ISO9001 We have been specializing in organic fluoro chemicals since 1984. We have been supplying it to Europe, USA, Japan, Korea etc. regularly for several years Superiority : 1.ISO certificate 2..Powerful R & D team 3.The abili
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inquiryDayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryHigh quality Trimethylsilyl trifluoromethanesulfonate CAS 27607-77-8 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its int
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inquiryTrimethylsilyl Trifluoro Methane Sulfonate[CAS:27607-77-8] Name Trimethylsilyl trifluoromethanesulfonate Synonyms Trifluoromethanesulfonic acid trimethylsilyl ester; Trimethylsilyl tri
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryhigh purity Storage:Sealed, dry, microtherm , avoid light and smell. Package:meet customer's demand Application:organic synthesis Transportation:by sea or by air Port:shanghai
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryTrimethylsilyl trifluoromethanesulfonate CAS 27607-77-8 Trimethylsilyl triflate CAS no 27607-77-8 Trifluoromethanesulfonic acid trimethylsilyl ester Methanesulfonic acid,1,1,1-trifluoro-, trimethylsilyl ester Trimethylsilyl trifluoromethanes
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inquiryProduct Name: Trimethylsilyl trifluoromethanesulfonate Synonyms: SILANE TMS-TRIFLATE;TMSOTF;TMS TRIFLATE;TRIMETHYLSILYL TRIFLATE;TRIMETHYLSILYL TRIFLUOROMETHANESULFONATE;TRIMETHYLSILYL TRIFLUOROMETHANESULPHONATE;TRIMETHYLSILYL TRIFLUOROMETHYLSULFO
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inquiryProduct Description Product website: http://www.finerchem.com Product Name Trimethylsllytrifluoromethanesulphonate CAS No. 27607-77-8
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryChemical Name: Trimethylsilyl trifluoromethanesulfonate CAS No.: 27607-77-8 Molecular Fomula: C4H9F3O3SSi Chemical Structure: Molecular weight: 222.25 Appearance: colorless or pale yellow liquid Assay: 99.5% Appearance: Colorless L
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inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At pre
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryTrimethylsilyl trifluoromethanesulfonate CAS:27607-77-8 Specification Item Specification Appearance Clear Colorless Liquid Assay 98%min Density 1.228 g/mL at 25 °C (lit.) Boiling Point
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiry1. Well-equipped, stable and high-quality raw material supply chain, to provide customers with the best quality products. 2.Strict quality inspection process and professional certificate testing to ensure the quality level of the final product. 3.E
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryReliable quality 27607-77-8 low price Trimethylsilyl trifluoromethanesulfonate superior manufacturer trimethylsilyl trifluoromethanesulfonate can be used in laboratory research and development processes and chemical and pharmaceutical research and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirytetramethylsilane
trifluorormethanesulfonic acid
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
for 1h; Ambient temperature; | 99% |
3-(trimethylsilyl)-2-oxazolidinone
trifluorormethanesulfonic acid
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 40℃; for 0.25h; | 98% |
for 0.0333333h; | 80% |
chloro-trimethyl-silane
trifluorormethanesulfonic acid
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In n-heptane at 50 - 60℃; for 13h; Large scale; | 96.55% |
for 7h; Heating; Yield given; | |
at 20℃; | |
at 40℃; for 24h; Schlenk technique; Inert atmosphere; |
trifluorormethanesulfonic acid
1-(Trimethylsilyl)imidazole
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In diethyl ether at 10℃; for 1h; | 96% |
(dimethylsilyl)methyl trifluoromethanesulfonate
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 80℃; for 9h; | 95% |
In benzene-d6 at 135℃; Rate constant; Mechanism; τ1/2; | |
In neat (no solvent) at 134.9℃; Rate constant; Thermodynamic data; lgA, EA, ΔH(excit.), ΔS(excit.), ΔG(excit.), ΔrH; | |
at 80℃; Kinetics; Rate constant; |
bis(trimethylsilyl)sulphate
barium trifluoromethanesulfonate
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 140 - 150℃; | 95% |
silver trifluoromethanesulfonate
A
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In benzene-d6 Inert atmosphere; | A 90% B 92% |
Trimethylsilanol
trifluoromethylsulfonic anhydride
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
Stage #1: Trimethylsilanol; trifluoromethylsulfonic anhydride at 45℃; for 3.5h; Stage #2: With chloro-trimethyl-silane at 15℃; for 2.5h; Temperature; | 89% |
Hexamethyldisiloxane
trifluoromethylsulfonic anhydride
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 70 - 75℃; for 2h; | 88% |
trichloromethyltrimethylsilane
trifluorormethanesulfonic acid
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 120℃; for 0.833333h; | 88% |
trifluorormethanesulfonic acid
allyl-trimethyl-silane
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 85% |
In dichloromethane at 0℃; for 2h; |
Trimethylsilanol
trifluoromethane sulfonyl chloride
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 15℃; for 4h; Temperature; | 80% |
2-(trimethylsilyl)propene
trifluorormethanesulfonic acid
A
trimethylsilyl trifluoromethanesulfonate
B
t-butyldimethylsiyl triflate
Conditions | Yield |
---|---|
In pentane at 0℃; for 0.166667h; Yield given; | A n/a B 66% |
In pentane at 0℃; for 0.166667h; Yields of byproduct given; | A n/a B 66% |
trifluorormethanesulfonic acid
(trifluoromethyl)trimethylsilane
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With boron tribromide at -25 - 20℃; | 54% |
trifluorormethanesulfonic acid
(Z)-trimethylsilyl N-trimethylsilylacetimidate
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
for 0.0833333h; | 43% |
trifluorormethanesulfonic acid
trimethylsilyl trichloroacetate
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
for 0.0833333h; | 40% |
trifluorormethanesulfonic acid
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
for 0.0833333h; | 35% |
chloro-trimethyl-silane
Chlorine(I) trifluoromethanesulfonate
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at -111 - 0℃; |
trifluoromethylsulfonic anhydride
methyl trimethylsilyl tert-butylphosphonate
A
trimethylsilyl trifluoromethanesulfonate
B
O-methyl-tert-butylphosphonic trifluoromethanesulfonic anhydride
Conditions | Yield |
---|---|
In dichloromethane for 12h; Ambient temperature; |
N,N,N'-tris(trimethylsilyl)phosphenimidous amide
bis(diisopropylamino)phosphanylium trifluoromethanesulfonate
A
trimethylsilyl trifluoromethanesulfonate
B
N,N,N',N'-tetraisopropyl-1,3-bis(trimethylsilanyl)[1,3,2,4]diazadiphosphetidine-2,4-diamine
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
N,N,N'-tris(trimethylsilyl)phosphenimidous amide
A
trimethylsilyl trifluoromethanesulfonate
B
N,N,N',N'-Tetraethyl-1,3-bis-trimethylsilanyl-[1,3,2,4]diazadiphosphetidine-2,4-diamine
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
μ-oxobis[(trifluoromethanesulfonato)(phenyl)iodine]
4,4-dimethyl-1-(trimethylsilyl)-2-pentyne
A
t-butylallene
B
Hexamethyldisiloxane
C
trimethylsilyl trifluoromethanesulfonate
D
4,4-dimethyl-1-(2-iodophenyl)-2-pentyne
Conditions | Yield |
---|---|
In dichloromethane-d2 at -80℃; Mechanism; or tributylstannyl compound; |
trimethyl(trimethylstannyl)silane
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at -78℃; |
A
trimethylsilyl fluoride
B
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With cesium fluoride In N,N,N,N,N,N-hexamethylphosphoric triamide |
A
trimethylsilyl trifluoromethanesulfonate
B
tert-butylphenylphosphinic trifluoromethanesulfonic anhydride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; |
trifluorormethanesulfonic acid
1-Phenyl-2-(trimethylsilyl)acetylene
A
trimethylsilyl trifluoromethanesulfonate
B
ethylbenzene
Conditions | Yield |
---|---|
With HW(CO)3(C5H5) In dichloromethane-d2 at 22℃; for 0.833333h; Product distribution; other times; without Cp(CO)3WH; | A 91 % Spectr. B 85 % Spectr. C 13 % Spectr. |
trifluorormethanesulfonic acid
Bis(trimethylsilyl)ethyne
A
trimethylsilyl trifluoromethanesulfonate
B
acetylene
Conditions | Yield |
---|---|
With HW(CO)3(C5H5) In dichloromethane-d2 at 22℃; for 0.5h; Product distribution; | A 100 % Spectr. B 48 % Spectr. |
trimethylsilyl trifluoromethanesulfonate
Acetic acid (2R,3R,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-6-[(2S,4aS,8aR)-5-(2-furan-3-yl-ethyl)-1,1,4a,6-tetramethyl-1,2,3,4,4a,7,8,8a-octahydro-naphthalen-2-yloxy]-5-hydroxy-tetrahydro-pyran-4-yl ester
baiyunyl 2-O-trimethylsilyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane for 10h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
(E)-6-((tert-butyldimethylsilyl)oxy)hex-3-en-2-one
(E)-6-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-hexa-1,3-diene
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 0.666667h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
(22E,24R)-3α,5-Cyclo-5α-ergost-7,22-dien-6-one
(22E,24R)-6-Trimethylsiloxy-3α,5-cyclo-5α-ergost-6,22-diene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 0.333333h; | 100% |
trimethylsilyl trifluoromethanesulfonate
1,9-dideoxyforskolin
7β-acetoxy-8,13-epoxy-6β-trimethylsilanyloxy-labd-14-en-11-one
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole In dichloromethane at 20℃; for 72h; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-(phenylsulfinyl)hexan-2-one
Trimethyl-{(E)-1-[1-phenylsulfanyl-meth-(E)-ylidene]-pent-2-enyloxy}-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 2h; Mechanism; Ambient temperature; other β-keto sulfoxides; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane for 2h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-Benzenesulfinyl-decan-2-one
Trimethyl-{(E)-1-[1-phenylsulfanyl-meth-(E)-ylidene]-non-2-enyloxy}-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 2h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-Benzenesulfinyl-4-(4-methoxy-phenyl)-butan-2-one
{(E)-3-(4-Methoxy-phenyl)-1-[1-phenylsulfanyl-meth-(E)-ylidene]-allyloxy}-trimethyl-silane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 2h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
(3Z)-4-(benzoyloxy)-1-(α-furyl)-1-methoxy-3-<(trimethylsilyl)oxy>-1,3-butadiene
Conditions | Yield |
---|---|
With triethylamine In diethyl ether 1.) -78 deg C, 10 min; 2.) room temp., 0.5 h; | 100% |
trimethylsilyl trifluoromethanesulfonate
2,2-dimethyl-6-cycloundecene-4,8-diyn-1-one
<(2,2-dimethyl-6,10-cycloundecdiene-4,8-diyn-1-yl)oxy>trimethylsilane
Conditions | Yield |
---|---|
With TEA In dichloromethane for 5h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
bis(p-dimethylaminophenyl)methanone
methylen>(trimethylsilyl)oxonium-trifluormethansulfonat
Conditions | Yield |
---|---|
In dichloromethane at 15℃; | 100% |
trimethylsilyl trifluoromethanesulfonate
(E)-2-(4-oxopent-2-en-1-yl)isoindoline-1,3-dione
2-((E)-4-Trimethylsilanyloxy-penta-2,4-dienyl)-isoindole-1,3-dione
Conditions | Yield |
---|---|
With triethylamine In benzene for 15h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 25℃; for 1h; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-methylcyclohexan-4-one
4-methyl-1-(trimethylsilyloxy)-1-cyclohexene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 1.5h; | 100% |
With triethylamine In dichloromethane for 1h; |
trimethylsilyl trifluoromethanesulfonate
(1S,2S,3R,4aS,13bR,14aS)-3-(tert-Butyl-dimethyl-silanyloxy)-1-hydroxy-2,11-dimethoxy-5-oxo-1,2,3,4,4a,5,7,8,13,13b,14,14a-dodecahydro-indolo[2',3':3,4]pyrido[1,2-b]isoquinoline-1-carboxylic acid methyl ester
(1S,2S,3R,4aS,13bR,14aS)-3-(tert-Butyl-dimethyl-silanyloxy)-2,11-dimethoxy-5-oxo-1-trimethylsilanyloxy-1,2,3,4,4a,5,7,8,13,13b,14,14a-dodecahydro-indolo[2',3':3,4]pyrido[1,2-b]isoquinoline-1-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane for 4h; Ambient temperature; | 100% |
trimethylsilyl trifluoromethanesulfonate
methyl (phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate
methyl (phenyl 2,3-di-O-benzyl-1-thio-4-O-trimethylsilyl-β-D-galactopyranosid)uronate
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at -10℃; for 0.0833333h; | 100% |
trimethylsilyl trifluoromethanesulfonate
benzyl (phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate
benzyl (phenyl 2,3-di-O-benzyl-1-thio-4-O-trimethylsilyl-β-D-galactopyranosid)uronate
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at -10℃; for 0.166667h; | 100% |
trimethylsilyl trifluoromethanesulfonate
Ethyl 2-methyl-3,3,3-trifluoropropionate
Conditions | Yield |
---|---|
With triethylamine at 100℃; for 5h; Substitution; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-ethoxycarbonyl-2-trimethylsilylaziridine
Conditions | Yield |
---|---|
Ring cleavage; Substitution; | 100% |
trimethylsilyl trifluoromethanesulfonate
2-Methoxycarbonyl-2-dimethylphenylsilyl-1-phenylaziridine
Conditions | Yield |
---|---|
Salt formation; | 100% |
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In tetrahydrofuran at -78 - 0℃; | 100% |
trimethylsilyl trifluoromethanesulfonate
2-(diphenylphosphinyl)-2'-(diphenylphosphanyl)-1,1'-binaphthalene
Conditions | Yield |
---|---|
at 20℃; | 100% |
trimethylsilyl trifluoromethanesulfonate
methoxybenzene
1,1-diphenyl-3-(trimethylsilyl)-1-(trimethylsilyloxy)prop-2-yne
Conditions | Yield |
---|---|
In dichloromethane at -78℃; for 3h; Friedel-Crafts reaction; | 100% |
trimethylsilyl trifluoromethanesulfonate
1-fluoro-1-isopropyl-1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ5-phospha-indan
Conditions | Yield |
---|---|
In diethyl ether at 20℃; | 100% |
In diethyl ether at 20℃; for 0.333333h; |
trimethylsilyl trifluoromethanesulfonate
1-ethylsulfanyl-1-fluoro-3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ5-phospha-indan
Conditions | Yield |
---|---|
In diethyl ether at 20℃; | 100% |
trimethylsilyl trifluoromethanesulfonate
8a-allyl-4-(tert-butyl-diphenyl-silanyloxy)-2-(toluene-4-sulfonyl)-3,4,4a,8a-tetrahydro-2H,5H-isoquinoline-1,6-dione
8a-allyl-4-(tert-butyl-diphenyl-silanyloxy)-2-(toluene-4-sulfonyl)-6-trimethylsilanyloxy-3,4,4a,8a-tetrahydro-2H-isoquinolin-1-one
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; | 100% |
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With tetrachlorosilane In dichloromethane; chloroform | 100% |
trimethylsilyl trifluoromethanesulfonate
1-(2,2-dimethoxyethyl)-4-phenylcyclohexanol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 0.5h; | 100% |
Stage #1: trimethylsilyl trifluoromethanesulfonate; 1-(2,2-dimethoxyethyl)-4-phenylcyclohexanol With 2,6-dimethylpyridine In dichloromethane at 0℃; for 0.5h; Stage #2: With water In dichloromethane | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at -78℃; for 1h; | 100% |
trimethylsilyl trifluoromethanesulfonate
(3S,4S)-4-Acetyl-3-methoxy-1-(4-methoxy-phenyl)-azetidin-2-one
(3S,4S)-3-Methoxy-1-(4-methoxy-phenyl)-4-(1-trimethylsilanyloxy-vinyl)-azetidin-2-one
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -78 - 20℃; for 2h; | 100% |
trimethylsilyl trifluoromethanesulfonate
(-)-(1Z,2S,3R,4S)-1-ethylidene-2,4-dimethyl-5-oxo-3-((1S)-1-phenylethoxy)-heptyl isobutyrate
Isobutyric acid (Z)-(2S,3R,4S)-1-eth-(Z)-ylidene-2,4-dimethyl-3-((S)-1-phenyl-ethoxy)-5-trimethylsilanyloxy-hept-5-enyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
With triethylamine In dichloromethane at -20 - 20℃; for 2h; |
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