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Cas:134-20-3
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inquiryProduct Description Product Name Methyl anthranilate CAS No. 134-20-3 Appearance White to yellowish crystal or liquid Assay ≥99%
Cas:134-20-3
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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inquiryProduct Name: Methyl anthranilate Synonyms: NEROLI;NEROLI OIL, ARTIFICIAL;2-AMINOBENZOIC ACID METHYL ESTER;ANTHRANILIC ACID METHYL ESTER;ANTHRANILIC ACID:METHYL ESTER;METHYL 2-ANTHRANILATE;METHYL 2-AMINOBENZOATE;Methl-O-Aminobenzoate CAS: 134-20-
Cas:134-20-3
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inquiryAbout Product Details
Cas:134-20-3
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:134-20-3
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Cas:134-20-3
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inquiryProduct name: Methyl anthranilate CAS:134-20-3 MF:C8H9NO2 MW:151.16 Density:1.168 g/ml Melting point:24°C Package:1 L/bottle, 25 L/drum, 200 L/drum Property:It is soluble in ethanol, ether and other organic solvents, slightly soluble in wa
Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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inquiryhigh quality Methyl anthranilate Basic information Product Name: Methyl anthranilate Synonyms: NEROLI;NEROLI OIL, ARTIFICIAL;2-AMINOBENZOIC ACID METHYL ESTER;ANTH
Product Name: Methyl anthranilate CAS: 134-20-3 MF: C8H9NO2 MW: 151.16 EINECS: 205-132-4 Methyl anthranilate Structure Methyl anthranilate Chemical Properties Melting point 24 °C (lit.) Boiling point 256 °C (lit.) den
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:liquid Storage:Refer to COA / MSDS Package:Fact
Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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Cas:134-20-3
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inquiryConditions | Yield |
---|---|
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran; water at 20℃; for 0.5h; | 100% |
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.5h; | 100% |
With sodium hypophosphite monohydrate; 5%-palladium/activated carbon; hypophosphorous acid In 2-methyltetrahydrofuran; water for 3h; Sonication; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
for 1h; | 99.5% |
5-methoxy-3H-1,4-benzodiazepine
2-carbomethoxyaniline
Conditions | Yield |
---|---|
In 1,4-dioxane; water for 2h; Heating; | 99% |
2-azido-benzoic acid methyl ester
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 0.0833333h; Ambient temperature; | 98% |
With hydrogen iodide at 20℃; for 1.5h; | 95% |
With ammonium chloride; indium In ethanol for 1h; Reduction; Heating; | 92% |
phthalimide
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With sodium hypochlorite; sodium hydroxide In methanol; water at 0 - 80℃; for 0.0583333h; Temperature; | 96.8% |
5-Methoxy-2-methyl-3H-benzo[e][1,4]diazepine
2-carbomethoxyaniline
Conditions | Yield |
---|---|
In 1,4-dioxane; water for 2h; Heating; | 96% |
2-[(2-methoxycarbonylphenylamino)methylene]malonic acid diethyl ester
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With ethylenediamine In ethanol at 20℃; for 2.3h; | 96% |
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 65℃; for 18h; Inert atmosphere; | 95% |
With thionyl chloride Reflux; | 93% |
With thionyl chloride at 0℃; Inert atmosphere; Reflux; | 88% |
2-[3-acetoxy-2-(2-methoxycarbonyl-phenylazo)-propyl]-benzoic acid methyl ester
B
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With hydrogen; nickel In methanol under 37503 Torr; for 2h; | A 84% B 95% |
Conditions | Yield |
---|---|
In methanol at 0 - 75℃; for 1h; | 95% |
Conditions | Yield |
---|---|
In diethyl ether at 0℃; | 94% |
With diethyl ether | |
In diethyl ether at 20℃; for 1h; |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; caesium carbonate at 20 - 30℃; for 4h; Reagent/catalyst; Sealed tube; | 93% |
With dihydrogen peroxide; sodium methylate Esterification; oxidation; |
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Reflux; | 92% |
With sodium hydride In mineral oil for 2h; Reflux; Inert atmosphere; | 91% |
With caesium carbonate at 20℃; | 88% |
2-Amino-3-triisopropylsilanyl-benzoic acid methyl ester
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With trifluoroacetic acid In tetrachloromethane for 2h; Heating; | 92% |
Conditions | Yield |
---|---|
With dichloro[2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II); triethylamine at 100℃; under 2585.74 Torr; for 16h; | 92% |
With triethylamine; 1,1'-bis(diphenylphosphino)ferrocene; [(Pd(μ-Cl)(κ(2)-P,C-P(OC6H2-2,4-tBu2)(OC6H3-2,4-tBu2)2))2] In toluene at 120℃; for 12h; |
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 80℃; for 24h; | 92% |
Conditions | Yield |
---|---|
90.4% |
methyl 2-(methyl(nitroso)amino)benzoate
A
benzoic acid methyl ester
B
4-nitrobenzoic acid methyl ester
C
diphenic acid dimethyl ester
D
dimethyl (1,1'-biphenyl)-2,4'-dicarboxylate
E
dimethyl (1,1'-biphenyl)-2,3'-dicarboxylate
F
2-(benzoyl-methylamino)benzoic acid methyl ester
G
2-carbomethoxyaniline
H
Methyl N-methylanthranilate
I
methyl 2-(benzamido)benzoate
J
N-formylanthranilic acid methyl ester
Conditions | Yield |
---|---|
at 220℃; for 0.25h; Sealed tube; | A n/a B n/a C n/a D n/a E n/a F n/a G n/a H n/a I 90% J n/a |
Conditions | Yield |
---|---|
With samarium; iodine In methanol for 5h; Heating; | 86% |
anthranilic acid
methyl salicylate
A
2-carbomethoxyaniline
B
salicylic acid
Conditions | Yield |
---|---|
Stage #1: anthranilic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl salicylate at 110℃; for 24h; | A 84% B n/a |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 1h; Heating; | 82% |
methyl 2-(3,3-diisopropylureido)benzoate
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With water for 18h; Reflux; | 80% |
2-(1-acetoxymethyl-3-ethoxycarbonylpropylazo)benzoic acid methyl ester
B
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With hydrogen; nickel In methanol under 37503 Torr; for 3h; | A 79% B n/a |
methanol
phthalimide
A
methyl 2-((methoxycarbonyl)amino)benzoate
B
2-carbomethoxyaniline
Conditions | Yield |
---|---|
Stage #1: methanol With iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid at 0℃; for 0.166667h; Inert atmosphere; Stage #2: phthalimide With potassium carbonate at 0 - 20℃; for 2h; Hofmann-type rearrangement; Inert atmosphere; regioselective reaction; | A 79% B 14% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 3h; Reflux; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
With acetamidine hydrochloride; caesium carbonate In N,N-dimethyl-formamide at 130℃; for 20h; Inert atmosphere; Green chemistry; | 76% |
With copper(I) oxide; sodium azide; L-proline In dimethyl sulfoxide at 100℃; for 0.25h; Inert atmosphere; | 64% |
With copper acetylacetonate; ammonium hydroxide; caesium carbonate; acetylacetone In water; N,N-dimethyl-formamide at 90℃; for 24h; Inert atmosphere; | 23% |
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 55℃; for 6h; | 75% |
Conditions | Yield |
---|---|
With dmap; ethyl 2-cyanoacetate at 20℃; for 4.5h; chemoselective reaction; | 73% |
Conditions | Yield |
---|---|
With samarium; iodine for 6h; Ambient temperature; | 70% |
methyl 2-isothiocyanatobenzoate
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With 3,4-dimercaptotoluene; sodium hydrogencarbonate In methanol at 25℃; for 2h; | 69% |
2-carbomethoxyaniline
p-toluenesulfonyl chloride
methyl N-tosylanthranilate
Conditions | Yield |
---|---|
In pyridine at 25℃; | 100% |
Stage #1: 2-carbomethoxyaniline With pyridine In dichloromethane at 25℃; for 1h; Inert atmosphere; Stage #2: p-toluenesulfonyl chloride In dichloromethane at 25℃; for 24h; Inert atmosphere; | 99% |
In pyridine at 0℃; for 1h; | 98% |
2-carbomethoxyaniline
3,4-dimethoxybenzoic acid chloride
methyl N-(3,4-dimethoxybenzoyl)anthranilate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 0.5h; | 100% |
pivaloyl chloride
2-carbomethoxyaniline
methyl N-trimethylacetylanthranilate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 16h; | 100% |
With potassium carbonate In benzene Heating; | 98% |
With triethylamine In benzene for 1h; Heating; | |
With triethylamine In dichloromethane at 0 - 20℃; |
n-valeryl chloride
2-carbomethoxyaniline
methyl 2-(valerylamino)benzoate
Conditions | Yield |
---|---|
With triethylamine In chloroform at 0℃; for 4h; | 100% |
With potassium carbonate In benzene Heating; | 82% |
methyl thioisocyanate
2-carbomethoxyaniline
2-mercapto-3-methyl-3,4-dihydroquinazolin-4-one
Conditions | Yield |
---|---|
In neat (no solvent) for 72h; Ambient temperature; | 100% |
Benzoyl isothiocyanate
2-carbomethoxyaniline
2-(3-Benzoylthioureido)benzoesaeuremethylester
Conditions | Yield |
---|---|
In neat (no solvent) Ambient temperature; | 100% |
2-chloroethyl isothiocyanate
2-carbomethoxyaniline
methyl 2-<3-(2-chloroethyl)ureido>benzoate
Conditions | Yield |
---|---|
for 16h; Ambient temperature; | 100% |
ethoxyacetyl chloride
2-carbomethoxyaniline
methyl (2-ethoxyacetamido)benzoate
Conditions | Yield |
---|---|
With potassium carbonate In benzene Heating; | 100% |
With triethylamine In dichloromethane | 92.8% |
2-carbomethoxyaniline
isopentanoyl chloride
2-(3-Methyl-butyrylamino)-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In benzene Heating; | 100% |
With sodium hydrogencarbonate In tetrahydrofuran |
Conditions | Yield |
---|---|
With water; fluorine In chloroform; acetonitrile at -15℃; for 0.0333333h; | 100% |
With tert.-butylhydroperoxide; chromium silicalite-2 In methanol at 65℃; for 5h; | 91% |
With tert.-butylhydroperoxide; molecular sieve In methanol for 5h; Heating; | 91% |
With dihydrogen peroxide; <ϖ-C5H5N(1+)(CH2)15CH3>34>(3-) In chloroform for 24h; Heating; | 81% |
bis(trichloromethyl) carbonate
2-carbomethoxyaniline
methyl 2-isocyanatobenzoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 4h; | 100% |
With triethylamine In 1,2-dichloro-ethane at 0 - 85℃; for 8.5h; Inert atmosphere; |
3-chlorosulfonyl-4-methylbenzoic acid chloride
2-carbomethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 2-carbomethoxyaniline With sodium hydride In tetrahydrofuran for 0.333333h; Stage #2: 3-chlorosulfonyl-4-methylbenzoic acid chloride In tetrahydrofuran at 20℃; | 100% |
2-(4-acetamidophenylsulfonamido)-4-methylpentanoic acid
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With phosphorus trichloride under 760.051 Torr; Heating; | 100% |
2-(4-acetamidophenylsulfonamido)propanoic acid
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With phosphorus trichloride Heating; | 100% |
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With phosphorus trichloride | 100% |
methyl chloroformate
2-carbomethoxyaniline
methyl 2-((methoxycarbonyl)amino)benzoate
Conditions | Yield |
---|---|
In toluene for 8h; Inert atmosphere; Reflux; | 99% |
In toluene for 8h; Reflux; | 88% |
Conditions | Yield |
---|---|
With bromine; sodium hydrogensulfite In dichloromethane; acetic acid | 99% |
Stage #1: 2-carbomethoxyaniline With bromine In dichloromethane; water at 20℃; for 0.166667h; Industrial scale; Stage #2: With dihydrogen peroxide In dichloromethane; water for 6h; Industrial scale; | 96% |
With dihydrogen peroxide; bromine In dichloromethane; water Solvent; | 96.86% |
2-carbomethoxyaniline
Glycine ethyl ester isocyanate
N-(carbamoyl)glycinaethylester
Conditions | Yield |
---|---|
for 16h; Ambient temperature; | 99% |
2-carbomethoxyaniline
dianthranilide
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 72h; Reflux; | 99% |
With sodium hydride In tetrahydrofuran for 96h; | 95% |
With sodium hydride In tetrahydrofuran; mineral oil at 25 - 30℃; for 76.5h; Inert atmosphere; | 81% |
di-tert-butyl dicarbonate
2-carbomethoxyaniline
Conditions | Yield |
---|---|
With lanthanum(III) nitrate at 20℃; for 0.0833333h; | 99% |
In ethanol at 50℃; for 216h; Inert atmosphere; | 98% |
With lanthanum(III) nitrate hexahydrate at 20 - 50℃; for 4h; | 93% |
acrylic acid methyl ester
2-carbomethoxyaniline
2-(E)-[2-methoxycarbonylphenyl]acrylic acid methylester
Conditions | Yield |
---|---|
Stage #1: 2-carbomethoxyaniline With tert.-butylnitrite In methanol at 0℃; for 0.5h; Stage #2: acrylic acid methyl ester With methanesulfonic acid; palladium diacetate In methanol at 0 - 25℃; Heck-Matsuda reaction; | 99% |
Stage #1: 2-carbomethoxyaniline With tert.-butylnitrite In methanol at 0℃; for 0.5h; Heck-Matsuda reaction; Stage #2: acrylic acid methyl ester With methanesulfonic acid; palladium diacetate In methanol at 0 - 25℃; for 48h; Heck-Matsuda reaction; | 99% |
With tert.-butylnitrite; methanesulfonic acid; palladium diacetate In methanol; N,N-dimethyl-formamide at 25℃; Heck Reaction; Flow reactor; | 96% |
2,2’-dibromodiphenylmethane
2-carbomethoxyaniline
2-(anthracen-9-yl)aniline
Conditions | Yield |
---|---|
Stage #1: 2,2’-dibromodiphenylmethane With magnesium In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; Reflux; Stage #2: 2-carbomethoxyaniline In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: cyclohexanone; 2-carbomethoxyaniline With chloro-trimethyl-silane In N,N-dimethyl-formamide Schlenk technique; Inert atmosphere; Stage #2: With sodium tetrahydroborate In N,N-dimethyl-formamide at 0℃; for 0.25h; Schlenk technique; Inert atmosphere; | 99% |
phthalic anhydride
2-carbomethoxyaniline
methyl 2-(1,3-dioxoisoindolin-2-yl)benzoate
Conditions | Yield |
---|---|
With triethylamine In toluene Reflux; Dean-Stark; | 98% |
With acetic acid for 5h; Condensation; Heating; | 72.2% |
With acetic acid | |
With acetic acid Reflux; |
chloroacetyl chloride
2-carbomethoxyaniline
methyl N-(chloroacetyl)anthranilate
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 4h; | 98% |
With sodium hydrogencarbonate In tetrahydrofuran; water | 96% |
In benzene Heating; | 95% |
formaldehyd
2-carbomethoxyaniline
N,N'-methanediyl-di-anthranilic acid dimethyl ester
Conditions | Yield |
---|---|
In water | 98% |
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