Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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Cas:91-63-4
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Cas:91-63-4
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
CAS No.91-63-4 Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scien
Cas:91-63-4
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inquiryProduct Name: Quinaldine Synonyms: 2-Methylchinolin;2-Methylpuinoiline;QUINALDINE MINIMUM 90% (GC);QUINALDINE 98+%;QUINALDINE MIN 96%;Quinaldine,~91%;Quinaldine97%;2- Methyl Quinoline (Quinaldine)
Cas:91-63-4
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry plac
Cas:91-63-4
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:91-63-4
Min.Order:10 Gram
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:91-63-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirymoderate price & quick delivery Appearance:yellowish-brown liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Increased alkali agent used
Product name: 2-Quinaldine CAS No.:91-63-4 Molecule Formula:C10H9N Molecule Weight:143.19 Purity: 80%, 85% or 87% Package: 200kg/drum Description:Yellow brown oily liquid Manufacture Standards:Enterprise Standard T
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
stable supply&competitive price Storage:Available Package:25KG Or as client requirement Application:Important pharm intermediate Transportation:By air or By sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:91-63-4
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
QuinaldineAppearance:yellow liquid Package:200kg/barrel Application:intermediate Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
in storeAppearance:Colorless - very pale yellow transparent liquid Package:100g Application:Organic Chemicals
Conditions | Yield |
---|---|
In benzene Ambient temperature; Irradiation; | A 100% B 100% |
Conditions | Yield |
---|---|
In benzene Ambient temperature; Irradiation; | A 100% B 100% |
2-methyl-1,2,3,4-tetrahydroquinolin-4-yl-(phenyl)amine
A
2-methylquinoline
B
aniline
Conditions | Yield |
---|---|
With palladium dichloride In acetonitrile | A 100% B 100% |
Conditions | Yield |
---|---|
Stage #1: 2-methyl-1,2-dihydroquinoline With sodium hydroxide In ethanol at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Irradiation; Stage #2: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; chloropyridinecobaloxime(III) In ethanol at 20℃; for 1h; | 99% |
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; Co(dmgH)2(4-MeCO2Py)Cl In water at 28℃; for 4h; Mechanism; Schlenk technique; Inert atmosphere; Irradiation; | 91% |
With arsenic(V) oxide | |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; iodine; (S)-(-)-(6,6’-dimethoxybiphenyl-2,2’-diyl)bis(diphenylphosphine) In toluene at 20℃; | |
With rose bengal; oxygen; potassium carbonate In N,N-dimethyl acetamide at 20℃; for 12h; Irradiation; |
Conditions | Yield |
---|---|
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; chloropyridinecobaloxime(III) In ethanol at 30℃; for 6h; Reagent/catalyst; Solvent; Schlenk technique; Inert atmosphere; Irradiation; | 99% |
With 6C44H32N6O4Ru(2+)*12Hf(2+)*8O(2-)*14HO(1-)*6C16H22ClCoN5O6(1-) In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 24h; Catalytic behavior; Inert atmosphere; Irradiation; | 99% |
With isolated cobalt single atom sites stabilized on an ordered porous nitrogen doped carbon matrix In 1,3,5-trimethyl-benzene at 120℃; for 8h; Schlenk technique; | 96% |
(E)-4-(2-aminophenyl)but-3-en-2-one
2-methylquinoline
Conditions | Yield |
---|---|
In tetrahydrofuran for 12h; Irradiation; | 99% |
In ethanol at 30℃; Concentration; Solvent; UV-irradiation; Flow reactor; | 91% |
In benzene for 0.366667h; Irradiation; | 74% |
Conditions | Yield |
---|---|
With methylene chloride; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide electrolysis, -2.0 V; | 90% |
1,1,2,2-Tetraphenyl-ethane-1,2-diol; compound with 2-methyl-quinoline
2-methylquinoline
Conditions | Yield |
---|---|
at 120℃; under 5 Torr; | 90% |
Conditions | Yield |
---|---|
With phospho-tungstic acid; phosphotungstic acid; silica gel for 0.166667h; Doebner-Miller reaction; microwave irradiation; | 90% |
With hydrogenchloride; chloranil In butan-1-ol for 0.333333h; Heating; |
Conditions | Yield |
---|---|
With 4 A molecular sieve; tin(ll) chloride; zinc(II) chloride In ethanol at 70℃; | 90% |
Stage #1: acetone; 2-nitro-benzaldehyde With zinc(II) chloride In methanol at 67℃; for 1h; Inert atmosphere; Molecular sieve; Stage #2: With tin(ll) chloride In methanol for 12h; Inert atmosphere; Molecular sieve; | 90% |
With Li*4.5 THF In methanol at 20 - 25℃; for 63h; | 77% |
β-anilinocrotonaldehyde
2-methylquinoline
Conditions | Yield |
---|---|
With sulfuric acid for 48h; Ambient temperature; | 89% |
With sulfuric acid at 25℃; Rate constant; |
4-phenyl-2-butanone oxime
A
2-methylquinoline
B
methyl-N-(benzyl-methyl)-formamide
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; tetrabutylammonium perrhenate In nitromethane Heating; | A 7% B 88% |
Conditions | Yield |
---|---|
With N-hydroxy-3,4,5,6-tetrachlorophthalimide; 5,6-bis(5-methoxythiophen-2-yl)pyrazine-2,3-dicarbonitrile In acetonitrile at 25℃; for 5h; Irradiation; Green chemistry; | 88% |
With 5,6-bis(5-methoxythiophen-2-yl)pyrazine-2,3-dicarbonitrile; C9H3Cl4NO2 In N,N-dimethyl acetamide; acetonitrile at 25℃; for 3h; Solvent; Irradiation; | 81% |
ethanol
carbon monoxide
aniline
A
2-methylquinoline
B
N-carboethoxyaniline
C
bis(diphenyl)urea
Conditions | Yield |
---|---|
With oxygen; rhodium contaminated with carbon at 160 - 170℃; under 63253.7 Torr; for 3h; Mechanism; Product distribution; further catalyst systems; other amines; | A n/a B 86% C 1.5% |
Conditions | Yield |
---|---|
With copper(I) bromide In tetrahydrofuran; diethyl ether 1.) -78 degC, 3h, 2.) RT, overnight; | 85% |
With copper(I) bromide In tetrahydrofuran at -78 - 20℃; Product distribution; other heteroaryl halides and cuprous salts as catalysts; | 85% |
Stage #1: methylmagnesium bromide With iron(III) trifluoride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0℃; Inert atmosphere; Stage #2: 2-Chloroquinoline In tetrahydrofuran at 20 - 60℃; for 26h; Inert atmosphere; | 40% |
Stage #1: methylmagnesium bromide With iron(III) trifluoride; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In tetrahydrofuran at 0℃; Inert atmosphere; Stage #2: 2-Chloroquinoline In tetrahydrofuran at 60℃; for 26h; Inert atmosphere; chemoselective reaction; | 40% |
Quinoline N-oxide
4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane
2-methylquinoline
Conditions | Yield |
---|---|
With sodium methylate In toluene at 80℃; for 3h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; regioselective reaction; | 85% |
4-(2-aminophenyl)-2-butanol
A
2-methylquinoline
B
1,2,3,4-tetrahydro-2-methylquinoline
Conditions | Yield |
---|---|
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium carbonate In toluene at 111℃; for 20h; | A 9% B 83% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; tert-butylmagnesium chloride In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere; | 82% |
With hydrogen iodide; acetic acid at 250 - 270℃; |
1-(2'-Acetamino-phenyl)-ethanol
2-methylquinoline
Conditions | Yield |
---|---|
With PPA at 210℃; for 20h; | 82% |
N-[2-((E)-3-Oxo-but-1-enyl)-phenyl]-acetamide
2-methylquinoline
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; [RhCl2(p-cymene)]2; copper(II) acetate monohydrate; acetic acid In tetrahydrofuran at 120℃; for 12h; Inert atmosphere; Sealed tube; | 81% |
With hydrogenchloride for 0.05h; Heating; | 93 mg |
Conditions | Yield |
---|---|
With silver tetrafluoroborate; oxygen; palladium diacetate; Trimethylacetic acid at 180℃; for 24h; Temperature; Reagent/catalyst; | 81% |
With gold on titanium oxide for 5h; Irradiation; | 75% |
With titania-supported iridium nanoclusters at 120℃; under 3800.26 Torr; for 28h; Autoclave; Inert atmosphere; | 74% |
With MoS1.73O0.1 at 190℃; for 4h; Reagent/catalyst; | 72% |
Stage #1: ethanol; nitrobenzene With MoS1.73O0.1; hydrogen In toluene at 160℃; for 8h; Stage #2: In toluene at 150℃; for 6h; Temperature; Solvent; Reagent/catalyst; | 70% |
Conditions | Yield |
---|---|
With [1-butyl-2,3-dimethylimidazolium][tppm] stabilized rhodium nanoarticles at 50℃; under 22502.3 Torr; for 5h; Ionic liquid; Autoclave; chemoselective reaction; | 100% |
With hydrogen at 50℃; under 22502.3 Torr; for 10h; Autoclave; Sealed tube; Ionic liquid; chemoselective reaction; | 100% |
With [2,2]bipyridinyl; formic acid; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium formate In water at 80℃; for 1h; pH=3.5; | 99% |
2-methylquinoline
formamide
2-methylquinoline-4-carboxamide
Conditions | Yield |
---|---|
With sulfuric acid; dihydrogen peroxide; titanium(IV) oxide for 5h; sunlight irradiation; | 100% |
With sulfuric acid; dihydrogen peroxide; iron(II) sulfate at 60℃; for 4h; | 100 % Turnov. |
With N-hydroxyphthalimide; ammonium cerium(IV) nitrate; trifluoroacetic acid at 70℃; for 6h; |
Conditions | Yield |
---|---|
With acetic anhydride for 6h; Reflux; | 100% |
With acetic anhydride for 6h; Reflux; | 100% |
2-methylquinoline
4-nitrobenzaldehdye
A
4-nitrobenzyl chloride
B
1,2,3,4-tetrahydro-2-methylquinoline
Conditions | Yield |
---|---|
With (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen In toluene at 80℃; for 18h; | A 100% B 78% |
2-methylquinoline
p-formylacetophenone
A
4-(hydroxymethyl)acetophenone
B
1,2,3,4-tetrahydro-2-methylquinoline
Conditions | Yield |
---|---|
With (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen In toluene at 80℃; for 18h; | A 100% B 100% |
Conditions | Yield |
---|---|
Stage #1: chromium(VI) oxide; hydrogen fluoride In water Stage #2: 2-methylquinoline In water for 1h; | 99.4% |
2-methylquinoline
formic acid
2-methyl-3,4-dihydroquinoline-1(2H)-carbaldehyde
Conditions | Yield |
---|---|
With nitrogen modified cobalt nanoparticles supported on carbon In toluene at 130℃; | 99% |
With isolated cobalt single atom sites stabilized on an ordered porous nitrogen doped carbon matrix In toluene at 120℃; for 1.5h; Schlenk technique; | 96% |
With sodium formate In water at 80℃; for 24h; pH=4.5; Schlenk technique; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With iron(II) acetate; trifluoroacetic acid In toluene at 100℃; for 24h; Inert atmosphere; Schlenk technique; Green chemistry; | 99% |
In water at 120℃; for 36h; Sealed tube; | 94% |
In 1,4-dioxane at 140℃; for 48h; Autoclave; Green chemistry; | 89% |
With zinc(II) chloride |
2-methylquinoline
3-nitro-benzaldehyde
3-[2-(quinolin-2-yl)ethenyl]nitrobenzene
Conditions | Yield |
---|---|
With lanthanum pentafluorobenzoate In toluene at 120℃; for 24h; | 99% |
With iron(II) acetate; trifluoroacetic acid In toluene at 100℃; for 24h; Inert atmosphere; Schlenk technique; Green chemistry; | 90% |
With acetic anhydride In water | 88% |
2-methylquinoline
4-nitrobenzaldehdye
2-[(E)-2-(4-nitrophenyl)ethenyl]quinoline
Conditions | Yield |
---|---|
With lanthanum pentafluorobenzoate In toluene at 120℃; for 24h; | 99% |
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 98% |
With iron(II) acetate; trifluoroacetic acid In toluene at 100℃; for 24h; Inert atmosphere; Schlenk technique; Green chemistry; | 92% |
2-methylquinoline
(R)-1,2,3,4-tetrahydroquinaldine
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-(+)-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine; hydrogen; iodine In tetrahydrofuran at 20℃; under 36201.3 Torr; for 24h; Autoclave; optical yield given as %ee; enantioselective reaction; | 99% |
With (R)-(-)-5,5’-bis(diphenyl;phosphine)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; bis(1,5-cyclooctadiene)diiridium(I) dichloride; hydrogen; iodine In tetrahydrofuran at 20℃; under 36201.3 Torr; for 24h; Autoclave; optical yield given as %ee; enantioselective reaction; | 99% |
With C34H39F3N2O5RuS2; hydrogen In methanol at 25℃; under 38002.6 Torr; for 14h; Autoclave; optical yield given as %ee; enantioselective reaction; | 99% |
2-methylquinoline
chromium(0) hexacarbonyl
pentacarbonyl(η(1)-quinaldine)chromium(0)
Conditions | Yield |
---|---|
In tetrahydrofuran; dibutyl ether Ar-atmosphere; heating equimolar amts. to 130°C for 9 h (in Bu2O/THF=10:1); cooling to room temp., filtration (Celite), evapn.; | 99% |
In tetrahydrofuran Irradiation (UV/VIS); Ar-atmosphere; irradiation of Cr-complex soln. (Hg lamp, λ=253 nm, room temp., 80 h), stirring with excess of ligand (room temp., 24 h); evapn. (vac.); | 60% |
2-methylquinoline
trans-chloromethylbis(dimethylsulfoxide)platinum(II)
trans(C,N)-chloromethyl(dimethyl sulfoxide)(2-methylquinoline)platinum(II)
Conditions | Yield |
---|---|
In dichloromethane stirring stoich. amts. for 30 min; addn. of pentane, pptn. on cooling, collection (filtration), washing (cold pentane), drying (vac.); elem. anal.; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2-methylquinoline With lithium diisopropyl amide In tetrahydrofuran; hexane at -70℃; for 1h; Stage #2: 4-Cyanochlorobenzene In tetrahydrofuran; hexane at -70 - 20℃; for 2h; Further stages.; | 99% |
2-methylquinoline
(S)-2-methyl-1,2,3,4-tetrahydroquinoline
Conditions | Yield |
---|---|
With C32H34F6IrN2O5S2; hydrogen; trifluoroacetic acid In methanol at 15℃; under 38002.6 Torr; for 24h; optical yield given as %ee; enantioselective reaction; | 99% |
With Ru(trifluoromethanesulfonate)(N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine)(η6-cymene); hydrogen at 25℃; under 38002.6 Torr; Autoclave; Neat (no solvent); optical yield given as %ee; enantioselective reaction; | 99% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (S)-6,6'-bis(diphenylphosphino)-1,1'-biphenyl-2,2'-diylbis(trifluoromethylsulfonate); hydrogen; iodine In tetrahydrofuran at 20℃; under 36201.3 Torr; for 22h; Inert atmosphere; Autoclave; optical yield given as %ee; enantioselective reaction; | 99% |
4-Cyanochlorobenzene
2-methylquinoline
2-(quinolin-2-yl)-1-(4-chlorophenyl)-1-ethenamine
Conditions | Yield |
---|---|
Stage #1: 2-methylquinoline With n-butyllithium; diisopropylamine In tetrahydrofuran at -70℃; for 1h; Inert atmosphere; Stage #2: 4-Cyanochlorobenzene In tetrahydrofuran at -70 - 20℃; Inert atmosphere; Stage #3: With water In tetrahydrofuran | 99% |
2-methylquinoline
1,1,1-trifluoroacetophenone
1,1,1-trifluoro-2-phenyl-3-(quinolin-2-yl)propan-2-ol
Conditions | Yield |
---|---|
With indium(III) chloride In tert-butyl alcohol at 60℃; for 24h; Reagent/catalyst; Solvent; | 99% |
With iron(II) perchlorate monohydrate In dimethyl sulfoxide at 60℃; for 24h; Catalytic behavior; Solvent; Temperature; Sealed tube; | 93% |
With ytterbium(III) triflate In 1,4-dioxane at 110℃; for 12h; | 90% |
2-methylquinoline
N-(p-chlorobenzyl)aniline
(E)-2-(4-chlorostyryl)quinoline
Conditions | Yield |
---|---|
Stage #1: N-(p-chlorobenzyl)aniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
Conditions | Yield |
---|---|
With 2,3-dichloro-5,6-dicyanohydroquinone In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
2-methylquinoline
N-(3-methoxybenzyl)aniline
(E)-2-(3-methoxystyryl)quinoline
Conditions | Yield |
---|---|
Stage #1: N-(3-methoxybenzyl)aniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
2-methylquinoline
N-(m-chlorobenzyl)aniline
(E)-2-(3-chlorostyryl)quinoline
Conditions | Yield |
---|---|
Stage #1: N-(m-chlorobenzyl)aniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: N-(2-methoxybenzyl)aniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
2-methylquinoline
N-(thiophen-2-ylmethyl)aniline
(E)-2-(2-(thiophen-2-yl)ethenyl)quinoline
Conditions | Yield |
---|---|
Stage #1: N-(thiophen-2-ylmethyl)aniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: N-Benzylaniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methylquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Reagent/catalyst; Solvent; Temperature; Time; Inert atmosphere; diastereoselective reaction; | 99% |
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