3-PyridinecarboxaldehydeProduct Name: 3-PyridinecarboxaldehydeSynonyms: Nicotinaldehyde; Pyridine-3-carboxaldehyde; pyridine-3-carbaldehyde; Pyridine-3-aldehyde; 3-Pyridine carboxaldehydeCAS RN.: 500-22-1EINECS: 207-900-4Molecular Weight: 107.11Appea
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:500-22-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:500-22-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryService we can provide: 1. mixed container: we can mix different items in one container. 2. quality control: before shipment, we can provide free sample for test. inspection before shipping. 3. packing: we can pack according to your requireme
Cas:500-22-1
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:
3-Pyridinecarboxaldehyde CAS RN.: 500-22-1 EINECS: 207-900-4 Molecular Weight: 107.11 Molecular Formula: C6H5NO Structural formula: melting point 8°C boiling point
Cas:500-22-1
Min.Order:1 Kilogram
FOB Price: $2.0 / 3.0
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:500-22-1
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryAs a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences, T
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Name: 3-Pyridinecarboxaldehyde Synonyms: 3-Formylpyridine;3-Nicotinaldehyde;3-Pyridinaldehyde;3-Pyridinealdehyde;3-Pyridylaldehyde;3-Pyridylcarboxaldehyde;3-Pyridylcarboxaldehyde DEG;beta-Pyridinecarbonaldehyde CAS: 500-22-1 MF: C6H5NO
Cas:500-22-1
Min.Order:1 Kilogram
FOB Price: $500.0
Type:Lab/Research institutions
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1966.html Product Name 3-Pyridinecarboxaldehyde CAS No. 500-22-1
Cas:500-22-1
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:500-22-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryName: Nicotinaldehyde Molecular Formula:C6H5NO Molecular Weight:107.11 CAS No.:500-22-1 Appearance:Brown clear Liquid Appearance:Brown clear Liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg Application
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:500-22-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: DL-Dithiothreitol Synonyms: DL-1,4-Dithiothreitol, 1M solution in water, for molecular biology;Dithiothreitol ,98%;DL-1,4-Dithiothreitol,DTT;DTT DL-1,4-Dithiothreitol;DL-Dithiothreitol ,99% [for Molecular biology];DL-1,4-Dithiothr
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:500-22-1
Min.Order:1 Gram
FOB Price: $102.0 / 124.0
Type:Trading Company
inquiry3-Pyridinecarboxaldehyde CAS:500-22-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:500-22-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:500-22-1
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:500-22-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: 3-Pyridinecarboxaldehyde Synonyms: Nicotinic Acid Impurity 4;3-Formylpyridine;3-Nicotinaldehyde;3-Pyridinaldehyde;3-Pyridinealdehyde;3-Pyridylaldehyde;3-Pyridylcarboxaldehyde;3-Pyridylcarboxaldehyde DEG CAS: 500-22-1 MF: C6H5NO
Cas:500-22-1
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: 3-Pyridinecarboxaldehyde Molecular Structure: Formula: C6H5NO Molecular Weight : 107.11 Synonyms: 3-Formylpyridine;3-Nicotinaldehyde;3-Pyridinaldehyde;3-P
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:500-22-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:500-22-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:500-22-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:500-22-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:500-22-1
Min.Order:100 Gram
Negotiable
Type:Other
inquiryConditions | Yield |
---|---|
With 10% Ru/C; oxygen In toluene at 90℃; under 760.051 Torr; for 24h; | 100% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide for 0.25h; Ambient temperature; | 99% |
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; oxygen; copper(I) bromide dimethylsulfide complex In chlorobenzene at 80℃; for 8h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In water; dimethyl sulfoxide at 60℃; for 8h; High pressure; Green chemistry; | 99.9% |
With C13H26B(1-)*K(1+) In tetrahydrofuran for 24h; Ambient temperature; | 96% |
Stage #1: pyridine-3-carbonitrile With diisobutylaluminium hydride In toluene at 20℃; for 0.222222h; Flow reactor; Stage #2: With water; sodium L-tartrate In toluene at 0℃; chemoselective reaction; | 52% |
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.25h; | 99% |
With diethyl ether; diisobutylaluminium hydride |
nicotinaldehyde oxime
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With titanium tetrachloride; sodium iodide In acetonitrile for 0.0833333h; Ambient temperature; other oximes, var. time; | 97% |
Conditions | Yield |
---|---|
With n-butyllithium; diisobutylaluminium hydride; tert-butyl alcohol In tetrahydrofuran; hexane at 0℃; | 97% |
Multi-step reaction with 2 steps 1: diethyl ether; lithium alanate 2: lead (IV)-acetate; benzene View Scheme |
N-methyl-N-(3-pyridylmethyl)amine
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In chloroform for 12h; Reflux; | 95% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In chloroform for 24h; Reflux; | 93% |
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; silica gel In dichloromethane at 20℃; for 1.8h; | 91% |
Conditions | Yield |
---|---|
With sodium hypochlorite; C8H18NPol; sodium hydrogencarbonate In water; toluene at 15 - 20℃; for 4.5h; Product distribution / selectivity; | A 90.1% B 3.4% |
With sodium hypochlorite; C13H26N2OPol; sodium hydrogencarbonate In water; toluene at 15 - 20℃; for 4.5h; Product distribution / selectivity; | A 87.7% B 3.5% |
With sodium hypochlorite; C16H28N2O5Pol; sodium hydrogencarbonate In water; 1,2-dichloro-ethane at 15 - 20℃; for 4.5h; Product distribution / selectivity; | A 85.3% B 5.3% |
3-pyridinecarbonyl chloride
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) In benzene for 0.166667h; Ambient temperature; | 90% |
With diethylene glycol dimethyl ether; lithium tri-t-butoxyaluminum hydride at -78℃; | |
With piperidine; diethyldihydroaluminate 1.) THF, RT, 30 min, 2.) THF, toluene, RT, 1 h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: benzene; pyridine 2: lithium alanate; tetrahydrofuran / 0 °C View Scheme |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate In dichloromethane at 20℃; | 90% |
3-Bromopyridine
n-butyllithium
N,N-dimethyl-formamide
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
Stage #1: 3-Bromopyridine; n-butyllithium In toluene at -50℃; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at -50 - -15℃; | 90% |
Conditions | Yield |
---|---|
With 2,6-dicarboxypyridinium fluorochromate for 0.333333h; | 90% |
With dihydrogen peroxide; phosphotungstic acid In various solvent(s) at 20℃; for 5h; Product distribution; Further Variations:; Catalysts; | 76% |
With oxygen; benzaldehyde In benzonitrile; toluene at 60℃; for 2.58333h; Green chemistry; |
3-Bromopyridine
dicobalt octacarbonyl
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With triethylsilane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium acetate In acetonitrile at 60℃; for 16h; Schlenk technique; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 80℃; under 7500.75 Torr; for 20h; Autoclave; Green chemistry; | 89% |
With rhodium(III) iodide; hydrogen; acetic anhydride; triethylamine; triphenylphosphine In N,N-dimethyl acetamide at 100℃; for 24h; Autoclave; | 60% |
3-Methylpyridine
2,2'-diphenyl-[3,3']biindolylidene 1,1'-dioxide
A
pyridine
B
3-pyridinecarboxaldehyde
C
nicotinic acid
D
2,2'-diphenyl-1H,1'H-3,3'-biindole
Conditions | Yield |
---|---|
at 140℃; for 14h; Product distribution; | A 5% B 18% C 60% D 88% |
at 140℃; for 14h; Further byproducts given; | A 5% B 18% C 60% D 88% |
2,2'-diphenyl-[3,3']biindolylidene 1,1'-dioxide
A
pyridine
B
3-pyridinecarboxaldehyde
C
nicotinic acid
D
2,2'-diphenyl-1H,1'H-3,3'-biindole
Conditions | Yield |
---|---|
With 3-Methylpyridine at 140℃; for 14h; Further byproducts given; | A 5% B 18% C 60% D 88% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane at 0 - 20℃; for 0.333333h; Inert atmosphere; Green chemistry; | 88% |
Multi-step reaction with 2 steps 1: 85 percent / CH2Cl2 / 12 h 2: 15 percent / NaOMe / methanol / 35 deg C -> 20 deg C, 2 h View Scheme |
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.166667h; | 86% |
With lithium-tris(diethylamino)hydridoaluminate In tetrahydrofuran for 12h; Ambient temperature; | 53% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; nitric acid; acetic acid at 40℃; under 1520.1 Torr; for 5h; Temperature; Pressure; Reagent/catalyst; Autoclave; Sealed tube; | 85% |
With tert.-butylhydroperoxide at 120℃; for 5h; Sealed tube; Green chemistry; | 80% |
With oxygen; V-Mo oxide at 370 - 430℃; Mechanism; | |
With selenium(IV) oxide | |
With oxygen In water at 290℃; under 760.051 Torr; Reagent/catalyst; |
N-methoxy-N-methylpyridine-3-carboxamide
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.25h; | 85% |
With lithium diisobutyl-tert-butoxyaluminum hydride In tetrahydrofuran; hexane at 0℃; Inert atmosphere; chemoselective reaction; | > 99 %Chromat. |
3-picolyl bromide
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With oxygen; kieselguhr; copper(l) chloride In hexane for 2.5h; Oxidation; Heating; | 84% |
2-nitropropane
A
3-pyridinecarboxaldehyde
B
α-(1-methyl-1-nitroethyl)-3-pyridinemethanol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran Hass-Bender/Henry reaction; | A n/a B 84% |
Conditions | Yield |
---|---|
With sodium carbonate In ethylene glycol for 0.025h; McFadyen-Stevens reaction; microwave irradiation; | 82% |
Conditions | Yield |
---|---|
With sodium formate In N,N-dimethyl-formamide at 110℃; under 760.051 Torr; for 8h; | 80% |
With sodium formate In N,N-dimethyl-formamide at 100℃; under 760.051 Torr; for 10h; | 79% |
With palladium(II) acetylacetonate; N,N,N,N,-tetramethylethylenediamine; hydrogen; bis-diphenylphosphinomethane In toluene at 100℃; under 7500.75 Torr; for 10h; Autoclave; | 78% |
Conditions | Yield |
---|---|
With carbon monoxide; triethylamine In benzene | 80% |
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With tetrafluoroboric acid In tetrahydrofuran; water for 192h; Ambient temperature; | 78% |
3-iodopyridine
9-methyl-9H-fluorene-9-carbonyl chloride
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)palladium(II); N-Methyldicyclohexylamine; potassium formate; tetra-(n-butyl)ammonium iodide; tricyclohexylphosphine tetrafluoroborate; bis(dibenzylideneacetone)-palladium(0); tri tert-butylphosphoniumtetrafluoroborate In acetonitrile at 80℃; for 18h; Sealed tube; Glovebox; Inert atmosphere; | 78% |
nicotinic anhydride
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With P(p-CH3OC6H4)3; methylphenylsilane; bis(dibenzylideneacetone)-palladium(0) In toluene at 40℃; for 20h; Schlenk technique; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 71% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 2h; Sealed tube; | 70% |
3-pyridinecarboxaldehyde
benzoic acid hydrazide
(E)-N'-(pyridin-3-ylmethylene)benzohydrazide
Conditions | Yield |
---|---|
at 205℃; under 4350.44 Torr; for 0.0666667h; Microwave irradiation; neat (no solvent); | 100% |
In ethanol for 3h; Heating; | 89% |
With hydrogenchloride In ethanol at 20℃; for 0.5h; Condensation; | 84% |
3-pyridinecarboxaldehyde
nicotinaldehyde oxime
Conditions | Yield |
---|---|
With pyridine; hydroxylamine hydrochloride In ethanol | 100% |
With hydroxylamine hydrochloride; sodium acetate In methanol; water for 0.5h; Reflux; | 58% |
With hydroxylamine hydrochloride; sodium hydroxide In water at 20℃; for 0.5h; | 47% |
3-pyridinecarboxaldehyde
2-Aminobenzyl alcohol
2-Pyridin-3-yl-1,4-dihydro-2H-benzo[d][1,3]oxazine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
3-pyridinecarboxaldehyde
3-hydrazino-5H-[1,2,4]triazino[5,6-b]indole
3-(Pyridine-3-aldehyde)hydrazono-1,2,4-triazino<5,6-b>indole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 1h; Heating; | 100% |
3-pyridinecarboxaldehyde
2-Hydroxybenzylamine
2-Pyridin-3-yl-3,4-dihydro-2H-benzo[e][1,3]oxazine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
3-pyridinecarboxaldehyde
u-2-amino-1-phenylpropan-1-ol
3-((4S,5R)-4-Methyl-5-phenyl-oxazolidin-2-yl)-pyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; Further byproducts given; | 100% |
3-pyridinecarboxaldehyde
Norpseudoephedrine
3-((4R,5R)-4-Methyl-5-phenyl-oxazolidin-2-yl)-pyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; Further byproducts given; | 100% |
3-pyridinecarboxaldehyde
potassium cyanide
2-hydroxy-2-(pyridin-3-yl)acetonitrile
Conditions | Yield |
---|---|
With water; acetic acid at 5 - 10℃; for 2h; | 100% |
With hydrogenchloride | |
With acetic acid In water for 18h; Ambient temperature; |
3-pyridinecarboxaldehyde
2-Amino-2-methyl-1-propanol
3-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
3-pyridinecarboxaldehyde
sulfanilamide
N4-(3-pyridylidene) sulfanilamide
Conditions | Yield |
---|---|
at 150 - 155℃; for 0.0833333h; | 100% |
In ethanol for 3h; Heating; |
3-pyridinecarboxaldehyde
acrylic acid methyl ester
methyl 2-[hydroxy(pyridin-3-yl)methyl]propenoate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In 1,4-dioxane; water at 20℃; for 8h; Baylis-Hillman reaction; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane at 20℃; for 0.75h; Baylis-Hillman reaction; neat (no solvent); | 100% |
With uracil-Cu2+ nanoparticles immobilized on alpha-zirconium hydrogen phosphate In N,N-dimethyl-formamide at 20℃; for 8.5h; Morita-Baylis-Hillman Alkylation; | 100% |
3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With piperidine In acetonitrile for 4h; Heating; | 100% |
3-pyridinecarboxaldehyde
propan-1-ol-3-amine
2-Pyridin-3-yl-[1,3]oxazinane
Conditions | Yield |
---|---|
In ethanol for 2h; Ambient temperature; | 100% |
3-pyridinecarboxaldehyde
p-aminoethylbenzoate
ethyl p-(3-pyridylmethyleneamino)benzoate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 12h; Reflux; | 100% |
toluene-4-sulfonic acid In toluene for 12h; Reflux; | 100% |
In benzene for 6h; Heating; | 98.5% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane at 0℃; for 0.833333h; Morita-Baylis-Hillman reaction; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In neat (no solvent) at 0℃; for 0.833333h; Catalytic behavior; Solvent; Temperature; Time; Morita-Baylis-Hillman Alkylation; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane at 20℃; for 0.2h; Baylis-Hillman reaction; neat (no solvent); | 99% |
Conditions | Yield |
---|---|
With triphenylphosphine-bound polystyrene In tetrahydrofuran at 20℃; for 24h; Staudinger/Aza-Wittig reaction; | 100% |
Conditions | Yield |
---|---|
With triphenylphosphine-bound polystyrene In tetrahydrofuran at 20℃; for 24h; Staudinger/Aza-Wittig reaction; | 100% |
3-pyridinecarboxaldehyde
p-toluidine
3-<(4-methylphenyl)iminomethyl>pyridine
Conditions | Yield |
---|---|
at 120 - 130℃; for 2.5h; | 100% |
In ethanol Heating; | |
With sulfonic acid supported on hydroxyapatite-γ-Fe2O3 In ethanol |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol for 0.416667h; Heating; | 100% |
With hydroxylamine hydrochloride | 100% |
With hydroxylamine hydrochloride; triethylamine In methanol at 80℃; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
In ethanol Heating; | 100% |
With iron(III) chloride In methanol at 20℃; for 0.5h; | 90% |
In methanol for 3h; Heating; | 85% |
In methanol at 80℃; for 0.5h; | 47% |
In methanol for 0.166667h; |
3-pyridinecarboxaldehyde
4-methoxy-aniline
3-<(4-methoxyphenyl)iminomethyl>pyridine
Conditions | Yield |
---|---|
In ethanol for 1h; Sonication; | 100% |
With acetic acid In ethanol at 85℃; for 12h; | 50.3% |
In tetrahydrofuran for 0.5h; Heating; |
Conditions | Yield |
---|---|
In ethanol Heating; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
3-pyridinecarboxaldehyde
(R)-1-phenyl-ethyl-amine
((R)-1-Phenyl-ethyl)-[1-pyridin-3-yl-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
In dichloromethane at 20℃; for 48h; |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
3-pyridinecarboxaldehyde
(R)-2-methoxy-1-phenylethylamine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
3-pyridinecarboxaldehyde
4-[bromo-(piperidin-4-ylidene)methyl]-N,N-diethylbenzamide
4-[bromo[1-(3-pyridinylmethyl)-4-piperidinylidene]methyl]-N,N-diethyl-benzamide
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 18h; | 100% |
3-pyridinecarboxaldehyde
3-(cyclopentyloxy)-4-methoxybenzenamine
Conditions | Yield |
---|---|
Stage #1: 3-pyridinecarboxaldehyde; 3-(cyclopentyloxy)-4-methoxybenzenamine With toluene-4-sulfonic acid In methanol for 4h; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; for 20h; | 100% |
3-pyridinecarboxaldehyde
4-(2,4-difluorophenoxy)aniline
N-(4-(2,4-difluorophenoxy)phenyl)pyrid-3-ylmethyleneamine
Conditions | Yield |
---|---|
In methanol at 55℃; for 3h; | 100% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View