Simagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:462-08-8
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:462-08-8
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Manufacturers
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Hefei TNJ chemical industry co.,ltd
Specifications Aminopyridine 1.Name:3-Aminopyridine 2.CAS:462-08-8 3.Assay:99.3% 4.Competitive price and high quality Appearance:light yellow solid Package:25kg/drum or as your needs Application:Fine Chemical Intermediate Transportation:b
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:462-08-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryChemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
TIANFUCHEM--462-08-8--3-Aminopyridine in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationship
Cas:462-08-8
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryLIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:462-08-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
CAS: 462-08-8 EINCES: 207-322-2 Other name: 3-Aminopyridine Molecular formula: C5H6N2 Molecular weight: 94.11450 Melting point: 248 °C(lit.) Density: 1.107g/cm3 Appearance: yellowish to brown solid Storage: Store in cool and dry pla
Hubei Langyou International Trading Co., Ltd
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best serv
Baoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At pres
Cas:462-08-8
Min.Order:1 Kilogram
FOB Price: $28.0 / 31.0
Type:Trading Company
inquiryWuhan Zenuo Biological Medicine Technology Co Ltd
Product Name: 3-Aminopyridine Synonyms: Alogliptin Impurity 40;3-amino-pyridin;3-Aminopyridine ,98%;3-mydroxypiperidine;AMINOPYRIDINE, 3-(RG);462-08-0;3-Aminopyridine,3-Pyridinamine;3-aminepyridin CAS: 462-08-8 MF: C5H6N2 MW: 94.11 EINECS
Cas:462-08-8
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:462-08-8
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Shanghai Massive Chemical Technology Co., Ltd.
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:462-08-8
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:462-08-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:462-08-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Fandachem Co.,Ltd
Hangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting 3-Aminopyridine (3-Pyridinamine;beta-Aminopyridine),CAS:462-08-8, Please contact us by email freely. We are leading exporter in China. If you really ne
Cas:462-08-8
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryHangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:white to light yellow crystal powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Interme
Hubei Vanz Pharm Co.,Ltd
ISO Factory/Good qualityAppearance:off white Storage:dry and cool place Package:10G/BAG; 1KG/BAG ;25KG/DRUM Application:Active pharaceutical ingredients Transportation:BY SEA,AIR,EXPRESS Port:SHANGHAI;BEIJING
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Synthetic route
| Conditions | Yield |
|---|---|
| With hydrogen In ethyl acetate at 20℃; under 7600.51 Torr; for 6h; Autoclave; | 99% |
| With 0.2C27H36N2*Pt; hydrogen In tetrahydrofuran at 60℃; under 3000.3 Torr; for 5h; chemoselective reaction; | 99% |
| With hydrogen In ethyl acetate under 760.051 Torr; for 2h; Heating; Flow reactor; Green chemistry; | 99% |
| Conditions | Yield |
|---|---|
| With cyclohexa-1,4-diene; 5%-palladium/activated carbon In methanol at 120℃; for 0.0833333h; Microwave irradiation; | 99% |
| With palladium 10% on activated carbon; hydrazine hydrate In methanol at 120℃; for 0.25h; Microwave irradiation; | 89% |
| With ethanol; palladium Hydrogenation; |
| Conditions | Yield |
|---|---|
| With cyclohexa-1,4-diene; 5%-palladium/activated carbon In methanol at 120℃; for 0.0833333h; Microwave irradiation; | 99% |
| With hydrazine hydrate In ethanol at 70℃; for 4h; chemoselective reaction; | 95% |
| With palladium 10% on activated carbon; hydrazine hydrate In methanol at 120℃; for 0.25h; Microwave irradiation; | 84% |
| With palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate In methanol at 20℃; under 760.051 Torr; for 2h; Sealed tube; chemoselective reaction; | 100 %Spectr. |
| Conditions | Yield |
|---|---|
| With sodium hypochlorite In water at 0 - 5℃; | 94.1% |
| With sodium hypochlorite at 5 - 10℃; Temperature; | 92.3% |
| With sodium hydroxide; bromine r.t., 30 min.; then 65-75 deg C, 2 h; | 62% |
| Conditions | Yield |
|---|---|
| With titanium tetrachloride; tin(ll) chloride In diethyl ether for 0.5h; Ambient temperature; | 94% |
| Conditions | Yield |
|---|---|
| With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 6h; | 94% |
| With ammonium hydroxide; potassium phosphate In dimethyl sulfoxide at 80℃; UV-irradiation; | 94% |
| With C46H71Cl3N2Pd; ammonia; sodium t-butanolate In 1,4-dioxane at 100℃; for 16h; Inert atmosphere; Schlenk technique; | 88% |
| Conditions | Yield |
|---|---|
| With iron(III) oxide; sodium hydroxide; copper(l) iodide; ammonia In ethanol; water at 90℃; for 16h; | 94% |
| With [N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; ammonia; sodium hydroxide In water at 120℃; for 12h; sealed tube; | 94% |
| With copper(I) oxide; ammonium hydroxide; C17H14N2O3; potassium hydroxide In ethanol at 60℃; for 24h; Schlenk technique; Inert atmosphere; | 93% |
| Conditions | Yield |
|---|---|
| With sodium hypochlorite; sodium hydroxide In water at 5 - 20℃; Temperature; | 93.8% |
| Multi-step reaction with 2 steps 1: manganese(IV) oxide / ethanol; water / 6 h / 85 °C 2: sodium hydroxide; sodium hypochlorite / 6 h / 90 °C View Scheme |
| Conditions | Yield |
|---|---|
| With [N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; ammonia; sodium hydroxide In water at 120℃; for 12h; sealed tube; | 93% |
| Stage #1: 3-Bromopyridine With copper(l) iodide; potassium carbonate; L-proline In dimethyl sulfoxide Inert atmosphere; Stage #2: With ammonium hydroxide In dimethyl sulfoxide at 90℃; for 12h; Inert atmosphere; | 93% |
| With oxalic acid hydrazide; ammonium hydroxide; tetrabutylammomium bromide; potassium carbonate; 2,5-hexanedione; copper(II) oxide In water at 90℃; for 1.33333h; | 90% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(pyridin-3-yl)acetamide With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.05h; Inert atmosphere; Stage #2: With water In tetrahydrofuran Inert atmosphere; | 89% |
| Conditions | Yield |
|---|---|
| With hydrogen In water; toluene at 50℃; under 4500.45 Torr; for 5h; Reagent/catalyst; | A 11.5% B 88.5% |
| With 1% platinum on charcoal; hydrogen; sodium carbonate In water; toluene at 50℃; under 4500.45 Torr; for 5h; Catalytic behavior; Reagent/catalyst; | |
| With hydrogen; NE-01M02; sodium carbonate In water; toluene at 50℃; under 4500.45 Torr; for 5h; Catalytic behavior; Reagent/catalyst; | |
| With platinum on activated charcoal; hydrogen; sodium carbonate In water; toluene at 50℃; under 4500.45 Torr; for 5h; Reagent/catalyst; |
-
-
10296-29-4
3-azidopyridine
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With iron In water at 20℃; Inert atmosphere; | 88% |
-
-
63458-55-9
N-monochloronicotinamide
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| Stage #1: N-monochloronicotinamide In water at 90℃; for 1.5h; Stage #2: With hydrogenchloride In water at 15 - 50℃; Product distribution / selectivity; | 86% |
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With ammonium sulfate; bis(1,5-cyclooctadiene)nickel (0); sodium t-butanolate at 100 - 110℃; for 12h; | 85% |
-
-
170839-31-3
benzyl N-(pyridin-3-yl)carbamate
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 0.25h; chemoselective reaction; | 78% |
| With hydrogenchloride; water |
| Conditions | Yield |
|---|---|
| With copper(ll) sulfate pentahydrate; potassium phosphate tribasic heptahydrate; water; Sucrose In water at 90℃; for 15h; Catalytic behavior; Green chemistry; | 75% |
-
-
1462-86-8
3-amino-pyridine-2-carboxylic acid
-
-
87-13-8
diethyl 2-ethoxymethylenemalonate
-
A
-
462-08-8
pyridin-3-ylamine
-
B
-
14029-71-1
2-(pyridin-3-yl)aminomethylene-malonic acid diethyl ester
| Conditions | Yield |
|---|---|
| at 140 - 150℃; for 12h; | A n/a B 63% |
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With methanesulfonic acid; palladium on activated charcoal In ethanol Heating; | 63% |
-
-
25604-13-1
succinic acid 3-pyridylmonoamide
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With ammonium peroxydisulfate; silver nitrate; trifluoroacetic acid In water at 70℃; for 6h; | 60% |
-
-
18364-47-1
N-methyl-N-(3-pyridyl)amine
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With piperidine; dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In acetonitrile at -78℃; for 72h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; | 60% |
-
-
56700-70-0
3-(tert-butoxycarbonylamino)pyridine
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With silica gel In dichloromethane for 0.05h; Irradiation; | 56% |
-
-
4122-56-9
methyl o-formylbenzoate
-
-
157562-24-8
3-aminopicolinic acid trimethylsilyl ester
-
A
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| In xylene at 140 - 145℃; for 18h; | A 49% B 50% |
-
-
1462-86-8
3-amino-pyridine-2-carboxylic acid
-
-
611-10-9
2-ethoxycarbonyl-1-cyclopentanone
-
A
-
462-08-8
pyridin-3-ylamine
-
B
-
61319-84-4
ethyl 2-(3-pyridylamino)-1-cyclopentene-1-carboxylate
| Conditions | Yield |
|---|---|
| at 150℃; for 20h; | A n/a B 50% C 13% D 36% |
-
-
157562-25-9
3-(3-oxobutylamido)picolinic acid
-
A
-
462-08-8
pyridin-3-ylamine
-
B
-
39642-60-9
N,N′-bis(m-pyridyl)urea
| Conditions | Yield |
|---|---|
| In 1,3,5-trimethyl-benzene at 160℃; for 15h; | A 47% B 47% |
| Conditions | Yield |
|---|---|
| With ammonium peroxydisulfate; silver nitrate; trifluoroacetic acid In water at 70℃; for 6h; | A 40% B 45% |
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; 5%-palladium/activated carbon; hydrazine hydrate; lithium hydroxide In 1,4-dioxane at 170℃; for 16h; Molecular sieve; Inert atmosphere; | 45% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; cesium acetate In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | A 17% B 42% |
| Conditions | Yield |
|---|---|
| Stage #1: pyridin-3-ylamine With sulfuric acid at 20℃; Cooling with ice; Stage #2: With sodium nitrite In water Reflux; | 100% |
| With sulfuric acid Diazotization; | |
| With sulfuric acid; water; sodium nitrite at 0℃; Erwaermen des Reaktionsgemisches auf 50grad; | |
| With sulfuric acid; water; sodium nitrite at 0℃; Erwaermen des Reaktionsgemisches auf 80grad.; |
-
-
462-08-8
pyridin-3-ylamine
-
-
116-11-0
2-Methoxypropene
-
-
32405-72-4
3-Pyridinyl(1-methylethylidene)amine
| Conditions | Yield |
|---|---|
| With pyridinium p-toluenesulfonate; triethylamine In chloroform at 100℃; for 9h; | 100% |
-
-
462-08-8
pyridin-3-ylamine
-
-
42166-50-7
3-hydrazinopyridine
| Conditions | Yield |
|---|---|
| Stage #1: pyridin-3-ylamine With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 0.583333h; Stage #2: With hydrogenchloride; tin(ll) chloride In water at 0 - 10℃; for 1.5h; | 100% |
| Stage #1: pyridin-3-ylamine With hydrogenchloride; sodium nitrite In water at 5℃; for 0.75h; Stage #2: With hydrogenchloride; tin(ll) chloride In water at 0 - 10℃; for 1.5h; Stage #3: With sodium hydroxide In water at 0 - 10℃; Product distribution / selectivity; | 83% |
| Stage #1: pyridin-3-ylamine With hydrogenchloride; sodium nitrite In water for 0.75h; Stage #2: With tin(ll) chloride In water at 5℃; for 1.5h; Stage #3: With sodium hydroxide In water | 83% |
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| With fluorosilicic acid In methanol | 100% |
| Conditions | Yield |
|---|---|
| at 200℃; for 0.05h; | 100% |
-
-
462-08-8
pyridin-3-ylamine
-
-
874298-19-8
4-(3-pyridyl)ureido-phenylboronic acid pinacol ester
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; toluene at 20℃; for 2.5h; | 100% |
| In tetrahydrofuran at 20℃; for 6h; | 94.3% |
| In tetrahydrofuran at 20℃; for 6h; | 94.3% |
| In tetrahydrofuran; toluene at 20℃; for 16h; | 93% |
| In 1,2-dimethoxyethane |
-
-
462-08-8
pyridin-3-ylamine
-
-
17823-69-7
2-cyano-3,3-bis(methylthio)acrylamide
-
-
1456732-10-7
2-cyano-3-(methylthio)-3-(pyridin-3-ylamino)acrylamide
| Conditions | Yield |
|---|---|
| In ethanol at 75℃; for 18h; | 100% |
-
-
462-08-8
pyridin-3-ylamine
-
-
24801-88-5
3-(triethoxypropyl) isocyanate
| Conditions | Yield |
|---|---|
| In dichloromethane at 20℃; for 48h; | 100% |
| Conditions | Yield |
|---|---|
| In dichloromethane at 20℃; | 100% |
-
-
462-08-8
pyridin-3-ylamine
-
-
1238056-80-8
pentafluorophenyl indirubin-5-carboxylate
-
-
1238056-92-2
5-[N-(pyridin-3-yl)aminocarbonyl]indirubin
| Conditions | Yield |
|---|---|
| With dmap In 1,4-dioxane Inert atmosphere; Reflux; | 99.9% |
| Conditions | Yield |
|---|---|
| In acetonitrile at 100℃; for 0.833333h; Microwave irradiation; | 99.4% |
| Conditions | Yield |
|---|---|
| With triethylamine In tetrahydrofuran; diethyl ether for 1h; Ambient temperature; | 99% |
| 96% | |
| With pyridine; dmap In dichloromethane at 0℃; for 2h; Temperature; Concentration; | 95.5% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at -20℃; for 0.25h; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
623-00-7
4-bromobenzenecarbonitrile
-
-
189100-30-9
4-(pyridin-3-ylamino)benzonitrile
| Conditions | Yield |
|---|---|
| With sodium phenoxide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 170℃; for 2h; microwave irradiation; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
196314-83-7
1-(isocyanatoethyl)-1,2-closo-dodecaborane
-
-
196314-53-1
1-((3'-pyridinylcarbamido)ethyl)-o-carborane
| Conditions | Yield |
|---|---|
| In acetonitrile absence of air and moisture; equimolar amts., stirring at room temp. up to 24 h; solvent removal, recrystn. or chromy. (not specified); | 99% |
| Conditions | Yield |
|---|---|
| With 3,5-Lutidine In dichloromethane at 25℃; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
1311568-99-6
1-{3-[(tert-butoxycarbonyl)amino]propyl}-2-(trimethoxymethyl)-1H-benzimidazole-6-carboxylic acid
-
-
1311569-35-3
tert-butyl {3-[6-(pyridin-3-ylcarbamoyl)-2-(trimethoxymethyl)-1H-benzimidazol-1-yl]propyl}carbamate
| Conditions | Yield |
|---|---|
| Stage #1: 1-{3-[(tert-butoxycarbonyl)amino]propyl}-2-(trimethoxymethyl)-1H-benzimidazole-6-carboxylic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate In N,N-dimethyl-formamide for 0.166667h; Stage #2: pyridin-3-ylamine With triethylamine In N,N-dimethyl-formamide at 45℃; for 20h; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
100-55-0
3-hydroxymethylpyridin
-
-
78675-94-2
N-(pyridin-3-ylmethyl)pyridin-3-amine
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 130℃; for 25h; Schlenk technique; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 130℃; for 25h; Schlenk technique; Inert atmosphere; | 99% |
| With potassium tert-butylate; benzonitrile In 1,4-dioxane at 120℃; for 15h; Inert atmosphere; Glovebox; Sealed tube; | 82% |
| With samarium diiodide; potassium tert-butylate In tetrahydrofuran; toluene at 140℃; for 1h; Microwave irradiation; Inert atmosphere; | 78% |
| With [(NH-C3H5)Tr(NHP(iPr)2)2CoCl2]; potassium tert-butylate In toluene at 80℃; for 24h; | 61% |
-
-
462-08-8
pyridin-3-ylamine
-
-
73831-13-7
4-cyano-3-methylbenzoic acid
| Conditions | Yield |
|---|---|
| Stage #1: 4-cyano-3-methylbenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide In tetrahydrofuran at 20 - 66℃; for 3h; Stage #2: pyridin-3-ylamine With pyridine at 20℃; for 16h; | 99% |
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 24h; | 99% |
| Conditions | Yield |
|---|---|
| With [COD(Pd-AlPhos)2]; 1,8-diazabicyclo[5.4.0]undec-7-ene In tert-butyl methyl ether at 20℃; for 3h; Reagent/catalyst; Inert atmosphere; Sealed tube; Schlenk technique; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
55162-34-0
1-bromo-4-(2-chloroethoxy)benzene
| Conditions | Yield |
|---|---|
| With [COD(Pd-AlPhos)2]; 1,8-diazabicyclo[5.4.0]undec-7-ene In tert-butyl methyl ether at 20℃; for 3h; Inert atmosphere; Sealed tube; Schlenk technique; | 99% |
-
-
462-08-8
pyridin-3-ylamine
| Conditions | Yield |
|---|---|
| Stage #1: 4-(4-(4-(4-(((6aS)-5-((allyloxy)carbonyl)-2-methoxy-12-oxo-6-((tetrahydro-2H-pyran-2-yl)oxy)-5,6,6a,7,8,9,10,12-octahydrobenzo[e]pyrido[1,2-a][1,4] diazepin-3-yl)oxy)butanamido)-1-methyl-1H-pyrrole-2- carboxamido)phenyl)-1-methyl-1H-pyrrole-2-carboxylic acid With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 0.25h; Stage #2: pyridin-3-ylamine In dichloromethane at 20℃; for 16h; | 99% |
-
-
462-08-8
pyridin-3-ylamine
-
-
87-13-8
diethyl 2-ethoxymethylenemalonate
-
-
14029-71-1
2-(pyridin-3-yl)aminomethylene-malonic acid diethyl ester
| Conditions | Yield |
|---|---|
| at 150℃; | 98% |
| In ethanol Reflux; | 97% |
| In ethanol for 24h; Reflux; | 96% |
-
-
462-08-8
pyridin-3-ylamine
-
-
1943-83-5
2-chloroethyl isothiocyanate
-
-
13908-58-2
1-(2-chloro-ethyl)-3-pyridin-3-yl-urea
| Conditions | Yield |
|---|---|
| In toluene at 0 - 20℃; for 5.5h; | 98% |
| In toluene at 0 - 20℃; for 5.5h; | 98% |
| In tetrahydrofuran for 1.5h; Ambient temperature; | 81% |
-
-
462-08-8
pyridin-3-ylamine
-
-
79-04-9
chloroacetyl chloride
-
-
78205-18-2
2-chloro-N-(pyridine-3-yl)acetamide
| Conditions | Yield |
|---|---|
| In acetone at 0℃; | 98% |
| With triethylamine In dichloromethane at 0 - 20℃; | 83% |
| With sodium hydroxide In water at 20℃; | 48% |
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