As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences,
Melting point 8-10 °C (lit.) Boiling point 223-224 °C (lit.) density 1.107 g/mL at 25 °C (lit.) refractive index n20/D 1.504(lit.) Fp 93 °C storage temp. 2-8°C solubility 50g/l pka pK1:3.35(+1) (25&
Cas:614-18-6
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inquiryItems Standard Result Appearance Colorless or light yellow transparent liquid Conforms Content
Cas:614-18-6
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name Ethyl nicotinoate CAS number 614-18-6 Assay ≥99% Appearance Yellowish to colorless liquid Capacity 200mt/year Application Pharmaceutical/pes
Cas:614-18-6
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:614-18-6
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryDayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:614-18-6
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiry1.Good capacity; 2.Safe deliver 3. High quality with best price Appearance:White Powder Storage:Dry and cool place Package:100g/ bag, 2 kg/ bag, 25kg/ carton or as required Application:For Pharmaceutical Intermediates Transportation:By DHL, TNT
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Cas:614-18-6
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inquiryEthyl nicotinate CAS:614-18-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
Cas:614-18-6
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Company information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big cust
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inquiryHubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medicine)
Cas:614-18-6
Min.Order:10 Milligram
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Type:Lab/Research institutions
inquiryProduct Name: Ethyl nicotinate Synonyms: Ethyl nicotinate,99%,stabilized;2-ethylpyridine-3-carboxylic acid;Ethyl Nicontinate;Ethyl nicotinate, stabilized, 99% 100GR;NSC 8872;β-Pyridinecarboxylic Acid Ethyl Ester;Nicotinic Acid Ethyl Ester E
Cas:614-18-6
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:614-18-6
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:614-18-6
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:614-18-6
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiry3-iodopyridine
ethanol
carbon monoxide
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate at 20 - 125℃; under 7500.75 - 22502.3 Torr; for 0.333333h; microwave irradiation; | 98% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 80℃; under 760.051 Torr; for 6h; | 94% |
With palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene at 120℃; under 9308.91 Torr; | |
With palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene at 120℃; under 8274.59 - 10136.4 Torr; | 88 %Spectr. |
With palladium diacetate; potassium carbonate at 60℃; under 20521.4 Torr; for 12h; Green chemistry; chemoselective reaction; | 21 %Spectr. |
3-Bromopyridine
ethanol
carbon monoxide
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine at 70℃; under 760.051 Torr; for 3h; Catalytic behavior; | 98% |
Conditions | Yield |
---|---|
With sulfuric acid In toluene at 55℃; for 4h; | 97.2% |
With sulfuric acid for 10h; Reflux; Sealed tube; | 83% |
With sulfuric acid for 4h; Reflux; | 81% |
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile for 2h; Heating; | 92% |
1-(pyridin-3-yl)pentan-1-one
ethyl trifluoroacetate,
A
3-pyridinecarboxylic acid ethyl ester
B
1,1,1-trifluoro-2-hexanone
Conditions | Yield |
---|---|
Stage #1: ethyl trifluoroacetate, With sodium hydride In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Schlenk technique; Stage #2: 1-(pyridin-3-yl)pentan-1-one In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Schlenk technique; Reflux; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 0℃; for 0.25h; Inert atmosphere; Schlenk technique; | A 92% B n/a |
dicobalt octacarbonyl
ethanol
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate at 50℃; for 12h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 91% |
dicobalt octacarbonyl
ethanol
pyridin-3-yl trifluoromethanesulfonate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate at 50℃; for 12h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 90% |
3-iodopyridine
ethanol
molybdenum hexacarbonyl
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With C35H20F34NO3(1-)*Pd(2+)*Cl(1-); N-ethyl-N,N-diisopropylamine In neat (no solvent) at 130℃; for 0.333333h; Microwave irradiation; | 89% |
1-oxy-nicotinic acid ethyl ester
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With cerium(III) chloride heptahydrate; zinc In methanol at 20℃; for 2.5h; | 87% |
Conditions | Yield |
---|---|
microwave irradiation; | 86% |
In toluene at 110℃; for 24h; | 81% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane at 40℃; for 5h; | 86% |
With chloro-trimethyl-silane at 20 - 40℃; for 5h; Inert atmosphere; | 86% |
3-Chloropyridine
dicobalt octacarbonyl
ethanol
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With (S)-1-[(R)-2-(di-1-naphthylphosphino)ferrocenyl]ethyl-di-tert.-butylphosphine; potassium acetate; palladium diacetate at 80℃; for 12h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 86% |
ethyl bromide
potassium nicotinate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With tetrabutylammomium bromide for 43h; Ambient temperature; | 82% |
3-Bromopyridine
potassium monoethyl oxalate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane In 1-methyl-pyrrolidin-2-one at 150℃; for 16h; Inert atmosphere; | 82% |
nicotinic acid
boron trifluoride diethyl etherate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
at 120℃; | 82% |
tetraethoxy tellurium(IV)
nicotinamide
A
pyridine-3-carbonitrile
B
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
In tetrachloromethane for 18h; Heating; | A 8% B 79% |
nicotinamide
A
pyridine-3-carbonitrile
B
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With tetraethoxy tellurium(IV) In tetrachloromethane for 18h; Heating; | A 8% B 79% |
3-iodopyridine
potassium monoethyl oxalate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With palladium diacetate In 1-methyl-pyrrolidin-2-one at 20 - 140℃; for 24h; Inert atmosphere; | 79% |
3-Bromopyridine
dicobalt octacarbonyl
ethanol
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With dmap; palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 90℃; for 0.5h; Microwave irradiation; | 78% |
Conditions | Yield |
---|---|
With 1,3-diazido-propane In neat (no solvent) at 20℃; for 0.333333h; | 78% |
ethyl 6-iodonicotinate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; phenylsilane; indium(III) acetate In ethanol at 20℃; for 18h; | 75% |
With indium In water for 10h; Heating; | 64% |
With indium; water for 10h; Reflux; | 64% |
ethyl trifluoroacetate,
C12H11NOS
A
3-pyridinecarboxylic acid ethyl ester
B
1,1,1-trifluoro-4-(2-thiophenyl)butan-2-one
Conditions | Yield |
---|---|
Stage #1: ethyl trifluoroacetate, With sodium hydride In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Schlenk technique; Stage #2: C12H11NOS In tetrahydrofuran at 0℃; Inert atmosphere; Schlenk technique; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 0℃; for 0.25h; Inert atmosphere; Schlenk technique; | A 75% B 74% |
piperidine
3-Chloropyridine
carbon monoxide
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; sodium phenoxide; palladium diacetate In toluene at 100℃; under 760.051 Torr; for 16h; | 71% |
3-Chloropyridine
ethanol
carbon monoxide
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With bis(benzonitrile)palladium(II) dichloride; sodium acetate; 1,4-di(diphenylphosphino)-butane at 100℃; under 750.075 Torr; for 16h; | 71% |
Conditions | Yield |
---|---|
With Josiphos Et2P-Fc-PtBu2 ligand; sodium acetate; palladium diacetate at 130 - 135℃; under 2068.59 Torr; for 20h; | 70% |
pyrrole
ethyl 2-bromo-2-diazoacetate
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium dithionite; c-type cytochrome maquette, C45 In ethanol at 5℃; for 2h; pH=8.6; Sealed tube; Inert atmosphere; Enzymatic reaction; | 69.4% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate for 144h; Heating; | 67% |
With iron(III) chloride for 21h; Heating; | 63.3% |
3-Bromopyridine
oxalic acid diethyl ester
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With dmap; bis-triphenylphosphine-palladium(II) chloride In ethanol at 140℃; for 0.333333h; Microwave irradiation; | 66% |
Propargylamine
propynoic acid ethyl ester
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver trifluoromethanesulfonate In toluene at 80℃; for 6h; Sealed tube; regioselective reaction; | 63% |
3-pyridinecarboxaldehyde
ethanol
A
3-pyridinecarboxylic acid ethyl ester
B
1,2-di(pyridine-3-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
With oxygen; Thiamine hydrochloride; triethylamine for 2h; Reflux; | A 30% B 58% |
2-aminobutanol
3-pyridinecarboxylic acid ethyl ester
N-(1-hydroxybutan-2-yl)nicotinamide
Conditions | Yield |
---|---|
at 50℃; for 0.5h; | 100% |
3-pyridinecarboxylic acid ethyl ester
3-amino-2-propanol
N-(2-hydroxypropyl)-3-pyridinecarboxamide
Conditions | Yield |
---|---|
at 50℃; for 0.5h; | 100% |
3-pyridinecarboxylic acid ethyl ester
propan-1-ol-3-amine
N-(3-hydroxypropyl)nicotinamide
Conditions | Yield |
---|---|
at 50℃; for 0.5h; | 100% |
3-pyridinecarboxylic acid ethyl ester
1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene
Conditions | Yield |
---|---|
In acetonitrile for 6h; Heating; | 100% |
Conditions | Yield |
---|---|
at 80 - 85℃; for 6.5h; | 99.5% |
3-pyridinecarboxylic acid ethyl ester
Ethyl nipecotate
Conditions | Yield |
---|---|
With hydrogen In hexane at 100℃; under 7600.51 Torr; for 24h; Temperature; Pressure; Autoclave; | 99% |
With sodium hydroxide; hydrogen; nickel In ethanol; water at 20 - 40℃; Electrolysis; | 98% |
With 1,4-dioxane; nickel at 165℃; under 110326 - 220652 Torr; Hydrogenation; |
3-pyridinecarboxylic acid ethyl ester
benzyl bromide
N-benzyl-3-(ethoxycarbonyl)pyridinium bromide
Conditions | Yield |
---|---|
In isopropyl alcohol for 18h; | 98% |
In isopropyl alcohol at 20℃; for 18h; | 90% |
In nitrobenzene at 40℃; Rate constant; | |
In acetone Reflux; |
Conditions | Yield |
---|---|
With PPA at 155℃; for 4.5h; | 98% |
With alkaline H2O In dimethyl sulfoxide at 30℃; Rate constant; other solvent (EtOH); variation of water concentrations; | |
esterase in WBN; IL-Ht rat abdominal skin homogenate at 37℃; Enzyme kinetics; |
3-pyridinecarboxylic acid ethyl ester
N-(N,N-diethylaminomethyl)-2-piperidone
Conditions | Yield |
---|---|
With sodium hydride In toluene for 8h; Heating; | 97% |
Conditions | Yield |
---|---|
With n-butyllithium; diisobutylaluminium hydride; tert-butyl alcohol In tetrahydrofuran; hexane at 0℃; | 97% |
Multi-step reaction with 2 steps 1: diethyl ether; lithium alanate 2: lead (IV)-acetate; benzene View Scheme |
3-pyridinecarboxylic acid ethyl ester
ethanolamine
N-(2-hydroxyethyl)nicotinamide
Conditions | Yield |
---|---|
Stage #1: 3-pyridinecarboxylic acid ethyl ester; ethanolamine at 125℃; for 4h; Large scale; Stage #2: With acetone at 45 - 60℃; for 1h; Large scale; Stage #3: at 10 - 30℃; for 2.5h; Temperature; Large scale; | 96.6% |
64.5% | |
64.5% |
3-pyridinecarboxylic acid ethyl ester
guanidine hydrochloride
N-(pyridyl-3-carbonyl)guanidine
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 12h; Heating; | 95% |
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 36h; | 95% |
Conditions | Yield |
---|---|
In tetrahydrofuran dry Ar-flushed Schlenk flask charged with organic compound, soln. of base added dropwise, stirred at -78 °C for 15 min; | 95% |
Conditions | Yield |
---|---|
Stage #1: 3-pyridinecarboxylic acid ethyl ester; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C10H10BrN3O With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 95% |
Conditions | Yield |
---|---|
Stage #1: 3-pyridinecarboxylic acid ethyl ester With potassium phosphate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; P,P'-(1,2-ethanediyl)bis{bis[3,5-di(trifluoromethyl)phenyl]phosphane} In toluene for 0.0833333h; Inert atmosphere; Microwave irradiation; Stage #2: methyl methacrylate In toluene at 120℃; for 24h; Inert atmosphere; Microwave irradiation; Sealed tube; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With hydrazine hydrate monohydrate In methanol at 140℃; for 1h; Microwave irradiation; Sealed tube; | 93% |
With hydrazine hydrate In ethanol for 1.08333h; Ambient temperature; | 85% |
With hydrazine hydrate In ethanol Reflux; Sealed tube; | 85% |
3-pyridinecarboxylic acid ethyl ester
2,2,2-trifluoroethyl(phenyl)iodonium trifluoromethanesulfonate
N-(2,2,2-Trifluoroethyl)-3-(ethoxycarbonyl)pyridinium triflate
Conditions | Yield |
---|---|
In dichloromethane for 0.166667h; Ambient temperature; | 93% |
Conditions | Yield |
---|---|
With graphene oxide In neat (no solvent) at 100℃; for 18h; Sealed tube; | 92% |
With silica gel In neat (no solvent) at 100℃; for 12h; Inert atmosphere; Sealed tube; | 87% |
3-pyridinecarboxylic acid ethyl ester
mesitylenesulfonylhydroxylamine
2,4,6-Trimethyl-benzenesulfonate1-amino-3-ethoxycarbonyl-pyridinium;
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; Ambient temperature; | 92% |
3-pyridinecarboxylic acid ethyl ester
3-(4-bromophenyl)-2-methylquinazolin-4(3H)-one
2-[2-Oxo-2-(3-pyridyl)ethyl]-3-p-bromophenyl-4(3H)-quinazolinone
Conditions | Yield |
---|---|
With sodium hydride In 1,2-dimethoxyethane Heating; | 92% |
2.43 g (92%) |
3-pyridinecarboxylic acid ethyl ester
acetic anhydride
ethyl 1-acetyl-1,4,5,6-tetrahydropyridine-3-carboxylate
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal under 5171.48 Torr; | 92% |
3-pyridinecarboxylic acid ethyl ester
ethyl acetate
A
3-oxo-3-pyridin-3-yl-propionic acid ethyl ester
B
ethyl acetoacetate
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -40℃; for 0.333333h; Claisen condensation; Inert atmosphere; | A 92% B n/a |
3-pyridinecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
In acetonitrile for 60h; Inert atmosphere; Reflux; | 92% |
3-pyridinecarboxylic acid ethyl ester
methyl iodide
3-(ethoxycarbonyl)-1-methylpyridin-1-ium iodide
Conditions | Yield |
---|---|
In nitromethane for 12h; Ambient temperature; | 91% |
In isopropyl alcohol for 18h; | 87% |
In nitrobenzene at 35℃; Rate constant; |
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