Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:100-55-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:100-55-0
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryHangzhou Dingyan Chem Co., Ltd
Items Standard Result Appearance A clear intense yellow, viscous, oily liquid Conforms Assay ≥
Cas:100-55-0
Min.Order:1 Gram
FOB Price: $2.0 / 5.0
Type:Manufacturers
inquiryJinan Finer Chemical Co., Ltd
Product Description Product website: http://www.finerchem.com Product Name 3-(Hydroxymethyl)pyridine CAS No. 100-55-0 Appearance
Cas:100-55-0
Min.Order:1 Gram
FOB Price: $8.0
Type:Lab/Research institutions
inquiryWuhan Fortuna Chemical Co.,Ltd
Unique advantages for 3-Pyridinemethanol Cas 100-55-0 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Light yellow liquid Storage:Store in 2-8℃ Package:1kg/bottle;25kg/dr
Cas:100-55-0
Min.Order:1 Kilogram
FOB Price: $350.0 / 366.0
Type:Trading Company
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Xi'an Xszo Chem Co., Ltd.
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:100-55-0
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryChemwill Asia Co., Ltd.
Highly quality and large production Factory Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Our main production base is located in Xuzhou industry park. We produce a wide range of organics includin
Henan Tianfu Chemical Co., Ltd.
3-Pyridinemethanol Basic information Product Name: 3-Pyridinemethanol Synonyms: 3-Pyridinylmethanol;beta-Picolyl alcohol;beta-picolylalcohol;beta-Pyridinecarbinol;beta-Pyridylcarbinol;Ni
Cas:100-55-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHebei Nengqian Chemical Import and Export Co., LTD
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:100-55-0
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryZhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:100-55-0
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:100-55-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Sartort Biopharma Co., Ltd
Appearance:clear light yellow to yellow liquid Storage:Inert atmosphere,Room Temperature Package:25kg/Barrel Application:pesticide intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:100-55-0
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryShanghai Upbio Tech Co.,Ltd
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:100-55-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryBaoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:100-55-0
Min.Order:1 Kilogram
FOB Price: $20.0 / 22.0
Type:Trading Company
inquiryQingdao Beluga Import and Export Co., LTD
3-Pyridinemethanol CAS:100-55-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:100-55-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Keyingchem Co.,Ltd
Hangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service professional enterprise, Our company mainly engages in global pharmaceutical,
Cas:100-55-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryXiamen Hisunny Chemical Co.,Ltd
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Shaanxi Cuicheng Biomedical Technology Co., Ltd.
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-55-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHANGZHOU YUNUO CHEMICAL CO.,LTD
moderate price & quick delivery. Appearance:clear light yellow to yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:antineoplasti
Siwei Development Group Ltd.
Product name: 3-Pyridinemethanol CAS No.：100-55-0 Molecule Formula：C6H7NO Molecule Weight：109.13 Purity: 98.0% Package: 200kg/drum Description：Yellowish to colorless liquid Manufacture Standards：Enterprise Standard
Cas:100-55-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryZibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Xiamen Jenny Chemical Technology Co., Ltd.
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Shanghai Minstar Chemical Co., Ltd
Product Name: 3-Pyridinemethanol Synonyms: 3-PYRIDYLMETHANOL;3-PYRIDINEMETHANOL;3-Hydroxymethyl pyridine (3-Pyridine methanol);3-(HYDROXYMETHYL)-PYRIDINE 97% (GC);ω-hydroxy-3-picoline;3-(HYDROXYMETHYL)PYRIDINE 98%;3-HYDROXYMETHYL PYRIDINE
EAST CHEMSOURCES LIMITED
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:100-55-0
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.
We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Synthetic route
| Conditions | Yield |
|---|---|
| With LaCu0.67Si1.33; hydrogen In methanol at 120℃; under 22502.3 Torr; for 9h; Autoclave; | 99% |
| With isopropyl alcohol at 300℃; for 3h; | 98% |
| With triethylamine; isopropyl alcohol; lithium bromide at 20℃; for 48h; Meerwein-Ponndorf-Verley reaction; | 97% |
| Conditions | Yield |
|---|---|
| With [RuCl2(N-heterocyclic carbene)(bis[2-(diphenylphosphino)ethyl]amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 50℃; under 7500.75 Torr; for 5h; Schlenk technique; Inert atmosphere; | 98% |
| With sodium tetrahydroborate; sodium methylate In methanol at 25℃; for 3h; Reagent/catalyst; Inert atmosphere; | 98% |
| With 2-(Aminomethyl)pyridine; 1,3-bis-(diphenylphosphino)propane; potassium tert-butylate; hydrogen In 2-methyltetrahydrofuran at 100℃; under 37503.8 Torr; for 16h; Reagent/catalyst; Autoclave; | 95% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide In methanol; water at 240℃; for 2h; Autoclave; Inert atmosphere; | 94% |
| With acetic acid; sodium nitrite Diazotization; |
| Conditions | Yield |
|---|---|
| With C30H34Cl2N2P2Ru; potassium methanolate; hydrogen In tetrahydrofuran at 100℃; under 38002.6 - 76005.1 Torr; for 10h; Glovebox; Autoclave; | 90% |
| With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 4h; | 87.4% |
| With C39H41FeMnN2O5P(1+)*Br(1-); hydrogen; potassium carbonate In ethanol at 90℃; under 37503.8 Torr; for 16h; | 80% |
| Conditions | Yield |
|---|---|
| With methyloxorhenium(V)(2-(mercaptomethyl)thiophenolate) triphenylphosphine; triphenylphosphine In benzene at 20℃; for 1h; | 90% |
| With 1,1,2,2-tetrabutyl-1,2-dichloro distannane In tetrahydrofuran for 1h; Heating; | 85% |
| With gallium In water for 7h; Heating; | 84% |
| Conditions | Yield |
|---|---|
| With [Zn(BH4)2(py)] In tetrahydrofuran for 0.7h; Heating; | 90% |
| Multi-step reaction with 2 steps 1: Et3N / tetrahydrofuran / 0.5 h / 0 °C 2: Tulusion A-27 exchange resin supporting borohydride anion, Ni(OAc)2 / methanol / 1 h / 10 °C View Scheme | |
| Multi-step reaction with 2 steps 1: sulfuric acid 2: aluminum (III) chloride; sodium tetrahydroborate / tetrahydrofuran; toluene / 0 - 5 °C View Scheme |
-
-
23100-12-1
6-chloronicotinylaldehyde
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With hydrogen; sodium acetate; palladium dichloride In methanol at 35℃; under 760.051 Torr; for 2h; | 88% |
-
-
113118-81-3
5-bromopyridine-3-carbaldehyde
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With hydrogen; sodium acetate; palladium dichloride In methanol at 35℃; under 760.051 Torr; for 2h; | 83% |
| Conditions | Yield |
|---|---|
| With TEA; magnesium bromide In dichloromethane at 20℃; for 48h; Cannizzaro reaction; | A 82% B n/a |
| With N,N,N',N'-tetramethylguanidine In water at 20℃; for 7h; Cannizzaro reaction; | A 44% B 41% |
| With barium dihydroxide; formaldehyd at 100 - 110℃; for 0.0333333h; Irradiation; | A 97 % Chromat. B 3 % Chromat. |
| With aluminum oxide; sodium hydroxide; water for 0.00416667h; Irradiation; Yield given; Yields of byproduct given; |
| Conditions | Yield |
|---|---|
| With bromine; isopentyl nitrite In dichloromethane Product distribution / selectivity; | A 81% B 11% C 3% |
| With bromine; isopentyl nitrite In tetrahydrofuran Product distribution / selectivity; | A 79% B 11% C 3% |
| With bromine; isopentyl nitrite In chloroform Product distribution / selectivity; | A 67% B 18% C 3% |
-
-
500-22-1
3-pyridinecarboxaldehyde
-
-
108460-23-7
5-carbamoyl 4,7-dihydro thieno<2,3-b>pyridine
-
A
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With magnesium(II) perchlorate; water In acetonitrile at 65℃; | A 80% B n/a |
| With magnesium(II) perchlorate; water In acetonitrile at 65℃; | A 80% B n/a |
| With magnesium(II) perchlorate; water In acetonitrile at 65℃; Product distribution; water-sensitivity; |
-
-
149806-06-4
6-bromonicotinaldehyde
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With hydrogen; sodium acetate; palladium dichloride In methanol at 35℃; under 760.051 Torr; for 4h; | 78% |
| Conditions | Yield |
|---|---|
| With formaldehyd; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; toluene at 90℃; | A 21% B 74% |
-
-
500-22-1
3-pyridinecarboxaldehyde
-
-
952-92-1
1-Benzyl-1,4-dihydronicotinamide
-
A
-
100-55-0
3-hydroxymethylpyridin
-
B
-
15519-25-2
3-(aminocarbonyl)-1-(phenylmethyl)pyridinium perchlorate
| Conditions | Yield |
|---|---|
| With magnesium(II) perchlorate In acetonitrile at 65℃; | A 70% B n/a |
| With magnesium(II) perchlorate In acetonitrile at 65℃; Product distribution; |
-
-
6968-72-5
3-pyridylcarbinol-N-oxide
-
A
-
500-22-1
3-pyridinecarboxaldehyde
-
B
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate; triethylamine In acetonitrile at 150℃; for 1h; Microwave irradiation; chemoselective reaction; | A 20% B 66% |
| Conditions | Yield |
|---|---|
| With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique; | 63% |
| With {Ru(H)(BH4)(CO)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methyl)propylamine)}; hydrogen In isopropyl alcohol at 150℃; under 37503.8 Torr; for 18h; Autoclave; | 95 %Chromat. |
| With C16H25MnN3O3P(1+)*Br(1-); potassium tert-butylate; hydrogen In tert-Amyl alcohol; cyclohexane at 140℃; under 37503.8 Torr; for 24h; Inert atmosphere; Autoclave; | 55 %Chromat. |
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With sodium hydrogen sulfate; eosin; dihydrogen peroxide In water; acetonitrile for 48h; Irradiation; | 57% |
| Conditions | Yield |
|---|---|
| With sodium carbonate; bis(dibenzylideneacetone)-palladium(0); ruphos In 1,4-dioxane; water for 48h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Reflux; | 51.9% |
| Conditions | Yield |
|---|---|
| With bromine; acetic acid; sodium nitrite In dichloromethane Product distribution / selectivity; | A 44% B 49% |
-
-
6968-72-5
3-pyridylcarbinol-N-oxide
-
-
16420-13-6
N,N-Dimethylthiocarbamoyl chloride
-
A
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| In acetonitrile at 81℃; for 4h; | A 47% B 9% |
-
-
500-22-1
3-pyridinecarboxaldehyde
-
-
6290-49-9
methyl methoxyacetate
-
A
-
100-55-0
3-hydroxymethylpyridin
-
B
-
93-60-7
methyl 3-pyridinecarboxylate
-
C
-
136138-66-4
methyl α-methoxy-β-(β-pyridyl)acrylate
| Conditions | Yield |
|---|---|
| With sodium methylate In toluene for 2h; Heating; | A n/a B 10% C 31% |
-
-
626-60-8
3-Chloropyridine
-
A
-
859842-81-2
3-(pivaloxymethyl)pyridine
-
B
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With potassium phosphate; water; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In 1,4-dioxane at 20 - 100℃; for 14.25h; | A 12% B 14% |
-
-
500-22-1
3-pyridinecarboxaldehyde
-
-
1342295-75-3
Br(1-)*C9H21N2O(1+)
-
A
-
100-55-0
3-hydroxymethylpyridin
-
B
-
59-67-6
nicotinic acid
| Conditions | Yield |
|---|---|
| Stage #1: Br(1-)*C9H21N2O(1+) With sodium hydroxide In dichloromethane; water at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 3-pyridinecarboxaldehyde In dichloromethane; water at 0 - 25℃; for 24h; Inert atmosphere; diastereoselective reaction; | A n/a B n/a C 10% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; palladium on activated charcoal Hydrogenation; |
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With water Zerlegen des entstandenen 3-Oxymethyl-pyridin-pikrats mit Natronlauge; |
| Conditions | Yield |
|---|---|
| With tin(IV) oxide In isopropyl alcohol at 300℃; for 0.5h; | A 5 % Chromat. B 35 % Chromat. |
-
-
77934-69-1
2-Methyl-benzoic acid pyridin-3-ylmethyl ester
-
A
-
118-90-1
ortho-methylbenzoic acid
-
B
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With water in alkaline medium In acetone Rate constant; Ambient temperature; |
| Conditions | Yield |
|---|---|
| With phosphate buffer In water at 65℃; Rate constant; Thermodynamic data; pH 5.17, ΔS, activation energy, other pH, solvent effect; |
-
-
13469-94-8
3-nitrooxymethylpyridine
-
A
-
500-22-1
3-pyridinecarboxaldehyde
-
B
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With sodium methylate In methanol for 3h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
| Conditions | Yield |
|---|---|
| With 10% Ru/C; oxygen In toluene at 90℃; under 760.051 Torr; for 24h; | 100% |
| With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide for 0.25h; Ambient temperature; | 99% |
| With 2,2,6,6-tetramethyl-piperidine-N-oxyl; oxygen; copper(I) bromide dimethylsulfide complex In chlorobenzene at 80℃; for 8h; | 99% |
| Conditions | Yield |
|---|---|
| With thionyl chloride In dichloromethane Reflux; | 100% |
| With thionyl chloride for 0.583333h; Cooling with ice; Reflux; | 72.5% |
| With 1-methyl-pyrrolidin-2-one; benzenesulfonyl chloride In 1,2-dichloro-ethane at 80℃; for 1.5h; | 41% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
222055-82-5
1-(2,2-diethoxyethyl)-4-(imidazol-1-yl)carbonyl-5-aminopyrazole
-
-
222055-89-2
5-amino-1-(2,2-diethoxy-ethyl)-1H-pyrazole-4-carboxylic acid pyridin-3-ylmethyl ester
| Conditions | Yield |
|---|---|
| With sodium hydride In tetrahydrofuran at 0 - 5℃; for 0.166667h; | 100% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
952596-21-3
C25H28N2O5S
| Conditions | Yield |
|---|---|
| With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; | 100% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
953435-15-9
6-methyl 1-pyridin-3-ylmethyl 3,4-dihydroquinoline-1,6(2H)-dicarboxylate
| Conditions | Yield |
|---|---|
| at 20℃; for 8h; | 100% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
760991-59-1
3-iodo-7-methoxy-4,4-dimethyl-1-{[2-(trimethylsilyl)ethoxy]methyl}-1,4-dihydroindeno[1,2-c]pyrazol-6-ol
-
-
760991-63-7
3-iodo-7-methoxy-4,4-dimethyl-6-(pyridin-3-ylmethoxy)-1-{[2-(trimethylsilyl)ethoxy]methyl}-1,4-dihydroindeno[1,2-c]pyrazole
| Conditions | Yield |
|---|---|
| With di-tert-butyl-diazodicarboxylate; Ph3P on solid support In tetrahydrofuran at 20℃; | 100% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 25℃; for 0.05h; Sonication; | 100% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 25℃; for 0.05h; Sonication; | 100% |
-
-
100-55-0
3-hydroxymethylpyridin
| Conditions | Yield |
|---|---|
| With C29H28F6N4OS at 20℃; for 3h; enantioselective reaction; | 100% |
| Conditions | Yield |
|---|---|
| With 4-N,N-dimethylaminopyridinium saccharinate at 25℃; for 0.5h; Inert atmosphere; Neat (no solvent); | 99% |
| With 4-N,N-dimethylaminopyridinium saccharinate In neat (no solvent) at 25℃; for 0.5h; Reagent/catalyst; | 99% |
| With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 99% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
149882-14-4
10,11-(methylenedioxy)-7-(chloromethyl)-(20S)-camptothecin
| Conditions | Yield |
|---|---|
| for 16h; Ambient temperature; | 99% |
| Conditions | Yield |
|---|---|
| Stage #1: 3-hydroxymethylpyridin; methyl iodide at 0℃; for 3h; Stage #2: With silver perchlorate In methanol at 0℃; for 1h; | 99% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
49673-77-0
3-Pyridinecarboxylic acid 3-pyridinylmethyl ester
| Conditions | Yield |
|---|---|
| With iodine; potassium carbonate In tert-butyl alcohol at 20℃; for 19h; | 99% |
| With RuH(CO)Cl(PPh3)(κ2-CP); caesium carbonate In toluene at 110℃; for 26h; Schlenk technique; Glovebox; Inert atmosphere; | 87% |
| With silver(I) hexafluorophosphate; oxygen; palladium diacetate; potassium carbonate; 1,2-bis[di(t-butyl)phosphinomethyl]benzene In toluene at 110℃; under 750.075 Torr; for 20h; chemoselective reaction; | 75% |
| Conditions | Yield |
|---|---|
| Stage #1: 3-hydroxymethylpyridin With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
| With ammonia; oxygen In tert-Amyl alcohol; water at 100℃; under 3750.38 Torr; for 4h; Autoclave; High pressure; | 99% |
| With potassium phosphate; ammonium formate In acetonitrile at 115℃; for 16h; Sealed tube; Green chemistry; | 91% |
| Conditions | Yield |
|---|---|
| With tert-butyldimethylsilyl chloride In methanol; water at 20℃; for 0.5h; Reagent/catalyst; Green chemistry; | 99% |
| With 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy In aq. buffer at 20℃; for 12h; pH=9.8 - 10.1; Electrolysis; | 96% |
| With ferrous(II) sulfate heptahydrate; Oxone In water at 20℃; for 0.5h; Sonication; Green chemistry; | 94% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
185346-79-6
1-(benzyloxy)-4-bromo-3-fluorobenzene
-
-
1355091-47-2
3-[5-(benzyloxy)-2-bromophenoxymethyl]pyridine
| Conditions | Yield |
|---|---|
| Stage #1: 3-hydroxymethylpyridin In 1-methyl-pyrrolidin-2-one; mineral oil at 20℃; for 0.5h; Stage #2: 4-(benzyloxy)-1-bromo-2-fluorobenzene In 1-methyl-pyrrolidin-2-one; mineral oil at 100℃; for 0.5h; | 99% |
| Stage #1: 3-hydroxymethylpyridin With sodium hydride In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h; Stage #2: 4-(benzyloxy)-1-bromo-2-fluorobenzene at 100℃; for 0.25h; |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
98-86-2
acetophenone
-
-
39976-56-2
1-phenyl-3-(pyridin-3-yl)propan-1-one
| Conditions | Yield |
|---|---|
| With titanium(IV) oxide; potassium hydroxide In toluene at 100℃; for 10h; Sealed tube; Irradiation; | 99% |
| With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); caesium carbonate In toluene at 140℃; for 20h; Inert atmosphere; Sealed tube; | 89% |
| With C38H43IrN2PS2(1+)*CF3O3S(1-); caesium carbonate In tert-Amyl alcohol at 120℃; for 24h; Schlenk technique; Inert atmosphere; | 86% |
-
-
462-08-8
pyridin-3-ylamine
-
-
100-55-0
3-hydroxymethylpyridin
-
-
78675-94-2
N-(pyridin-3-ylmethyl)pyridin-3-amine
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 130℃; for 25h; Schlenk technique; Inert atmosphere; | 99% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
74-88-4
methyl iodide
-
-
6457-55-2
3-(Hydroxymethyl)-1-methylpyridinium iodide
| Conditions | Yield |
|---|---|
| In toluene for 1h; Heating; | 98% |
| In dichloromethane at 20℃; for 12h; | 90% |
| Conditions | Yield |
|---|---|
| With TEA In ethyl acetate at 0℃; for 3h; | 98% |
| With triethylamine In dichloromethane at 0 - 25℃; |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
999-97-3
1,1,1,3,3,3-hexamethyl-disilazane
-
-
85719-72-8
3-<(trimethylsilyloxy)methyl>pyridine
| Conditions | Yield |
|---|---|
| With potassium fluoride incorporated on clinoptilolite nanoparticles In dichloromethane at 20℃; for 0.666667h; chemoselective reaction; | 98% |
| With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In acetonitrile at 20℃; for 0.25h; | 90% |
| With polyvinylpolypyrrolidonium tribromide In acetonitrile at 20℃; for 0.25h; | 60% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; sodium hydroxide; sodium chloride; 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide | 98% |
| Stage #1: 3-hydroxymethylpyridin With 1,1'-carbonyldiimidazole In tetrahydrofuran at 10 - 20℃; for 1h; Stage #2: p-aminomethylbenzoic acid With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine In tetrahydrofuran at 20℃; for 5h; Stage #3: With hydrogenchloride; water pH=5; | 91% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
6089-09-4
4-pentynoic acid
-
-
1268158-83-3
2-pyridinylmethyl 4-pentynoate
| Conditions | Yield |
|---|---|
| With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 98% |
| Conditions | Yield |
|---|---|
| With triethylamine In tetrahydrofuran at 0 - 20℃; | 98% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
91-63-4
2-methylquinoline
-
-
21203-10-1
2-(2-(pyridin-3-yl)ethyl)quinolone
| Conditions | Yield |
|---|---|
| With [Mn(HN(C2H4PiPr2)2)(CO)2Br]; potassium tert-butylate In tert-Amyl alcohol at 140℃; for 24h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox; | 98% |
| With cesium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 160℃; for 24h; | 92% |
| With ruthenium(III) chloride trihydrate; potassium tert-butylate In 1,4-dioxane at 130℃; for 24h; Inert atmosphere; | 65% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
98-86-2
acetophenone
-
-
4452-13-5
1-phenyl-3-(pyridin-3-yl)prop-2-en-1-one
| Conditions | Yield |
|---|---|
| With titanium nitride; potassium hydroxide In toluene at 100℃; for 10h; Sealed tube; Irradiation; | 98% |
-
-
100-55-0
3-hydroxymethylpyridin
-
-
1670-14-0
benzamidine monohydrochloride
-
-
1596320-79-4
2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine
| Conditions | Yield |
|---|---|
| With oxygen; copper(II) acetate monohydrate; sodium carbonate In toluene at 110℃; for 24h; | 97% |
| With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium); caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 20 - 110℃; for 20h; Reagent/catalyst; Solvent; | 81% |
| With [RhCl2(p-cymene)]2; caesium carbonate In dimethyl sulfoxide at 110℃; for 16h; Sealed tube; | 78% |
| Stage #1: 3-hydroxymethylpyridin; benzamidine monohydrochloride With caesium carbonate In dimethyl sulfoxide at 20℃; for 0.0833333h; Schlenk technique; Green chemistry; Stage #2: With N-iodo-succinimide In dimethyl sulfoxide at 100℃; for 16h; Schlenk technique; Green chemistry; | 72% |
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