CAS No.556-64-9,Methyl thiocyanate Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Methyl thiocyanate

Cas:556-64-9

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Methyl thiocyanate

Cas:556-64-9

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality Appearance: CLEAR COLOURLESS TO LIGHT YELLOW LIQUID Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used in synthetic pesticides

Methyl thiocyanate

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Methyl thiocyanate

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Henan Tianfu Chemical Co., Ltd.

Methane, thiocyanato-;Methyl sulfocyanate;methylrhodanate;Methylrhodanid;Methylsalfocyanate;methylsulfocyanate;Methylthiokyanat CAS No.: 556-64-9 Molecular formula: C2H3NS Molecular weight: 73.12 Methyl thiocyanate Melting point -5 &d

Methyl sulfocyanate

Cas:556-64-9

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Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Methyl Thiocyanate

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

thiocyanatoMethane

Cas:556-64-9

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Methyl Thiocyanate

Cas:556-64-9

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 556-64-9 with competitive price

Cas:556-64-9

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Antimex Chemical Limied

Methyl thiocyanateAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier

Methyl thiocyanate

Cas:556-64-9

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Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

Methyl thiocyanate

Cas:556-64-9

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HENAN SUNLAKE ENTERPRISE CORPORATION

Methyl thiocyanate Basic information Product Name: Methyl thiocyanate

556-64-9 C2H3NS Methyl thiocyanate

Cas:556-64-9

Min.Order:100 Gram

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Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

Methyl Thiocyanate

Cas:556-64-9

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Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

Methyl thiocyanate

Cas:556-64-9

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Nanjing Chemlin Chemical Co., Ltd.

please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant information Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place Package:as your needs A

Methyl thiocyanate

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GZ HONESTCHEM CO., LTD

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

thiocyanatoMethane

Cas:556-64-9

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Shanghai Haoyuan Chemexpress Co., Ltd.

Methyl thiocyanate

Cas:556-64-9

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yuyongmei

YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a

Thiocyanic acid, methylester

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Parish Chemical Company

Methyl thiocyanate

Cas:556-64-9

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Synthetic route

: 333-20-0
potassium thioacyanate

: 74-88-4
methyl iodide

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
With poly(vinylbenzyltriphenylphosphonium chloride) In benzene for 2h; Heating;	88%

: 75532-40-0
dimethyl phosphoroisothiocyanatidite

: 431-03-8
dimethylglyoxal

A: 556-64-9
methyl thiocyanate

B: 933-43-7
2-methoxy-4,5-dimethyl-[1,3,2]dioxaphosphole 2-oxide

Conditions

Conditions	Yield
In dichloromethane at 0℃;	A n/a B 80%

...Expand

: 59103-08-1
3-methylsulfanyl-5,6-diphenyl-[1,4,2]dithiazine

A: 556-64-9
methyl thiocyanate

B: 23181-79-5
2,3,5,6-tetraphenyl-1,4-dithia-2,5-cyclohexadiene

C: 501-65-5
diphenyl acetylene

Conditions

Conditions	Yield
In dichloromethane for 4h; Irradiation;	A n/a B 72% C n/a
In dichloromethane for 8h; Quantum yield; Mechanism; Irradiation;

...Expand

: 2911-22-0
6-methyl-4-oxo-2-thioxo-3,4-dihydro-2H-1,3-oxazine

: 74-88-4
methyl iodide

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
With potassium carbonate In acetone for 1h; Ambient temperature;	64%

: 79306-34-6
1-azido-2,2-dimethylcyclopropyl methylsulfide

A: 556-64-9
methyl thiocyanate

B: 2-(methylthio)-4,4-dimethyl-1-azetine

C: 79780-50-0
2-(methylthio)-3,3-dimethyl-1-azetine

D: 115-11-7
isobutene

Conditions

Conditions	Yield
In tetrachloromethane for 3h; Heating;	A 30% B 6% C 63% D n/a
In tetrachloromethane for 3h; Rate constant; Heating;	A 30% B 6% C 63% D n/a
In tetrachloromethane for 3h; Heating;

...Expand

: 83319-07-7
C19H18NS(1+)*CNS(1-)

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
at 240℃;	52%

poly(N-methyl-4-vinyl-pyridinium)thiocyanate: poly(N-methyl-4-vinyl-pyridinium)thiocyanate

: 74-88-4
methyl iodide

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
In hexane at 20℃; for 72h;	50%

: 333-20-0
potassium thioacyanate

: S-methylthiolanium fluorosulphate

A: 110-01-0
thiophene

B: 556-64-9
methyl thiocyanate

C: 4430-36-8
erucin

D: 41756-12-1
4-(methylthio)butyl thiocyanate

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 70℃; for 7h; Yields of byproduct given;	A n/a B n/a C n/a D 45%

...Expand

: 333-20-0
potassium thioacyanate

: S-methylthietanium fluorosulphate

A: 556-64-9
methyl thiocyanate

B: 15394-33-9
methyl 4-(methylsulfanyl)butyl sulfide

C: 86702-84-3
3-(methylthio)propyl thiocyanate

D: 103707-78-4
1-(4-Methylsulfanyl-butylsulfanyl)-4-thiocyanato-butane

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 60℃; for 1.5h;	A 20% B 7% C 25% D 18%

...Expand

: 333-20-0
potassium thioacyanate

: S-methylthianium fluorosulphate

A: 1613-51-0
sulfure de pentamethylene

B: 556-64-9
methyl thiocyanate

C: 1-Methylsulfanyl-5-thiocyanato-pentane

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 80℃; for 5h; Yields of byproduct given;	A n/a B n/a C 4%

...Expand

: 186581-53-3, 908094-01-9
diazomethane

: 463-56-9
thiocyanic acid

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
With diethyl ether at -5℃;

: 67-56-1
methanol

: 463-56-9
thiocyanic acid

: 13118-32-6
p-nitrophenyldimethylsulphonium methylsulphate

A: 556-64-9
methyl thiocyanate

B: 701-57-5
1-methylthio-4-nitro-benzene

Conditions

Conditions	Yield
at 25 - 45℃; Rate constant;

...Expand

: 75-18-3
dimethylsulfide

: 506-68-3
bromocyane

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
at 100℃; im geschlossenen Rohr;

: 506-68-3
bromocyane

: 766-92-7
[(methylthio)methyl]-benzene

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
at 60 - 70℃;

: 506-68-3
bromocyane

: 766-92-7
[(methylthio)methyl]-benzene

A: 556-64-9
methyl thiocyanate

B: 100-39-0
benzyl bromide

Conditions

Conditions	Yield
at 60 - 70℃; im Rohr;

...Expand

: 35266-49-0
methoxycarbonylisothiocyanate

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
beim Erhitzen;

: bis-methylsulfanylcarboximidoyl-diazene

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
at 110℃;

: bis-methylsulfanylcarboximidoyl-diazene

A: 556-64-9
methyl thiocyanate

B: 74586-16-6
S,S'-dimethyl-dithiodiisobiurea

C: 624-92-0
Dimethyldisulphide

D: 460-19-5
ethanedinitrile

Conditions

Conditions	Yield
at 110℃; Zersetzen; Produkt 5: 5-Methylmercapto-3-imino-1.2.4-triazolidin;

...Expand

: 333-20-0
potassium thioacyanate

: 75-58-1
tertamethylammonium iodide

A: 556-64-9
methyl thiocyanate

B: 556-61-6
methyl thioisocyanate

C: 75-50-3
trimethylamine

Conditions

Conditions	Yield
at 210℃;

...Expand

: 15597-46-3
tetramethylammonium thiocyanate

A: 556-64-9
methyl thiocyanate

B: 75-50-3
trimethylamine

Conditions

Conditions	Yield
at 304 - 305℃;

: 333-20-0
potassium thioacyanate

: 77-78-1
dimethyl sulfate

: 556-64-9
methyl thiocyanate

: 2092-17-3
barium thiocyanate

: 77-78-1
dimethyl sulfate

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
With water

: 1701-93-5
silver thiocyanate

: 74-88-4
methyl iodide

: 556-64-9
methyl thiocyanate

: 4818-24-0
3-methylsulfanyl-5,6,7,8-tetrahydro-benzo[1,4,2]dithiazine

A: 556-64-9
methyl thiocyanate

B: 501-65-5
diphenyl acetylene

Conditions

Conditions	Yield
In dichloromethane for 8h; Quantum yield; Irradiation;

: 29897-71-0
2,4,6-tricyanoanisole

A: 556-64-9
methyl thiocyanate

B: potassium 2,4,6-tricyanophenolate

Conditions

Conditions	Yield
With potassium thioacyanate In dimethyl sulfoxide Product distribution; Mechanism;

: 51404-78-5
dimethyl-p-tolylsulfonium tetrafluoroborate

A: 556-64-9
methyl thiocyanate

B: 623-13-2
4-methylphenyl methylsulfide

Conditions

Conditions	Yield
With cyclophane (1); HPLC buffer; potassium thioacyanate at 45.9℃; Rate constant; pD 9; without cyclophanes;

: 33613-52-4
dimethylphenyl sulfonium tetrafluoroborate

A: 556-64-9
methyl thiocyanate

B: 100-68-5
methyl-phenyl-thioether

Conditions

Conditions	Yield
With cyclophane (1); HPLC buffer; potassium thioacyanate at 45.9℃; Rate constant; pD 9; without cyclophanes;

: 78949-38-9
methyl phosphorodiisothiocyanatidite

: 3735-81-7
Phosphoric acid dimethyl ester 2,2,2-trichloro-ethyl ester

: 556-64-9
methyl thiocyanate

Conditions

Conditions	Yield
Product distribution;

: dimethyl(p-fluorophenyl)sulfonium tetrafluoroborate

A: 556-64-9
methyl thiocyanate

B: 371-15-3
p-fluorothioanisole

Conditions

Conditions	Yield
With cyclophane (1); HPLC buffer; potassium thioacyanate at 45.9℃; Rate constant; pD 9; without cyclophanes;

: dimethyl(p-chlorophenyl)sulfonium tetrafluoroborate

A: 556-64-9
methyl thiocyanate

B: 123-09-1
4-chlorophenyl methyl sulfide

Conditions

Conditions	Yield
With cyclophane (1); HPLC buffer; potassium thioacyanate at 45.9℃; Rate constant; pD 9; without cyclophanes;

: 556-64-9
methyl thiocyanate

: 521287-10-5
ethyl 2-amino-6-cyanoindole-3-carboxylate

: 722485-03-2
ethyl 5-cyano-2-(methylsulfanylimidoylamino)-1H-indole-3-carboxylate hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In 1,4-dioxane at 20 - 60℃;	100%

: 556-64-9
methyl thiocyanate

: 1192739-52-8
C13H21NO

: 1192739-72-2
2-cyclohexyl-4-(methylthio)-5,6,7,8-tetrahydroquinazoline

Conditions

Conditions	Yield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 23℃; Inert atmosphere;	100%

: 556-64-9
methyl thiocyanate

: 100-20-9
terephthaloyl chloride

: 125077-76-1
2,2'-(1,4-Phenylen)bis<4,6-bis(methylthio)-1,3,5-oxadiazinium>-dihexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane for 2h; Ambient temperature;	98%

: 556-64-9
methyl thiocyanate

: 122-01-0
4-chloro-benzoyl chloride

: 2-(4-Chlorphenyl)-4,6-bis(methylthio)-1,3,5-oxadiazinium-hexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane at 0℃; for 1h;	97%

: 556-64-9
methyl thiocyanate

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 125077-78-3
2,2'-(1,3-Phenylen)bis<4,6-bis(methylthio)-1,3,5-oxadiazinium>-dihexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane for 2h; Ambient temperature;	97%

: 556-64-9
methyl thiocyanate

: 5299-98-9
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

: 330808-35-0
3-methyl-2-thiomethyl-5-(2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-2,4-pentadienenitrile

Conditions

Conditions	Yield
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -85℃;	97%

: 556-64-9
methyl thiocyanate

: 18228-46-1
1-(p-methoxyphenyl)-2-methylpropan-1-ol

: S-methyl N-[1-(4-hydroxyphenyl)-2-methylprop-2-yl]thiocarbamate

Conditions

Conditions	Yield
With sulfuric acid In toluene Ritter reaction;	97%

: 556-64-9
methyl thiocyanate

: 20638-88-4
9-trans-13-trans-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-7,9,11,13-nonatetraene-15-nitrile

: 3,7-dimethyl-2-thiomethyl-9-(2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-2,4,6,8-nonatetraenenitrile

Conditions

Conditions	Yield
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -85℃;	96%

: 556-64-9
methyl thiocyanate

: 32974-66-6
1-[(1-chloro-1-methylethyl)azo]-2,4,6-trichlorobenzene

: 2,3-Dimethyl-5-methylthio-1-(2,4,6-trichlorophenyl)-1H-1,2,4-triazolium Hexachloroantimonate

Conditions

Conditions	Yield
With antimonypentachloride In dichloromethane at -60 - 23℃;	95%

: 556-64-9
methyl thiocyanate

: 10533-37-6
potassium O,O-diisopropyl phoshorodithioate

: 22907-64-8
O,O-diisopropyl S-methyl phosphorothioate

Conditions

Conditions	Yield
at 90 - 100℃; for 2.5h;	95%

: 556-64-9
methyl thiocyanate

: 10533-36-5
diisopropyl monothiophosphoric acid, sodium salt

: 22907-64-8
O,O-diisopropyl S-methyl phosphorothioate

Conditions

Conditions	Yield
at 90 - 100℃; for 2.5h;	95%

: 556-64-9
methyl thiocyanate

: 122-04-3
4-nitro-benzoyl chloride

: 2,4-Bis(methylthio)-6-(4-nitrophenyl)-1,3,5-oxadiazinium-hexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane at 0℃; for 1h;	95%

: 556-64-9
methyl thiocyanate

: 107-56-2
O,O-diisopropyl hydrogen phosphorodithioate

: 69674-00-6
diisopropoxythiophosphoryl isothiocyanate

Conditions

Conditions	Yield
at 100℃; for 3h;	95%

: 556-64-9
methyl thiocyanate

: 2253-43-2
O.O-Dipropyl-dithyophosphat

: 61680-00-0
O,O-dipropyl phosphoroisothiocyanatidothioate

Conditions

Conditions	Yield
at 100℃; for 3h;	95%

: 556-64-9
methyl thiocyanate

: 523-80-8
apiol

: 4,9-dimethoxy-7-methyl-5-methylsulfanyl-7,8-dihydro[1,3]dioxolo[4,5g]isoquinoline

Conditions

Conditions	Yield
With trifluorormethanesulfonic acid In chloroform for 0.25h; Reagent/catalyst; Ritter Amidation; Reflux;	95%

: 556-64-9
methyl thiocyanate

: 20939-15-5
4-amino-5-methyl-2,4-dihydro-[1,2,4]triazole-3-thione

: 13228-91-6
3-methyl-6-methylsulfanyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Conditions

Conditions	Yield
With PPA for 6h; boiling water bath;	94%

: 556-64-9
methyl thiocyanate

: 22288-78-4
Methyl 3-aminothiophene-2-carboxylate

: 176530-46-4
2-(methylthio)thieno[3,2-d]pyrimidin-4(3H)-one

Conditions

Conditions	Yield
With hydrogenchloride In 1,4-dioxane at 90℃; for 24h; Sealed tube;	94%

: 556-64-9
methyl thiocyanate

: 697288-02-1
dimethyl 2-(3-phenyl-3-butenyl)-2-(2-propynyl)malonate

: dimethyl 2-(3-methylthio-2-propynyl)-2-(3-phenyl-3-butenyl)malonate

Conditions

Conditions	Yield
Stage #1: dimethyl 2-(3-phenyl-3-butenyl)-2-(2-propynyl)malonate With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: methyl thiocyanate In tetrahydrofuran; hexane at -78 - 20℃; for 17h;	93.4%

: 556-64-9
methyl thiocyanate

: 2873-74-7
gloutaric dichloride

: 125077-70-5
2,2'-(1,3-Propandiyl)bis<4,6-bis(methylthio)-1,3,5-oxadiazinium>-dihexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane for 2h; Ambient temperature;	93%

: 556-64-9
methyl thiocyanate

: 3454-66-8
potassium O,O-diethyldithiophosphate

: 3288-58-2
O,O-diethyl S-methyl phosphorodithioate

Conditions

Conditions	Yield
at 100 - 130℃; for 3h;	93%

: 556-64-9
methyl thiocyanate

: 7472-54-0
N-(p-methoxyphenyl)benzamide

: 959217-28-8
6-methoxy-4-(methylthio)-2-phenylquinazoline

Conditions

Conditions	Yield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 140℃; for 0.35h; Inert atmosphere; Microwave irradiation;	93%

: 556-64-9
methyl thiocyanate

: 874-60-2
4-methyl-benzoyl chloride

: 2-(4-Methylphenyl)-4,6-bis(methylthio)-1,3,5-oxadiazinium-hexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane at 0℃; for 1h;	92%

: 556-64-9
methyl thiocyanate

: 372-48-5
2-fluoropyridine

: 2-fluoro-3-methylthiopyridine

Conditions

Conditions	Yield
With lithium diisopropyl amide In tetrahydrofuran at -78 - 0℃; for 2.5h;	92%

: 556-64-9
methyl thiocyanate

: 373-02-4, 14998-37-9, 33025-09-1, 94044-50-5, 98268-31-6
nickel diacetate

: 24246-07-9
methyl 2-(5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetate

: C28H26N6NiO6S2

Conditions

Conditions	Yield
In methanol for 3h; Reflux;	92%

...Expand

: 556-64-9
methyl thiocyanate

: 29515-99-9
5-methylsulfanyl-1H-tetrazole

Conditions

Conditions	Yield
With sodium azide; titanium(IV) dioxide In N,N-dimethyl-formamide at 110℃; for 20h; regiospecific reaction;	91%
Stage #1: methyl thiocyanate With sodium azide In water at 20℃; for 0.5h; Stage #2: With hydrogen bromide In water pH=1-2;	88%
With ammonium azide; N,N-dimethyl-formamide; lithium chloride
With azide(1-)

: 556-64-9
methyl thiocyanate

: 627-63-4
fumaryl dichloride

: 125077-74-9
2,2'-(1,2-Ethendiyl)bis<4,6-bis(methylthio)-1,3,5-oxadiazinium>-dihexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane for 2h; Ambient temperature;	91%

: 556-64-9
methyl thiocyanate

: 7023-78-1
2-diazo-1-(3-chlorophenyl)ethanone

A: 1-(3-chlorophenyl)-2-ethoxyethan-1-one

B: 2-methylthio-5-(m-chlorophenyl)oxazole

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate at 0℃;	A 4% B 91%

...Expand

: 556-64-9
methyl thiocyanate

: 293313-46-9
N-(But-3-ynyl)-N-(4-methylpenta-2,3-dienyl)-4-methylbenzenesulfonamide

: 293313-47-0
N-(4-Methythiobut-3-ynyl)-N-(4-methylpenta-2,3-dienyl)-4-methylbenzenesulfonamide

Conditions

Conditions	Yield
Stage #1: N-(But-3-ynyl)-N-(4-methylpenta-2,3-dienyl)-4-methylbenzenesulfonamide With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.25h; Metallation; Stage #2: methyl thiocyanate In tetrahydrofuran; hexane at -78℃; for 0.5h; Substitution;	91%

: 556-64-9
methyl thiocyanate

: 100-86-7
2-Methyl-1-phenyl-2-propanol

: 132628-97-8
1-methylsulfanyl-3,3-dimethyl-3,4-dihydroisoquinoline

Conditions

Conditions	Yield
With sulfuric acid	90%

: 556-64-9
methyl thiocyanate

: 111-50-2
Adipic acid dichloride

: 125077-72-7
2,2'-(1,4-Butandiyl)bis<4,6-bis(methylthio)-1,3,5-oxadiazinium>-dihexachloroantimonat(V)

Conditions

Conditions	Yield
With antimonypentachloride In tetrachloromethane for 2h; Ambient temperature;	90%

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Synthetic route

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