de; | 98% |
Stage #1: (S)-4-benzyl-5,5-dimethyl-3-propanoyl-1,3-oxazolidin-2-one With 1,2,2,6,6-pentamethylpiperidine; titanium tetrachloride In dichloromethane at 0℃; for 0.75h; Inert atmosphere; Stage #2: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane at 45℃; for 12h; | 97% |
Stage #1: (S)-4-benzyl-5,5-dimethyl-3-propanoyl-1,3-oxazolidin-2-one With titanium tetrachloride In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 0.75h; Inert atmosphere; Stage #3: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane for 12h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | 96% |
Stage #1: (S)-4-benzyl-5,5-dimethyl-3-propanoyl-1,3-oxazolidin-2-one With titanium tetrachloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 0.666667h; Inert atmosphere; Stage #2: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane at 45℃; for 12h; Inert atmosphere; Sealed flask; optical yield given as %de; stereoselective reaction; | 95% |
Bromotrichloromethane
4-(methoxycarbonyl)benzyl alcohol
p-methyloxycarbonylbenzyl chloride
Conditions | Yield |
---|---|
Stage #1: Bromotrichloromethane With triphenylphosphine In dichloromethane at 20℃; for 0.666667h; Appel reaction; in air; Stage #2: 4-(methoxycarbonyl)benzyl alcohol In dichloromethane at 20℃; Appel reaction; in air; | 98% |
Bromotrichloromethane
D
4-methyl-2-(trichloromethylsulfanyl)-thiazole
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In benzene at 80℃; | A 10% B n/a C n/a D 98% |
Bromotrichloromethane
B
4-methyl-2-(trichloromethylsulfanyl)-thiazole
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In benzene at 80℃; | A 94% B 98% |
styrene
Bromotrichloromethane
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R,R)-4,5-Bis-2,2-dimethyl-1,3-dioxolan In hexane; toluene at -78 - 20℃; Catalytic behavior; Temperature; Concentration; Solvent; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | A 98% B n/a |
Conditions | Yield |
---|---|
With C62H44N6Ru(2+)*2Cl(1-) In dimethyl sulfoxide for 24h; Sealed tube; Irradiation; | 98% |
With Benzoylformic acid In Petroleum ether for 18h; Sealed tube; Irradiation; Green chemistry; | 94% |
Bromotrichloromethane
Hexadecanoic acid 2-(4-methoxy-phenyl)-4-thioxo-4H-quinazolin-3-yl ester
2-(4-Methoxy-phenyl)-4-trichloromethylsulfanyl-quinazoline
Conditions | Yield |
---|---|
In dichloromethane for 0.0833333h; Ambient temperature; Irradiation; | 97% |
Conditions | Yield |
---|---|
With carbon monoxide In further solvent(s) Irradiation (UV/VIS); Irradiation of complex at 350-380 nm under 20 atm of CO in CBrCl3;; | A 81-87 B 97% C 78-85 D <4 E >65 |
Conditions | Yield |
---|---|
In dichloromethane Irradiation (UV/VIS); mixt. irradiation (10 min, vac.); (1)H-NMR spectroscopy; | 97% |
Bromotrichloromethane
trans-[Rh(CO)(Cl){P{(CH2)14}3P2(Rh-P2)}]
[Rh(CO)ClBr(CCl3)((P((CH2)7)3)2)]
Conditions | Yield |
---|---|
In benzene-d6 NMR; | 97% |
Conditions | Yield |
---|---|
Stage #1: C23H33NO3 With titanium tetrachloride In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 0.666667h; Inert atmosphere; Stage #3: Bromotrichloromethane With tris(triphenylphosphine)ruthenium(II) chloride In dichloromethane at 45℃; for 12h; Inert atmosphere; Sealed vial; optical yield given as %de; | 97% |
Conditions | Yield |
---|---|
In benzene-d6 Inert atmosphere; | 97% |
Bromotrichloromethane
3-chloroprop-1-ene
3-bromo-1,1,1,4-tetrachlorobutane
Conditions | Yield |
---|---|
In pentane for 7h; Irradiation; T < 20 deg C; | 96.2% |
With Benzoylformic acid In Petroleum ether for 18h; Sealed tube; Irradiation; Green chemistry; | 64% |
With C62H44N6Ru(2+)*2Cl(1-) In dimethyl sulfoxide for 24h; Sealed tube; Irradiation; | 50% |
allylbenzene
Bromotrichloromethane
3-bromo-1,1,1-trichloro-4-phenylbutane
Conditions | Yield |
---|---|
With iron In N,N-dimethyl-formamide at 60℃; for 5h; | 96% |
With sodium acetate In 1,2-dimethoxyethane at 90℃; for 24h; Reagent/catalyst; Solvent; Kharash-Sosnovsky Allylic Oxidation; Green chemistry; | 88% |
With 3',6'-bis(diethylamino)-2-(naphthalen-2-yl)spiro[isoindoline-1,9'-xanthen]-3-one; benzoic acid anhydride at 80℃; for 20h; Inert atmosphere; | 84% |
Bromotrichloromethane
3-palmitoyloxy-4-phenylthiazolin-2(3H)-thione
A
pentadecyl bromide
B
5-phenyl-2-trichloromethylthiothiazole
Conditions | Yield |
---|---|
In benzene for 2h; Ambient temperature; Irradiation; | A 96% B 92% |
Bromotrichloromethane
3,5-dinitrobenzyl alcohol
3,5-dinitrobenzyl chloride
Conditions | Yield |
---|---|
Stage #1: Bromotrichloromethane With triphenylphosphine In dichloromethane at 20℃; for 0.666667h; Appel reaction; in air; Stage #2: 3,5-dinitrobenzyl alcohol In dichloromethane at 20℃; Appel reaction; in air; | 96% |
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