As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:1067-12-5
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inquiryAbout Product Details Item Specification Test Results Appearance White crystalline powder Conform
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Min.Order:1 Kilogram
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inquiryphosphinylidynetrimethanol CAS:1067-12-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryProduct Name: phosphinylidynetrimethanol Synonyms: phosphinylidynetrimethanol;Tris(hydroxymethyl)phosphine oxide;Phosphinylidynetrismethanol CAS: 1067-12-5 MF: C3H9O3P MW: 124.075521 Appearance:powder Sto
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Min.Order:1 Gram
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inquiryTIANFUCHEM--1067-12-5---phosphinylidynetrimethanol Application:TIANFUCHEM--1067-12-5---phosphinylidynetrimethanol
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inquiryMethanol,1,1',1''-phosphinylidynetris- cas 1067-12-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 50℃; for 2h; Elimination; | 100% |
With barium carbonate In water | |
With sodium hydroxide | |
With sodium hydroxide; dihydrogen peroxide at 70 - 80℃; for 1h; | |
With sodium hydroxide at 20℃; Rate constant; |
Conditions | Yield |
---|---|
With air at 80℃; for 5h; Reagent/catalyst; Temperature; | 95% |
With dihydrogen peroxide | |
With oxygen at 50 - 60℃; for 5h; Green chemistry; | 220 g |
With dihydrogen peroxide In water at 20℃; | |
With air In water; toluene at 90℃; for 16h; |
Conditions | Yield |
---|---|
Stage #1: formaldehyd With phosphan In 5,5-dimethyl-1,3-cyclohexadiene at 68℃; under 30003 Torr; for 3h; Inert atmosphere; Autoclave; Large scale; Stage #2: With dihydrogen peroxide In 5,5-dimethyl-1,3-cyclohexadiene at 55℃; for 5h; Solvent; Pressure; Temperature; Inert atmosphere; Large scale; | 95% |
tetrakis(hydroxymethyl)phosphonium sulfate
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
Stage #1: tetrakis(hydroxymethyl)phosphonium sulfate With barium(II) hydroxide In water at 60℃; Stage #2: With dihydrogen peroxide In water at 20℃; | 94% |
diiodotris<(trimethylsiloxy)methyl>phosphorane
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With methanol | 93% |
1-iodo-butane
tris(hydroxymethyl)phosphine
A
tri(hydroxymethyl)phosphine oxide
B
butyl bis(hydroxymethyl)phosphineoxide
Conditions | Yield |
---|---|
Stage #1: 1-iodo-butane; tris(hydroxymethyl)phosphine In methanol at 0 - 70℃; for 4.5h; Inert atmosphere; Schlenk technique; Stage #2: With triethylamine at 60℃; for 1h; Inert atmosphere; Schlenk technique; Stage #3: With dihydrogen peroxide In methanol for 2h; | A 12% B 45% |
tetrakis(hydroxymethyl)phosphonium chloride
A
tri(hydroxymethyl)phosphine oxide
B
tris(hydroxymethyl)phosphine
Conditions | Yield |
---|---|
Stage #1: tetrakis(hydroxymethyl)phosphonium chloride With sodium hydroxide In ethanol at 20℃; for 1.25h; Stage #2: With 4 A molecular sieve; potassium carbonate for 6h; | A 20% B n/a |
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
Stage #1: tetrakis(hydroxymethyl)phosphonium sulphate With sodium hydroxide Stage #2: | 0.1% |
chlorure de tetrakis(hydroxymethyl)phosphonium
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol |
chlorure de tetrakis(hydroxymethyl)phosphonium
A
tri(hydroxymethyl)phosphine oxide
B
tris(hydroxymethyl)phosphine
Conditions | Yield |
---|---|
With sodium hydroxide |
tris<(trimethylsiloxy)methyl>phosphine
A
tri(hydroxymethyl)phosphine oxide
B
tris(chloromethyl)phosphine oxide
C
bis(chloromethyl)(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With methanol; chlorine 1) CH2Cl2, 20 deg C, 1 h, 2) 20 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given; |
tris<(trimethylsiloxy)methyl>phosphine oxide
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With hydrogenchloride; methanol 1) C6H6; Yield given. Multistep reaction; |
dichlorotris<(trimethylsiloxy)methyl>phosphorane
A
methylene chloride
B
Methoxytrimethylsilane
C
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With methanol In dichloromethane at -70℃; Yield given; |
dibromotris<(trimethylsiloxy)methyl>phosphorane
A
Methoxytrimethylsilane
B
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With methanol In dichloromethane at -70℃; Yield given; |
tri(hydroxymethyl)phosphine oxide
1,4-dioxo-2,6,7-trioxa-1,4-diphosphabicyclo[2.2.2]octane
Conditions | Yield |
---|---|
With sodium methylate; phosphorous acid trimethyl ester at 150℃; for 5h; Temperature; Reagent/catalyst; Inert atmosphere; | 96.2% |
With trimethyl phosphite; sodium methylate at 150℃; for 6h; Reagent/catalyst; Temperature; Inert atmosphere; | 95.5% |
With trichlorophosphate In 1,4-dioxane; water at 10 - 100℃; for 6h; Solvent; Temperature; | 95.3% |
With phosphoric acid triphenyl ester; sodium methylate at 150℃; for 8h; Reagent/catalyst; Temperature; Inert atmosphere; | 93.2% |
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With pyridine; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine at 130℃; for 5h; Reagent/catalyst; Temperature; Inert atmosphere; | 96.1% |
Conditions | Yield |
---|---|
With sodium methylate; methoxybenzene at 150℃; for 5h; Reagent/catalyst; Temperature; Inert atmosphere; | 95.9% |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene at 20 - 140℃; for 6h; Solvent; Temperature; | 95.3% |
Conditions | Yield |
---|---|
In diethylene glycol dimethyl ether at 40 - 130℃; for 13h; Solvent; Temperature; | 95.3% |
tri(hydroxymethyl)phosphine oxide
Conditions | Yield |
---|---|
With phosphorus trichloride In acetonitrile at 0 - 80℃; for 4h; Reagent/catalyst; Temperature; | 94.4% |
With triphenyl phosphite; sodium methylate at 150℃; for 7h; Temperature; Reagent/catalyst; Inert atmosphere; | 94.7% |
Conditions | Yield |
---|---|
at 20 - 160℃; for 7h; Temperature; Inert atmosphere; | 94.2% |
Conditions | Yield |
---|---|
With phosphorus pentachloride In chloroform at 60℃; Chlorination; | 86% |
With pyridine; thionyl chloride | |
With hydrogenchloride at 180 - 200℃; for 8h; Yield given; |
Conditions | Yield |
---|---|
Stage #1: tri(hydroxymethyl)phosphine oxide With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 35℃; Green chemistry; Stage #2: 3-chloroprop-1-ene In water at 0 - 50℃; for 12h; Green chemistry; | 80% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 0 - 45℃; for 12h; | 75% |
Conditions | Yield |
---|---|
Stage #1: tri(hydroxymethyl)phosphine oxide With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 35℃; Williamson Ether Synthesis; Stage #2: propargyl bromide In water; toluene at 0 - 50℃; for 12h; Williamson Ether Synthesis; | 62.9% |
Conditions | Yield |
---|---|
With pyridine at 20℃; for 20h; | 51% |
tri(hydroxymethyl)phosphine oxide
4,4'-dimethoxytrityl chloride
Conditions | Yield |
---|---|
With pyridine at 20℃; for 20h; | 50% |
tri(hydroxymethyl)phosphine oxide
sirolimus
(21E,23E,25E,26E,31R,32S,33R,34R,36S,38S,41S,42R,43R,52R)-40-[bis(hydroxymethyl)phosphorylmethoxy]-42,52-dihydroxy-41-[(1R)-2-[(1S,3R,4R)-4-hydroxy-3-methoxy-cyclohexyl]-1-methyl-ethyl]-43-methoxy-31,32,33,34,44,45-hexamethyl-65,66-dioxa-53-azatricyclohexatriaconta-21,23,25(44),26(45)-tetraene-46,47,48,49,50-pentone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In tetrahydrofuran; water at 25℃; for 4h; | 9% |
n-dodecanoyl chloride
tri(hydroxymethyl)phosphine oxide
tris-lauroyloxymethyl-phosphine oxide
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
With sodium hydroxide |
1-bromo-butane
tri(hydroxymethyl)phosphine oxide
tris-butoxymethyl-phosphane oxide
Conditions | Yield |
---|---|
(i) NaOMe, benzene, (ii) /BRN= 1098260/; Multistep reaction; |
methyl bromide
tri(hydroxymethyl)phosphine oxide
tris-methoxymethyl-phosphane oxide
Conditions | Yield |
---|---|
(i) NaOMe, benzene, (ii) /BRN= 1209223/, toluene; Multistep reaction; |
ethyl bromide
tri(hydroxymethyl)phosphine oxide
tris(ethoxymethyl)phosphine oxide
Conditions | Yield |
---|---|
(i) NaOMe, benzene, (ii) /BRN= 1209224/, toluene; Multistep reaction; |
formaldehyd
tri(hydroxymethyl)phosphine oxide
(5-oxo-5λ5-[1,3,5]dioxaphosphinan-5-yl)-methanol
Conditions | Yield |
---|---|
at 180 - 200℃; |
chloro-trimethyl-silane
tri(hydroxymethyl)phosphine oxide
tris<(trimethylsiloxy)methyl>phosphine oxide
1-Bromopentane
tri(hydroxymethyl)phosphine oxide
tris-pentyloxymethyl-phosphane oxide
Conditions | Yield |
---|---|
(i) NaOMe, benzene, (ii) /BRN= 1730981/; Multistep reaction; |
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