As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences,
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:93-60-7
Min.Order:0 Metric Ton
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Type:Manufacturers
inquiryAnalysis tests Standard Results Appearance Yellowish Crystallization Hangzhou Dingyan Chem is a leading manufacturer and supplie
Cas:93-60-7
Min.Order:1 Kilogram
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inquiryUnique advantages for Methyl nicotinate Cas 93-60-7 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Storage:Store below +30°C Package:25kg/drum Appli
Cas:93-60-7
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:93-60-7
Min.Order:1 Gram
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:93-60-7
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:93-60-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryProduct Name: Methyl nicotinate Synonyms: RARECHEM AL BF 0185;PYRIDINE-3-CARBOXYLIC ACID METHYL ESTER;PELLAGRA PREVENTIVE FACTOR METHYL ESTER;NICONACID METHYL ESTER;NICOTINIC ACID METHYL ESTER;NIACIN METHYL ESTER;METHYL NICOTINATE DAC;METHYL PYRID
Cas:93-60-7
Min.Order:1 Kilogram
FOB Price: $500.0
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:93-60-7
Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:93-60-7
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryAppearance:Off-white or light yellow crystal Storage:Room temperature Package:25kg/drum Application:Pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:93-60-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:93-60-7
Min.Order:10 Gram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:93-60-7
Min.Order:1 Kilogram
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:93-60-7
Min.Order:10 Gram
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Type:Trading Company
inquiryProduct Name: Methyl nicotinate CAS: 93-60-7 MF: C7H7NO2 MW: 137.14 EINECS: 202-261-8 Mol File: 93-60-7.mol Methyl nicotinate Structure Methyl nicotinate Chemical Properties Melting point 42-44 °C (lit.) Boiling point
Cas:93-60-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/821.html Product Name Methyl nicotinate CAS No. 93-60-7
Cas:93-60-7
Min.Order:1 Gram
FOB Price: $22.0
Type:Lab/Research institutions
inquiryMethyl nicotinateCAS: 93-60-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
Cas:93-60-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:93-60-7
Min.Order:10 Kilogram
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Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:93-60-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryCompany information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in carbomer,carbopol,lead acetate,meglumine diphenyl ethylamine and other chemical raw materials and chemical reagents research and development production enterpr
Cas:93-60-7
Min.Order:1 Kilogram
FOB Price: $8.0 / 10.0
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:93-60-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
PRODUCT DETAILS
Cas:93-60-7
Min.Order:500 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryProduct Name: Methyl nicotinate Synonyms: Methyl Nicotinate (Nicotinic Acid Methyl Ester);Methyl nicotinate puriss., >=99.0% (GC);Methyl pyridine-3-carboxylate Nicotinic acid methyl ester;3-(carbomethoxy)pyridine;3-(Methoxycarbonyl)pyridine;3
Cas:93-60-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryPrice, service, company and transport advantage : 1. best service, high quality and reasonable price 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's customers' r
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/A
Cas:93-60-7
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:93-60-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1-oxy-nicotinic acid methyl ester
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol for 0.0166667h; Ambient temperature; | 98% |
With sodium hypophosphite; palladium on activated charcoal In acetic acid at 60℃; for 1.5h; | 98% |
With (4,4′-di-tert-butyl-2,2′-bipyridine)bis[(2-pyridinyl)phenyl]iridium(III) hexafluorophosphate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 1.5h; Inert atmosphere; Irradiation; chemoselective reaction; | 98% |
3-iodopyridine
methanol
carbon monoxide
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With triethylamine at 100℃; for 1.5h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With phosphotungstic acid for 6h; Reflux; | 96% |
With sulfuric acid at 65℃; for 18h; | 89% |
With sulfuric acid for 14h; Heating / reflux; | 88% |
Conditions | Yield |
---|---|
With oxygen; potassium carbonate at 60℃; under 750.075 Torr; for 20h; | 95% |
With iodine; potassium carbonate for 24h; Heating; | 82% |
With dibromamine-T; potassium carbonate In acetonitrile at 20℃; for 2h; | 78% |
3-Bromopyridine
methanol
carbon monoxide
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With C57H43IP2Pd; triethylamine at 130℃; under 3750.38 Torr; for 24h; Autoclave; | 94% |
With tert-Amyl alcohol; sodium hydride; cobalt(II) acetate In tetrahydrofuran at 40℃; under 760 Torr; for 61h; Irradiation; | 70% |
With sodium methylate; C2H5OOCCH2Co(CO)4 In diethyl ether at 25 - 35℃; | 57% |
Conditions | Yield |
---|---|
With 4-ethyl-1-methyl-4H-[1,2,4]-triazol-1-ium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 20℃; for 0.333333h; | 93% |
With potassium carbonate In water at 20℃; for 2h; | 92% |
With oxygen at 70℃; under 750.075 Torr; for 16h; | 87% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal at 25℃; for 2h; | 92% |
With sulfuric acid at 100℃; for 0.5h; Temperature; Sealed tube; |
Conditions | Yield |
---|---|
magnesium(II) perchlorate In nitromethane at 40℃; for 16h; | 92% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; for 8h; | A n/a B n/a C 90% |
Conditions | Yield |
---|---|
microwave irradiation; | 88% |
In toluene at 110℃; for 24h; | 77% |
nicotinic acid
methyl salicylate
A
methyl 3-pyridinecarboxylate
B
salicylic acid
Conditions | Yield |
---|---|
Stage #1: nicotinic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl salicylate at 110℃; for 24h; | A 81% B n/a |
Conditions | Yield |
---|---|
for 1h; Heating; | 80% |
A
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
In methanol; water at 25℃; for 18h; Ring cleavage; in 70 percent MeOH; evapn.; purification by ODS column chromy.; | A n/a B 80% |
Conditions | Yield |
---|---|
With 1,3-diazido-propane In neat (no solvent) at 20℃; for 0.333333h; | 75% |
3-Chloropyridine
methanol
carbon monoxide
lithium methanolate
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; 5 mol% Pd/C; sodium fluoride In 1,4-dioxane at 150℃; Inert atmosphere; | 75% |
methanol
pyridin-3-yl trifluoromethanesulfonate
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate In dimethyl sulfoxide at 70℃; for 2h; | 72% |
nicotinic acid
methyl iodide
A
methyl 3-pyridinecarboxylate
B
3-methoxycarbonyl-1-methyl-pyridinium
Conditions | Yield |
---|---|
Stage #1: nicotinic acid With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 0.166667h; Stage #2: methyl iodide In acetonitrile at 20℃; for 4h; | A 72% B n/a |
6-Chloronicotinic acid methyl ester
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at 25℃; for 2h; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 62% |
pyridine-2,5-dicarboxylic acid 5-methyl ester
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With methanol at 40℃; for 48h; Schlenk technique; Irradiation; Inert atmosphere; | 62% |
Conditions | Yield |
---|---|
With iron(III) chloride for 32h; Heating; | 61.3% |
With boron trifluoride diethyl etherate for 168h; Heating; | 43% |
Conditions | Yield |
---|---|
With sulfuric acid for 22h; Neat (no solvent); Reflux; | 54.7% |
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With CH3OH In dichloromethane MeOH added under N2 to soln. of Pd complex in CH2Cl2, kept for 24 h; evapd. under reduced pressure, extd. with Et2O, evapd., dissolved in CD2Cl2; identified by NMR; | 48% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | 40% |
1-oxy-nicotinic acid methyl ester
N,N-Dimethylthiocarbamoyl chloride
B
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
In acetonitrile at 81℃; for 4h; | A 10% B 36% |
3-pyridinecarboxaldehyde
methyl methoxyacetate
A
3-hydroxymethylpyridin
B
methyl 3-pyridinecarboxylate
C
methyl α-methoxy-β-(β-pyridyl)acrylate
Conditions | Yield |
---|---|
With sodium methylate In toluene for 2h; Heating; | A n/a B 10% C 31% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | 26% |
A
methyl 3-pyridinecarboxylate
B
methyl 6-isopropylnicotinate
Conditions | Yield |
---|---|
In methanol for 1.5h; Irradiation; | A 6.5% B 4% |
In methanol for 1.5h; Mechanism; Irradiation; intramolecular electron-transfer-induced photochemical cyclization; | A 6.5% B 4% |
Conditions | Yield |
---|---|
With diethyl ether; water | |
In diethyl ether |
Conditions | Yield |
---|---|
With selenium; sulfuric acid at 300℃; Erwaermen des Reaktionsgemisches mit Methanol; |
methyl 3-pyridinecarboxylate
methyl 1,4,5,6-tetrahydro-3-pyridinecarboxylate
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen; triethylamine In methanol at 23℃; for 48h; | 100% |
With palladium 10% on activated carbon; hydrogen; triethylamine In methanol under 879.175 Torr; for 12h; | 10.1 g |
Conditions | Yield |
---|---|
With hydrogen In water at 120℃; under 11251.1 Torr; for 1h; | 100% |
Conditions | Yield |
---|---|
In acetone for 10h; Substitution; Heating; | 99.6% |
Conditions | Yield |
---|---|
With hydrazine hydrate for 5h; Heating; | 99% |
With hydrazine hydrate In ethanol at 20℃; for 3h; | 93.2% |
With hydrazine hydrate In methanol at 100℃; for 24h; | 85% |
methyl 3-pyridinecarboxylate
prenyl tributylstannane
methyl chloroformate
1,3-bis(methoxycarbonyl)-4-(1,1-dimethyl-2-propenyl)-1,4-dihydropyridine
Conditions | Yield |
---|---|
In dichloromethane at 0℃; | 99% |
Conditions | Yield |
---|---|
With lanthanum(III) isopropoxide; 2-(2-methoxyethoxy)ethyl alcohol at 110℃; for 6h; Reagent/catalyst; Molecular sieve; | 99% |
With N,N'-biscyclohexyl-imidazol-2-ylidene; 4 A molecular sieve In tetrahydrofuran at 20℃; for 0.25h; | 96% |
With lanthanum (III) nitrate * water; 1,1,1-trioctyl-1-methylphosphonium methylcarbonate In hexane for 1h; Molecular sieve; Reflux; | 92% |
With platinum; 1-butyl-3-methylimidazolium Tetrafluoroborate at 20 - 60℃; for 2h; Inert atmosphere; Electrochemical reaction; Green chemistry; | 62% |
With 3,5-bistrifluoromethylphenylisothiocyanate; 4-pyrrolidin-1-ylpyridine In n-heptane for 24h; Reflux; |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran Barbier reaction; Cooling with ice; Inert atmosphere; | 99% |
methyl 3-pyridinecarboxylate
(Bis-trimethylsilanyloxy-methylene)-cyclohexane
1-{3-(methoxycarbonyl)-1-[(trifluoromethyl)sulfonyl]-1,4-dihydropyridin-4-yl}cyclohexanecarboxylic acid
Conditions | Yield |
---|---|
Stage #1: methyl 3-pyridinecarboxylate With trifluoromethylsulfonic anhydride In dichloromethane at -78℃; for 0.5h; Inert atmosphere; Stage #2: (Bis-trimethylsilanyloxy-methylene)-cyclohexane In dichloromethane at -78 - 20℃; | 99% |
Conditions | Yield |
---|---|
at 150 - 160℃; for 3h; Condensation; | 98% |
at 50℃; for 0.5h; | 71% |
Conditions | Yield |
---|---|
With [RuCl2(N-heterocyclic carbene)(bis[2-(diphenylphosphino)ethyl]amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 50℃; under 7500.75 Torr; for 5h; Schlenk technique; Inert atmosphere; | 98% |
With sodium tetrahydroborate; sodium methylate In methanol at 25℃; for 3h; Reagent/catalyst; Inert atmosphere; | 98% |
With 2-(Aminomethyl)pyridine; 1,3-bis-(diphenylphosphino)propane; potassium tert-butylate; hydrogen In 2-methyltetrahydrofuran at 100℃; under 37503.8 Torr; for 16h; Reagent/catalyst; Autoclave; | 95% |
methyl 3-pyridinecarboxylate
1-oxy-nicotinic acid methyl ester
Conditions | Yield |
---|---|
With phthalic anhydride; urea-hydrogen peroxide In dichloromethane for 4h; Ambient temperature; | 98% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 24h; Inert atmosphere; | 98% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 24h; | 98% |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane for 0.2h; | 98% |
methyl 3-pyridinecarboxylate
methyl iodide
3-(methoxycarbonyl)-1-methylpyridinium iodide
Conditions | Yield |
---|---|
In acetonitrile at 90℃; for 1h; Sealed tube; | 97% |
In benzene for 3h; Heating; | |
In ethyl acetate |
methyl 3-pyridinecarboxylate
phenyl chloroformate
2H-pyridine-1,3-dicarboxylic acid 3-methyl ester 1-phenyl ester
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at -78℃; for 3h; Fowler reduction; | 97% |
methyl 3-pyridinecarboxylate
6-methoxy-tryptophyl bromide
Conditions | Yield |
---|---|
In methanol; diethyl ether at 100℃; for 1h; | 97% |
Conditions | Yield |
---|---|
With N,N'-biscyclohexyl-imidazol-2-ylidene; 4 A molecular sieve In tetrahydrofuran at 20℃; for 2h; | 97% |
With tetraethylammonium bicarbonate at 60℃; for 2h; | 84% |
With platinum; 1-butyl-3-methylimidazolium Tetrafluoroborate at 20 - 60℃; for 2h; Inert atmosphere; Electrochemical reaction; Green chemistry; | 62% |
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With (Ra)-4-hydroxy-2,6-bis(2,4,6-tricyclohexylphenyl)dinaphtho-[1,3,2]dioxaphosphepine 4-oxide; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate In 1,4-dioxane for 14h; Minisci Aromatic Substitution; Irradiation; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
Stage #1: nickel(II) sulfate hexahydrate; naphthalene-2-sulfonate In hexane at 40℃; for 0.5h; Stage #2: methyl 3-pyridinecarboxylate; water In methanol; ethanol at 40℃; for 2h; | 96.6% |
methyl 3-pyridinecarboxylate
1-phenyl-1-trimethylsiloxypropene
methyl chloroformate
1,3-bis(methoxycarbonyl)-4-(1-methyl-2-oxo-2-phenylethyl)-1,4-dihydropyridine
Conditions | Yield |
---|---|
In dichloromethane Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With 14C2H2F3O(1-)*6C4H8O*La2Na8(14+) at 80℃; for 6h; Inert atmosphere; | 96% |
With silica gel In neat (no solvent) at 100℃; for 12h; Inert atmosphere; Sealed tube; | 87% |
With bis(trimethylaluminum)–1,4-diazabicyclo[2.2.2]octane adduct In tetrahydrofuran at 130℃; for 0.133333h; Concentration; Solvent; Inert atmosphere; Microwave irradiation; | 80% |
With potassium phosphate; 2,2,2-trifluoroethanol In tetrahydrofuran at 90℃; for 22h; Sealed tube; | 67% |
methyl 3-pyridinecarboxylate
(phenylmethoxy)methylphosphonic acid diethyl ester
diethyl [1-benzyloxy-2-oxo-2-(pyridin-3-yl)ethyl]phosphonate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -5 - 0℃; for 0.75h; Inert atmosphere; | 95.9% |
methyl 3-pyridinecarboxylate
benzyl bromide
1-benzyl-3-(methoxycarbonyl)pyridinium bromide
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; for 18h; | 95% |
In isopropyl alcohol at 20℃; for 18h; Inert atmosphere; | 93% |
With methanol | |
Alkylation; |
methyl 3-pyridinecarboxylate
tris(methylthio)methane
A
tetrathioorthocarbonic acid tetramethyl ester
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane 1.) -95 deg C, 2 h, 2.) -78 deg C, 30 min; | A n/a B 95% |
Conditions | Yield |
---|---|
In ethyl acetate at 20℃; for 3h; Substitution; | 95% |
methyl 3-pyridinecarboxylate
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate In acetonitrile at 20℃; for 12h; Minisci Aromatic Substitution; Inert atmosphere; Irradiation; | 95% |
methyl 3-pyridinecarboxylate
cholesterol
(3S,8S,9S,10R,13R,14S,17R)-10,13-dimethyl-17-((R)-6-methylheptan-2-yl)-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl nicotinate
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane for 18h; Ambient temperature; | 94% |
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