Product Name: Nikethamide Synonyms: N,N-DIETHYLNICOTINAMIDE 59-26-7 Nicethamide Specification: BP, EP Packing: 25kg/plastic drum, outside is carton or drum MOQ: 25KG Origin: China Wel
Cas:59-26-7
Min.Order:25 Kilogram
Negotiable
Type:Other
inquiryItems Standard Result Character Colorless to light yellow oily liquid comply Relative density
Cas:59-26-7
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Trading Company
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:59-26-7
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:59-26-7
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:59-26-7
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
TIANFUCHEM--59-26-7--N,N-DIETHYLNICOTINAMIDE in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relat
Cas:59-26-7
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:59-26-7
Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
Cas:59-26-7
Min.Order:10 Gram
Negotiable
Type:Other
inquiry1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: N,N-Diethylnicotinamide Structure: Formula: C10H14N2O Molecular Weight : 178.23 Synonyms: CORVOTONE;DYNACORYL;EUCORAN;LABOTEST-BB LT00134638;PYRIDINE-3-CAR
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:59-26-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:59-26-7
Min.Order:1 Kilogram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryN,N-DIETHYLNICOTINAMIDE CAS: 59-26-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
Cas:59-26-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:59-26-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:59-26-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:59-26-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:59-26-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless micro treacly oil liquid or crystalline solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per yo
Cas:59-26-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:59-26-7
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:59-26-7
Min.Order:1 Kilogram
FOB Price: $8.2 / 8.8
Type:Trading Company
inquiryProduct name: Nikethamide CAS No.:59-26-7 Molecule Formula:C10H14N2O Molecule Weight:178.23 Purity: 99.0% Package: 200kg/drum Description:Clear colorless to yellow liquid Manufacture Standards:Enterprise Standard T
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:59-26-7
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:59-26-7
Min.Order:0
Negotiable
Type:Trading Company
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
N,N-DIETHYLNICOTINAMIDE Chemical Properties Melting point 23 °C (lit.) Boiling point 296-300 °C (lit.) density 1.06 g/mL at 25 °C (lit.) refractive index n20/D 1.524(lit.) Fp >230 °F form Liquid pka pKa 3
Cas:59-26-7
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
3-Bromopyridine
carbon monoxide
diethylamine
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 105℃; under 3000.3 Torr; for 12h; | 92% |
With (1,3,5-triaza-7-phosphaadamantan-1-ium-1-yl)butane-1-sulfonate; palladium diacetate; triethylamine In N,N-dimethyl-formamide at 20 - 60℃; under 2068.65 Torr; for 24h; Inert atmosphere; Autoclave; chemoselective reaction; | 92% |
With palladium diacetate; sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 100℃; for 16h; Sealed tube; | 75% |
Conditions | Yield |
---|---|
With hydrogenchloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In 1,4-dioxane at 120℃; for 33h; | 92% |
3-(N,N-diethylcarbamoyl)pyridine 1-oxide
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With (4,4′-di-tert-butyl-2,2′-bipyridine)bis[(2-pyridinyl)phenyl]iridium(III) hexafluorophosphate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 2.5h; Inert atmosphere; Irradiation; chemoselective reaction; | 92% |
Conditions | Yield |
---|---|
at 210℃; for 1h; | 88% |
Conditions | Yield |
---|---|
Stage #1: diethylamine With n-butyllithium In tetrahydrofuran at -78 - 0℃; for 0.833333h; Stage #2: methyl 3-pyridinecarboxylate In tetrahydrofuran at -78 - 20℃; for 2h; | 84% |
potassium tert-butylate at 285℃; under 22502.3 Torr; for 0.0116667h; autoclave; Industry scale; Microwave irradiation; |
Conditions | Yield |
---|---|
With cesiumhydroxide monohydrate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 80℃; for 24h; Glovebox; Inert atmosphere; Sealed tube; | 79% |
Conditions | Yield |
---|---|
Stage #1: nicotinic acid With niobium pentachloride In 1,4-dioxane Stage #2: diethylamine In 1,4-dioxane at 45 - 50℃; for 12h; | 73% |
With phosphorus pentoxide | |
With phosphorus pentoxide; benzene | |
With trichlorophosphate | |
With N,N'-ethylenethiourea; bis(trichloromethyl) carbonate at 70℃; for 1h; Temperature; Reagent/catalyst; Green chemistry; |
Conditions | Yield |
---|---|
With triethylamine at 20℃; for 0.0166667h; | 72% |
With silica gel; triethylamine; p-toluenesulfonyl chloride at 20℃; for 0.0166667h; | 70% |
With phosphorus pentachloride |
carbon monoxide
3-pyridylboronic acid
triethylamine
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With copper(l) iodide; oxygen; palladium dichloride In acetonitrile at 100℃; under 1520.1 Torr; for 12h; Autoclave; High pressure; | 62% |
N,N-dimethylnicotinamide
lithium diethylamide
A
N,N-Dimethyl-4-(pyridine-3-carbonyl)-nicotinamide
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
In diethyl ether for 5h; Ambient temperature; | A 6% B 60% |
N,N-dimethylnicotinamide
A
N,N-Dimethyl-4-(pyridine-3-carbonyl)-nicotinamide
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With lithium diethylamide In diethyl ether for 5h; Ambient temperature; | A 6% B 60% |
N,N-dimethylnicotinamide
lithium diethylamide
A
N,N-Dimethyl-4-(pyridine-3-carbonyl)-nicotinamide
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
In ethanol for 5h; Product distribution; Ambient temperature; | A 6% B 60% C n/a |
3-pyridinecarboxylic acid ethyl ester
dimethyl amine
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
sodium methylate In ethylene glycol at 85℃; for 25h; Conversion of starting material; | 37% |
3-pyridinecarboxylic acid ethyl ester
hexaethylphosphoric triamide
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
at 210 - 220℃; for 2h; | 34.8% |
3-pyridinecarbonyl chloride
diethyl amine hydrochloride
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
Erhitzen des Reaktionsprodukts auf 180grad; |
3-Bromopyridine
carbon monoxide
diethylamine
A
N,N-diethyl-α-oxo-3-pyridineacetamide
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
PdCl2(PMePh2)2 at 100℃; under 7600 Torr; for 63h; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With pyridine In toluene at 60 - 90℃; for 4h; | |
With triethylamine In dichloromethane at 20℃; for 0.5h; |
4-chloro-N,N-diethyl-3-pyridinecarboxamide
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With hydrogen; palladium |
pyridine-3-carbonyl chloride hydrochloride
diethylamine
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
In dichloromethane |
Conditions | Yield |
---|---|
at 200℃; |
3-iodopyridine
carbon monoxide
diethylamine
A
N,N-diethyl-α-oxo-3-pyridineacetamide
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With potassium phosphate; chloromethyl(1,5-cyclooctadiene)palladium(II) In 1,4-dioxane at 100℃; under 7600 Torr; for 15h; | |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane at 100℃; for 3h; Inert atmosphere; Schlenk technique; |
propylamine
α-(3-pyridyl)-α-(4-morpholino)acetonitrile
B
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With nickel(IV) oxide In tetrahydrofuran at 20℃; for 16h; | A 97 % Chromat. B n/a |
Diethyl-carbamic acid 3-diethylcarbamoyl-pyridin-4-yl ester
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaOMe; 2.) POCl3 / 1.) MeOH 2: H2 / Pd View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2, pyridine / toluene / 1 h / 90 °C 2: pyridine / toluene / 4 h / 60 - 90 °C View Scheme |
Conditions | Yield |
---|---|
With trifluoroacetic acid In water; acetonitrile | |
Multi-step reaction with 2 steps 1: thionyl chloride / toluene; N,N-dimethyl-formamide / 20 °C 2: triethylamine / dichloromethane / 0.5 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.25h; | 99% |
With diethyl ether; diisobutylaluminium hydride |
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With 1,1,2-trichloroethane; palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 760.051 Torr; for 46h; | 99% |
N,N-diethylnicotinamide
N,N-diethyl-α,α-dichloro-3-pyridylmethylamine
Conditions | Yield |
---|---|
With oxalyl dichloride In tert-butyl methyl ether at 20℃; for 5h; Heating / reflux; | 95% |
With oxalyl dichloride In tert-butyl methyl ether at 20℃; for 5h; Inert atmosphere; Reflux; | 95% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C10H10FN3O With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 95% |
Conditions | Yield |
---|---|
In acetonitrile for 18h; Heating; | 94% |
N,N-diethylnicotinamide
2,2,2-Trichloroethyl chloroformate
Conditions | Yield |
---|---|
Stage #1: 2-(1-(4-methoxyphenyl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane With (3,5-bis(trifluoromethyl)phenyl)lithium In tetrahydrofuran at -78℃; Stage #2: N,N-diethylnicotinamide; 2,2,2-Trichloroethyl chloroformate In tetrahydrofuran at -40℃; diastereoselective reaction; | 94% |
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
With nickel at 180 - 190℃; for 10h; | 93.2% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: 2-diazo-N-methyl-N-phenylpropanamide With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 93% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C10H10BrN3O With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 93% |
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
Stage #1: sodium coumarilate; N,N-diethylnicotinamide In ethanol; water at 20℃; for 0.5h; Stage #2: copper(II) nitrate trihydrate In ethanol at 55℃; for 3h; Stage #3: In ethanol at 20℃; for 840h; | 92% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C10H10ClN3O With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 91% |
Conditions | Yield |
---|---|
at 20℃; for 360h; | 90.4% |
1,1-bis(trimethylsiloxy)-2-methylprop-1-ene
N,N-diethylnicotinamide
methyl chloroformate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | 90% |
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
In water soln. of diethylnicotinamide in H2O added dropwise with stirring to soln. of p-chlorobenzoate in hot H2O; soln. heated to 50°C and stirred for 4 h; cooled to room temp.; allowed to stay 10-12 ds for crystn.; filtered; washed (cold water, acetone); dried (vac.); elem. anal.; | 90% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C11H13N3O With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 90% |
2-diazo-N-methyl-N-phenylacetamide
N,N-diethylnicotinamide
Allyl chloroformate
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: 2-diazo-N-methyl-N-phenylacetamide With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 90% |
bromoacetic acid (-)-8-phenylmenthol ester
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
at 90℃; | 89% |
N,N-diethylnicotinamide
α-deuterio-3-pyridinecarboxaldehyde
Conditions | Yield |
---|---|
With zirconocene dichloride; diisobutylaluminium deuteride In tetrahydrofuran at 0 - 23℃; | 89% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel(0); C85H88N2O2; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum at 135℃; for 18h; Inert atmosphere; Glovebox; regioselective reaction; | 89% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide; Allyl chloroformate In tetrahydrofuran at -20℃; for 0.166667h; Molecular sieve; Stage #2: C11H13N3O2 With bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at -20℃; for 13h; diastereoselective reaction; | 88% |
Conditions | Yield |
---|---|
Stage #1: N,N-diethylnicotinamide With boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: o-TolMgBr·LiCl In tetrahydrofuran at -30℃; for 2h; Inert atmosphere; Stage #3: With chloranil In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; regioselective reaction; | 87% |
(S)-4,4,5,5-tetramethyl-2-(1-phenylpropyl)-1,3,2-dioxaborolane
N,N-diethylnicotinamide
2,2,2-Trichloroethyl chloroformate
Conditions | Yield |
---|---|
Stage #1: (S)-4,4,5,5-tetramethyl-2-(1-phenylpropyl)-1,3,2-dioxaborolane With (3,5-bis(trifluoromethyl)phenyl)lithium In tetrahydrofuran at -78℃; Stage #2: N,N-diethylnicotinamide; 2,2,2-Trichloroethyl chloroformate In tetrahydrofuran at -40℃; diastereoselective reaction; | 87% |
Conditions | Yield |
---|---|
With ZrIII6(μ3-O)4(μ3-ONa)4H6Na6(1,3,5-benzenetricarboxylate)2 at 90℃; for 18h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 87% |
With ammonium tetraphenylborate In [D3]acetonitrile at 90℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; regioselective reaction; | 79% |
N,N-diethylnicotinamide
Conditions | Yield |
---|---|
Stage #1: sodium coumarilate; N,N-diethylnicotinamide In ethanol; water at 20℃; for 0.5h; Stage #2: zinc(II) nitrate hexahydrate In ethanol at 55℃; for 3h; Stage #3: In ethanol at 20℃; for 840h; | 87% |
Conditions | Yield |
---|---|
With n-butyllithium; borane-THF; diisopropylamine at 65℃; for 2h; | 86% |
With phenylsilane; potassium hydroxide In neat (no solvent) at 20℃; for 16h; | 80% |
With diethylzinc; lithium chloride In tetrahydrofuran; hexane at 20℃; for 24h; Catalytic behavior; Inert atmosphere; chemoselective reaction; | 72% |
N,N-diethylnicotinamide
Zn(p-chlorobenzoate)2(diethylnicotinamide)2(H2O)2
Conditions | Yield |
---|---|
In water soln. of diethylnicotinamide in H2O added dropwise with stirring to soln. of p-chlorobenzoate in hot H2O; soln. heated to 50°C and stirred for 4 h; cooled to room temp.; allowed to stay 10-12 ds for crystn.; filtered; washed (cold water, acetone); dried (vac.); elem. anal.; | 86% |
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