DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:421-83-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:421-83-0
Min.Order:1 Metric Ton
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Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:421-83-0
Min.Order:1
Negotiable
Type:Other
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:421-83-0
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $8.0 / 20.0
Type:Trading Company
inquiryProduct Name: TRIFLUOROMETHANESULFONYL CHLORIDE Synonyms: TRIFLUOROMETHANESULFONYL CHLORIDE;TRIFLUOROMETHANESULPHONYL CHLORIDE; TRIFLUOROMETHANESULFONYL CHLORIDE, 99+%;TRIFLYL CHLORIDE;P
Cas:421-83-0
Min.Order:1 Kilogram
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryTRIFLUOROMETHANESULFONYL CHLORIDE CAS:421-83-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
Cas:421-83-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $400.0 / 500.0
Type:Lab/Research institutions
inquiry1. Well-equipped, stable and high-quality raw material supply chain, to provide customers with the best quality products. 2.Strict quality inspection process and professional certificate testing to ensure the quality level of the final product. 3.E
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:421-83-0
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:421-83-0
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:421-83-0
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHot sale 421-83-0 low price Trifluoromethanesulfonyl chloride manufacturer 1) Preparation of trifluoromethyl sulfonyl fluoride from trifluoromethyl sulfonyl chloride. Trifluoromethyl sulfonyl fluoride is an important organic intermediate, which can
Cas:421-83-0
Min.Order:1 Gram
Negotiable
Type:Other
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:421-83-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als
Cas:421-83-0
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:421-83-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used for Pesticide intermediat
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:421-83-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
TRIFLUOROMETHANESULFONYL CHLORIDE Chemical Properties Melting point -26 °C Boiling point 29-32 °C (lit.) density 1.583 g/mL at 25 °C (lit.) vapor pressure 10.36 psi ( 20 °C) refractive index n20/D 1.334(lit.) Fp
Cas:421-83-0
Min.Order:1 Gram
FOB Price: $65.0
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct name: Trifluoromethanesulfonyl Chloride CAS No.:421-83-0 Molecule Formula:CClF3O2S Molecule Weight:168.52 Purity: 98.0% Package: 200kg/drum Description:Light yellow liquid Manufacture Standards:Enterprise Standard
Cas:421-83-0
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:421-83-0
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:421-83-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryTrifluoromethylsulfenyl chloride
water
chlorine
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
excess of Cl2 and H2O, 20°C, 7 days; | 98% |
excess of Cl2 and H2O, 20°C, 7 days; | 98% |
Conditions | Yield |
---|---|
260°C, 2 h; | 94% |
260°C, 2 h; | 94% |
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide at 40℃; for 12h; Cooling with ice; Green chemistry; | 87.5% |
With phosphorus pentachloride at 100℃; | 85% |
With phosphorus pentachloride |
methanol
trans-chlorotetrafluoro(trifluoromethyl)sulfur(VI)
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
in presence of (CH3)4N, 25°C, 10 h; | 75% |
in presence of (CH3)4N, 25°C, 10 h; | 75% |
chlorine
pentafluoroethanesulfinic acid
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
In acetic acid chlorination; | 74.6% |
In acetic acid chlorination; | 74.6% |
Conditions | Yield |
---|---|
With chlorine In water at 5℃; under 3040 Torr; for 2h; | 70% |
(Dichloroiodo)benzene
pentafluoroethanesulfinic acid
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
chlorination; | 65.7% |
chlorination; | 65.7% |
trifluorormethanesulfonic acid
phosphorus pentachloride
A
trifluoromethane sulfonyl chloride
B
trichlorophosphate
Conditions | Yield |
---|---|
A 63% B n/a | |
A 63% B n/a |
zinc trifluoromethanesulfonate
zinc(II) chloride
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
anhydr. ZnCl2, heating, Fischer burner, 4 h; fractional distn.; | 43% |
anhydr. ZnCl2, heating, Fischer burner, 4 h; fractional distn.; | 43% |
Trifluoromethylsulfenyl chloride
dihydrogen peroxide
A
Bis(trifluoromethyl)disulfid
B
trifluorormethanesulfonic acid
C
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
35% H2O2 soln.; | A 35% B 7% C 40% |
35% H2O2 soln.; | A 35% B 7% C 40% |
trans-chlorotetrafluoro(trifluoromethyl)sulfur(VI)
sodium methylate
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
25°C, 10 h; | 30% |
25°C, 10 h; | 30% |
Conditions | Yield |
---|---|
With water; chlorine |
trifluoromethylsulfinyl chloride
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With water |
trifluoromethanesulfinyl fluoride
A
Trifluoromethylsulfenyl chloride
B
trifluoromethane sulfonyl chloride
C
trifluoromethylsulfinyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride at -183℃; |
zinc trifluoromethanesulfonate
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With PCl5*2ZnCl2 at 260℃; |
Conditions | Yield |
---|---|
With sulfur tetrafluoride; hydrogen fluoride; water; chlorine 1.) 80 deg C, 16 h, 2.) 20 deg C, 24 h, 40-50 deg C, 24 h; Yield given. Multistep reaction; |
trifluoromethylsulfonic anhydride
A
trifluoromethane sulfonyl chloride
B
seleninyl bis(trifluorometanesulfonate)
Conditions | Yield |
---|---|
With selenium oxychloride at 60℃; |
Conditions | Yield |
---|---|
With chlorine In water at 0 - 10℃; under 2250.2 Torr; for 2h; Yield given; |
trifluoromethanesulfonate
A
phosgene
B
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
distn.; |
trifluoromethylsulfonic anhydride
sodium chloride
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
In further solvent(s) solvent: tetramethylenesulfone, 3 h; |
Conditions | Yield |
---|---|
260°C, 2 h; | 80-85 |
260°C, 2 h; | 80-85 |
Trifluoromethanesulfonyl fluoride
chlorine
hydrazine
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
In further solvent(s) redn. of 95% N2H4 in CFCl2CF2Cl at 0-10°C, after addn. of Cl2; |
trifluoromethylsulfinyl chloride
water
A
Trifluoromethylsulfenyl chloride
B
trifluoromethane sulfonyl chloride
trifluoromethyl hypochlorite
trifluoromethylsulfinyl chloride
A
thionyl chlorofluoride
B
carbon tetrafluoride
C
Carbonyl fluoride
D
chlorotrifluoromethane
E
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
25°C, 2 h; further products; | |
25°C, 2 h; further products; |
trans-chlorotetrafluoro(trifluoromethyl)sulfur(VI)
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With NaOCH3 25°C, 10 h; | |
With CH3OH in presence of (CH3)3N, 25°C, 10 h; |
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With water; chlorine at 10 - 30℃; under 73.5572 - 735.572 Torr; |
Conditions | Yield |
---|---|
With rhodium(III) chloride; sulfuryl dichloride; sulfuric acid; dihydrogen peroxide; urea at 65℃; for 12h; |
Conditions | Yield |
---|---|
With copper at 200℃; for 24h; | 100% |
With pyridine; copper dichloride In 1,4-dioxane at 100℃; for 1h; Inert atmosphere; Schlenk technique; | 8 %Spectr. |
3',5'-bis-O-(tert-butyldimethylsilyl)-β-D-adenosine
trifluoromethane sulfonyl chloride
9-[3,5-bis-O-[(1,1-dimethylethyl)dimethylsilyl]-2-trifluoromethylsulfonyloxy-β-D-arabinofuranosyl]-9H-purin-6-amine
Conditions | Yield |
---|---|
With dmap; triethylamine In pyridine at 0 - 20℃; for 3h; Esterification; | 100% |
trifluoromethane sulfonyl chloride
9-[3-O-benzoyl-5-O-(triphenylmethyl)-β-D-ribofuranosyl]-6-chloro-9H-purine
5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside
Conditions | Yield |
---|---|
With dmap In toluene | 100% |
With dmap In toluene |
(2-hydroxy-6-methoxy-naphthalen-1-yl)-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone
trifluoromethane sulfonyl chloride
trifluoro-methanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 0.25h; | 100% |
With pyridine In dichloromethane at 0℃; for 0.25h; | 100% |
Stage #1: (2-hydroxy-6-methoxy-naphthalen-1-yl)-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone; trifluoromethane sulfonyl chloride With pyridine In dichloromethane for 0.5h; Stage #2: With water In dichloromethane | 100% |
7-hydroxy-8-nitro-1,2,4,5-tetrahydrobenzo[d]azepine-3-carboxylic acid tert-butyl ester
trifluoromethane sulfonyl chloride
7-nitro-8-trifluoromethanesulfonyloxy-1,2,4,5-tetrahydrobenzo[d]azepine-3-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In acetone at 20℃; for 1h; | 100% |
With triethylamine In acetone at 0℃; for 0.5h; | 87% |
In acetone at 0 - 20℃; for 2h; Product distribution / selectivity; |
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 4 - 15℃; for 17.25h; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 4 - 15℃; for 17.25h; | 100% |
trans-[4-(4-hydroxyphenyl)cyclohexyl]acetic methyl ester
trifluoromethane sulfonyl chloride
(trans)-methyl 2-(4-(4-(((trifluoromethyl)sulfonyl)oxy)phenyl)cyclohexyl)acetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 4 - 15℃; for 17.25h; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 4 - 15℃; for 17.25h; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; |
9-(3,5-O-isopropylidene-β-L-xylofuranosyl)adenine
trifluoromethane sulfonyl chloride
9-(3,5-O-isopropylidene-2-O-triflyl-β-L-xylofuranosyl)adenine
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
trifluoromethane sulfonyl chloride
trifluoro-methanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester
Conditions | Yield |
---|---|
Stage #1: (2-hydroxy-6-methoxy-naphthalen-1-yl)-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone With pyridine In dichloromethane at 0℃; Stage #2: trifluoromethane sulfonyl chloride In dichloromethane for 0.5h; Stage #3: With water In dichloromethane | 100% |
9-[2'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-xylofuranosyl]adenine
trifluoromethane sulfonyl chloride
9-[2'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-trifluoromethanesulfonyl-xylofuranosyl]adenine
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0℃; for 1h; | 100% |
trifluoromethane sulfonyl chloride
triethylamine
acetylacetone
3,3-dichloropentane-2,4-dione
Conditions | Yield |
---|---|
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
triethylamine
malonic acid dimethyl ester
dimethyl 2,2-dichloromalonate
Conditions | Yield |
---|---|
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
ethyl acetoacetate
triethylamine
ethyl 2,2-dichloroacetoacetate
Conditions | Yield |
---|---|
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
triethylamine
methyl 2-cyanoacetate
methyl dichlorocyanoacetate
Conditions | Yield |
---|---|
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
acetylacetone
3,3-dichloropentane-2,4-dione
Conditions | Yield |
---|---|
With 1,5-Diazabicyclo[5.4.0]undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
With 1,5-diazabicyclo(5.4.0)undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
phosphonic acid diethyl ester
diethyl chlorophosphate
Conditions | Yield |
---|---|
With 1,5-Diazabicyclo[5.4.0]undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
With 1,5-diazabicyclo(5.4.0)undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
malonic acid dimethyl ester
dimethyl 2,2-dichloromalonate
Conditions | Yield |
---|---|
With 1,5-Diazabicyclo[5.4.0]undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
With 1,5-diazabicyclo(5.4.0)undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
ethyl acetoacetate
ethyl 2,2-dichloroacetoacetate
Conditions | Yield |
---|---|
With 1,5-Diazabicyclo[5.4.0]undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
With 1,5-diazabicyclo(5.4.0)undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
methyl 2-cyanoacetate
methyl dichlorocyanoacetate
Conditions | Yield |
---|---|
With 1,5-Diazabicyclo[5.4.0]undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
With 1,5-diazabicyclo(5.4.0)undec-5-ene In dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h; | 100% |
trifluoromethane sulfonyl chloride
diethyl malonate
A
diethyl dichloromalonate
B
trifluoromethanesulfinic acid
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 10 - 50℃; Mechanism; Reagent/catalyst; Solvent; | A 100% B n/a |
trifluoromethane sulfonyl chloride
1,2-diamino-benzene
p-toluenesulfonyl chloride
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride In dichloromethane at -78℃; | 100% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 0.25h; Inert atmosphere; | 99% |
With triethylamine | 91% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 6h; Inert atmosphere; | 82% |
trifluoromethane sulfonyl chloride
hydroxy(phenyl)-λ3-iodanyl diphenylphosphinate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.25h; | 99% |
trifluoromethane sulfonyl chloride
N-tosyl-(4-pentenyl)amine
N-(4-chloro-6,6,6-trifluorohexyl)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; tris(1,10-phenanthroline)ruthenium(II) dichloride In acetonitrile at 25℃; for 15h; Reagent/catalyst; Solvent; Inert atmosphere; Irradiation; regioselective reaction; | 99% |
With dipotassium hydrogenphosphate; tris(1,10-phenanthroline)ruthenium(II) dichloride In acetonitrile at 25℃; for 15h; Catalytic behavior; Reagent/catalyst; Solvent; Photolysis; Inert atmosphere; regioselective reaction; | 32 mg |
trifluoromethane sulfonyl chloride
N-(but-3-en-1-yl)-4-chlorobenzamide
4-chloro-N-(3-chloro-5,5,5-trifluoropentyl)benzamide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; tris(1,10-phenanthroline)ruthenium(II) dichloride In acetonitrile at 25℃; for 15h; Inert atmosphere; Irradiation; Sealed tube; regioselective reaction; | 99% |
6-chloroindole
trifluoromethane sulfonyl chloride
Conditions | Yield |
---|---|
With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane In 1,4-dioxane at 40℃; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
With triphenylphosphine; sodium iodide In acetonitrile at 60℃; for 4h; Schlenk technique; Inert atmosphere; | 91% |
With phosphonic acid diethyl ester In acetonitrile at 90℃; for 10h; | 80% |
trifluoromethane sulfonyl chloride
5-methoxycarbonylindole
3-trifluoromethylsulfanyl-5,1H-indolecarboxylc acid methyl ester
Conditions | Yield |
---|---|
With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane In 1,4-dioxane at 40℃; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
With triphenylphosphine; sodium iodide In acetonitrile at 60℃; for 22h; Schlenk technique; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With [5,10,15,20-tetraphenylporphyrin]cobalt(III) chloride; Langlois reagent In acetonitrile at 100℃; for 12h; Inert atmosphere; Sealed tube; | 99% |
trifluoromethane sulfonyl chloride
bis(trifluoromethane)sulfonimide lithium
Conditions | Yield |
---|---|
With lithium carbonate In acetonitrile Reagent/catalyst; | 98.8% |
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