CAS No.372-64-5,BIS(TRIFLUOROMETHYL)DISULFIDE Suppliers

Shanghai Upbio Tech Co.,Ltd

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Disulfide,bis(trifluoromethyl)

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Disulfide,bis(trifluoromethyl)

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:gas Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used for Pesticide intermediat

Disulfide,bis(trifluoromethyl)

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

BIS(TRIFLUOROMETHYL)DISULFIDE

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Disulfide,bis(trifluoromethyl)

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

BIS(TRIFLUOROMETHYL)DISULFIDE

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Hunan chemfish Pharmaceutical co.,Ltd

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Bis(trifluoromethyl) disulfide

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Henan Allgreen Chemical Co.,Ltd

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3-Chloro-4-(N-pyrrolidin-1-ylcarbonyl)benzeneboronic acid 97%

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

BIS(TRIFLUOROMETHYL)DISULFIDE

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

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Hangzhou Fandachem Co.,Ltd

BIS(TRIFLUOROMETHYL)DISULFIDEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

BIS(TRIFLUOROMETHYL)DISULFIDE

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Henan Kanbei Chemical Co.,LTD

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BIS(TRIFLUOROMETHYL)DISULFIDE

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Hunan Russell Chemicals Technology Co.,Ltd

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Bis(trifluoromethyl) disulfide 372-64-5

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Shenzhen Foris Technology Co. LTD

Bis(trifluoromethyl) disulfide 372-64-5

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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BIS(TRIFLUOROMETHYL)DISULFIDE

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Pure Chemistry Scientific Inc.

Bis(trifluoromethyl) disulfide Application:2025690

Bis(trifluoromethyl) disulfide

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Shanghai Petrochemical Co.,Ltd

*stable huge quantity supply*best service*powerful r&d team*gmp standard factory*we have the separate r&d dept.,the advanced equipments and the experienced engineers,we have established the excellent cooperative relations with many famous universitie

BIS(TRIFLUOROMETHYL)DISULFIDE

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Sparrow Chemical Co.,Ltd

Our company provides the best service for our customers. Under the premise of ensuring quality and delivery date, give customers the best price. The company is more willing to meet our customers. If you want to visit our factories and warehouses, we

BIS(TRIFLUOROMETHYL)DISULFIDE

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NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

trifluoro-(trifluoromethyldisulfanyl)methane

Cas:372-64-5

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Crescent Chemical Co., Inc.

Disulfide,bis(trifluoromethyl)

Cas:372-64-5

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Synthetic route

: 21259-75-6
mercury bis(trifluoromethanethiolate)

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: trifluoromethylthio-mercury(II) chloride

C: 83665-28-5
bis(trifluoromethylthio)tellurium

Conditions

Conditions	Yield
With tellurium tetrachloride for 1h; Heating;	A n/a B n/a C 83%

...Expand

: 2314-97-8
iodotrifluoromethane

: 7704-34-9
sulfur

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
390-420°C, atm. pessure in a continuous flow system;	80.6%
390-420°C, atm. pessure in a continuous flow system;	80.6%
>200°C, in autoclave;
>200°C, in autoclave;

: 79378-29-3
O,O-diethyl S-trifluoromethyl phosphorothioate

A: 420-32-6
thiocarbonyl fluoride

B: 358-74-7
diethyl fluorophosphate

C: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 10℃; for 0.166667h;	A n/a B 76% C n/a

...Expand

: 21259-75-6
mercury bis(trifluoromethanethiolate)

: 13360-57-1
dimethylamino sulfonyl chloride

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: N,N-Dimethyl-S-(trifluormethyl)thiosulfamidsaeure

Conditions

Conditions	Yield
In acetonitrile	A n/a B 76%

...Expand

: 7664-39-3
hydrogen fluoride

: 594-42-3
chlorothio-trichloro-methane

A: 421-17-0
Trifluoromethylsulfenyl chloride

B: 372-64-5
Bis(trifluoromethyl)disulfid

C: 358-15-6
Trifluoro-methanethiosulfonic acid S-trifluoromethyl ester

Conditions

Conditions	Yield
180°C; chrom oxide fluoride catalyst;	A 74% B n/a C n/a

...Expand

: 676-71-1
dimethyl(bromo)arsine

: 3872-23-9
Copper(I) trifluoromethanethiolate

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 372-06-5
bis(trifluoromethyl)trisulfide

C: 372-07-6
bis(trifluoromethyl)tetrasulfide

D: 1959-80-4
dimethyl(trifluoromethylthio)arsine

Conditions

Conditions	Yield
at 80 - 90℃; for 6h; Further byproducts given;	A n/a B n/a C n/a D 70%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 108-88-3
toluene

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 351-60-0
benzyl trifluoromethyl sulfide

C: 100-44-7
benzyl chloride

Conditions

Conditions	Yield
byproducts: HCl; Irradiation (UV/VIS);	A n/a B 70% C 3%
byproducts: HCl; Irradiation (UV/VIS);	A n/a B 70% C 3%
for 0.283333h; Mechanism; Irradiation; effect of bis(heptafluoro-n-propyl) disulfide;

...Expand

: potassium fluoride

: 594-42-3
chlorothio-trichloro-methane

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With hydrogen bromide In further solvent(s) 160-175°C; solvent: tetramethylenesulfone;	68%
With HBr In further solvent(s) 160-175°C; solvent: tetramethylenesulfone;	68%

: potassium fluoride

: 15110-08-4
Bis(trichloromethyl)disulfane

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
In further solvent(s) 150-160°C; solvent: tetramethylenesulfone;	58%
In further solvent(s) 150-160°C; solvent: tetramethylenesulfone;	58%

: 3042-22-6
2-phenyl-1H-pyrrole

: 1443036-49-4
1-phenyl-2-(phenyl-λ3-iodaneylidene)-2-((trifluoromethyl)sulfonyl)ethan-1-one

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 2-phenyl-5-((trifluoromethyl)thio)-1H-pyrrole

Conditions

Conditions	Yield
Stage #1: 1-phenyl-2-(phenyl-λ3-iodaneylidene)-2-((trifluoromethyl)sulfonyl)ethan-1-one With copper (II)-fluoride In 1-methyl-pyrrolidin-2-one at 20℃; for 0.333333h; Stage #2: 2-phenyl-1H-pyrrole at 20℃; for 5h; regioselective reaction;	A 28% B 58%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 127-09-3
sodium acetate

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 358-15-6
Trifluoro-methanethiosulfonic acid S-trifluoromethyl ester

C: 42530-92-7
trifluoromethyl-sulfenyl acetate

D: 108-24-7
acetic anhydride

Conditions

Conditions	Yield
at 0℃; for 12h;	A n/a B n/a C 52% D n/a

...Expand

: 4317-00-4
tris(trifluoromethylmercapto)amine

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 80653-51-6
tetrakis (trifluormethylmarcapto)-hydrazine

Conditions

Conditions	Yield
In trichlorofluoromethane at -73.1℃; for 6h; Irradiation;	A n/a B 50%
In trichlorofluoromethane at -73.1℃; for 6h; Product distribution; Irradiation; other temperature 298 deg K;	A n/a B 10 % Turnov.

: 593-89-5
methyldichloroarsane

: 21259-75-6
mercury bis(trifluoromethanethiolate)

A: 420-24-6
methyldifluoroarsine

B: 372-64-5
Bis(trifluoromethyl)disulfid

C: 461-08-5
bis(trifluoromethyl)trithiocarbonate

D: bis(trifluoromethylthio)methylarsine

Conditions

Conditions	Yield
at 95 - 100℃; for 4h;	A n/a B n/a C n/a D 48%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 75-28-5
Isobutane

A: CF3SCH2C(CH3)3

B: 507-20-0
tertiary butyl chloride

C: 2708-84-1
2-methyl-2-[(trifluoromethyl)thio]propane

D: 372-64-5
Bis(trifluoromethyl)disulfid

E: 513-36-0
isobutyryl chloride

Conditions

Conditions	Yield
byproducts: HCl; Irradiation (UV/VIS);	A 12% B 33% C 24% D 47% E 1%
byproducts: HCl; Irradiation (UV/VIS);	A 12% B 33% C 24% D 47% E 1%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 106-97-8
n-butane

A: 78-86-4, 53178-20-4
s-butyl chloride

B: 109-69-3
n-Butyl chloride

C: 372-64-5
Bis(trifluoromethyl)disulfid

D: 6214-34-2
Trifluormethyl-sek.-butyl-sulfid

E: 7412-26-2
1-[(trifluoromethyl)thio]butane

Conditions

Conditions	Yield
byproducts: HCl; Irradiation (UV/VIS);	A 12% B 1% C 28% D 46% E 13%
byproducts: HCl; Irradiation (UV/VIS);	A 12% B 1% C 28% D 46% E 13%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 110-82-7
cyclohexane

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 6476-52-4
cyclohexyl(trifluoromethyl)sulfane

C: 542-18-7
cyclohexyl chloride

Conditions

Conditions	Yield
byproducts: HCl; Irradiation (UV/VIS);	A 35% B 45% C 28%
byproducts: HCl; Irradiation (UV/VIS);	A 35% B 45% C 28%
for 0.2h; Mechanism; Irradiation; effect of bis(heptafluoro-n-propyl) disulfide;

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

: 7722-84-1
dihydrogen peroxide

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 1493-13-6
trifluorormethanesulfonic acid

C: 421-83-0
trifluoromethane sulfonyl chloride

Conditions

Conditions	Yield
35% H2O2 soln.;	A 35% B 7% C 40%
35% H2O2 soln.;	A 35% B 7% C 40%

...Expand

: 421-17-0
Trifluoromethylsulfenyl chloride

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 99028-27-0
tetrakis(trifluoromethylthiazyl)

Conditions

Conditions	Yield
With trimethylsilylazide In trichlorofluoromethane at -30℃; for 24h;	A n/a B 37%

: 110-00-9
furan

: 421-17-0
Trifluoromethylsulfenyl chloride

A: 58679-57-5
2-Trifluormethylmercapto-furan

B: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With pyridine at 20℃; for 12h; other sulfenyl chloride;	A 35% B n/a
With pyridine at 20℃; for 12h;	A 35% B n/a

...Expand

: 13955-08-3
F2S2O6

: 1493-15-8
trifluoromethylsulfide

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
-183 to 25°C;	30%
-183 to 25°C;	30%

: 13709-32-5
bis(fluorosulfuryl) peroxide

: 1493-15-8
trifluoromethylsulfide

A: 13036-75-4
fluorosulfonyl anhydride

B: 372-64-5
Bis(trifluoromethyl)disulfid

C: 7446-09-5
sulfur dioxide

D: 7704-34-9
sulfur

Conditions

Conditions	Yield
CF3SH:S2O6F2 molar ratio 1:1, from -183 to +25°C;	A n/a B 30% C n/a D n/a

...Expand

: 598-14-1
ethylarsenic dichloride

: 3872-23-9
Copper(I) trifluoromethanethiolate

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 371-73-3
trifluoromethylmercaptothiocarbonyl fluoride

C: 372-06-5
bis(trifluoromethyl)trisulfide

D: ethyl bis(trifluoromethylthio)arsine

Conditions

Conditions	Yield
at 85 - 95℃; for 6h; Further byproducts given;	A n/a B n/a C n/a D 25%

...Expand

: CF2HC(O)OSCF3

A: 371-72-2
difluoromethyl-trifluoromethyl sulfide

B: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
Irradiation (UV/VIS); in Pyrex bulb;	A n/a B 25%
Irradiation (UV/VIS); in Pyrex bulb;	A n/a B 25%

: 993-35-1
trichloromethanesulfenyl bromide

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With sulfolane; potassium fluoride at 175℃; Inert atmosphere;	15%

: 421-17-0
Trifluoromethylsulfenyl chloride

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 114541-92-3
hexachloro-3-cyclopentenylidenaminotrifluormethylsulfide

Conditions

Conditions	Yield
With trimethylsilylazide; hexachlorocyclopentadiene In toluene at 110℃; under 0.01 Torr; for 3h;	A n/a B 6.2%

: 421-17-0
Trifluoromethylsulfenyl chloride

: 4648-54-8
trimethylsilylazide

: 77-47-4
hexachlorocyclopentadiene

A: 372-64-5
Bis(trifluoromethyl)disulfid

B: 114541-92-3
hexachloro-3-cyclopentenylidenaminotrifluormethylsulfide

Conditions

Conditions	Yield
In toluene at 110℃; under 0.01 Torr; for 3h;	A n/a B 6.2%

...Expand

: 75-15-0
carbon disulfide

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With iodine pentafluoride at 195℃;
With mercury(II) fluoride at 500℃;

: 2314-97-8
iodotrifluoromethane

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With sulfur at 310℃;

: 1717-50-6
tetrafluoro-1,3-dithiaetane

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
With sulfur tetrafluoride at 250℃;

: 421-17-0
Trifluoromethylsulfenyl chloride

: 372-64-5
Bis(trifluoromethyl)disulfid

Conditions

Conditions	Yield
iron pentacarbonyl In tetrahydrofuran at -80℃;
With perfluoropropylene for 72h; Irradiation;
With trifluoro-methoxy-ethene for 0.166667h; Irradiation; Further byproducts given;

: 187737-37-7
propene

: 372-64-5
Bis(trifluoromethyl)disulfid

: 34994-61-1
1,2-Bis-trifluoromethylsulfanyl-propane

Conditions

Conditions	Yield
Irradiation (UV/VIS); 20 h;	100%
Irradiation (UV/VIS); 20 h;	100%
Irradiation;

: 74-85-1
ethene

: 372-64-5
Bis(trifluoromethyl)disulfid

: 674-64-6
1,2-Bis-trifluormethyl-mercapto-ethan

Conditions

Conditions	Yield
Irradiation (UV/VIS); 44 h;	100%
Irradiation (UV/VIS); 44 h;	100%
Irradiation;

: 996-70-3
Tetrakis(dimethylamino)ethylen

: 372-64-5
Bis(trifluoromethyl)disulfid

: tetrakis(dimethylamino)ethanebis(ylium) bis(trifluoro-methanethiolate)

Conditions

Conditions	Yield
In 1,2-dimethoxyethane at -20℃; for 0.166667h; Reduction;	98.3%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 66954-57-2
benzyl tetraethylphosphorodiamidite

A: 351-60-0
benzyl trifluoromethyl sulfide

B: bis(diethylamido)-S-trifluoromethylphosphorothioate

Conditions

Conditions	Yield
In pentane at -50℃; for 0.0833333h;	A 95% B n/a

...Expand

: 7790-91-2
chlorine trifluoride

: 372-64-5
Bis(trifluoromethyl)disulfid

: 374-10-7
trifluoro(trifluoromethyl)sulfur(IV)

Conditions

Conditions	Yield
In dichloromethane -78°C;	95%
In dichloromethane -78°C;	95%
In Dichlorodifluoromethane excess ClF3, -196 to -78°C;
In Dichlorodifluoromethane excess ClF3, -196 to -78°C;

: 116-15-4
perfluoropropylene

: 372-64-5
Bis(trifluoromethyl)disulfid

A: 646-86-6
2,5-bis(trifluoromethylmercapto)-4-trifluoromethyl-nonafluoropentane

B: 679-31-2
1,2-bis(trifluoromethylsulfanyl)hexafluoropropane

Conditions

Conditions	Yield
Irradiation (UV/VIS); 184 h;	A 90.5% B 9.5%
Irradiation (UV/VIS); 184 h;	A 90.5% B 9.5%

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: C12H27N2O3P

A: 65540-51-4
Ethyl <(trifluoromethyl)thio>acetate

B: bis(diethylamido)-S-trifluoromethylphosphorothioate

Conditions

Conditions	Yield
In pentane at -50℃; for 0.0833333h;	A 90% B n/a

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: C13H29N2O3P

A: 84132-15-0
Ethyl 2-<(trifluoromethyl)thio>propanoate

B: bis(diethylamido)-S-trifluoromethylphosphorothioate

Conditions

Conditions	Yield
In pentane at -50℃; for 0.0833333h;	A 90% B n/a

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: 393-02-2
Tetrakis(trifluoromethyl)cyclotetraphosphane

A: 1898-62-0
Trifluormethyl-(bis-methylmercapto)-phosphin

B: 745-23-3, 54548-49-1
pentakis-trifluoromethyl-cyclopentaphosphane

Conditions

Conditions	Yield
143°C, 1 h;	A 90% B n/a
143°C, 1 h;	A 90% B n/a
20°C, 12 h;
20°C, 12 h;

...Expand

: 14221-01-3
tetrakis(triphenylphosphine) palladium(0)

: 372-64-5
Bis(trifluoromethyl)disulfid

: 50298-23-2, 50298-22-1
Pd(SCF3)2{P(C6H5)3}2

: 50298-23-2, 50298-22-1
Pd(SCF3)2{P(C6H5)3}2

Conditions

Conditions	Yield
In pentane Irradiation (UV/VIS); with low-pressure mercury lamp, 25°C, 30 min;	A 10% B 90%
In pentane Irradiation (UV/VIS); with low-pressure mercury lamp, 25°C, 30 min;	A 10% B 90%

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: 7782-41-4
fluorine

: 374-10-7
trifluoro(trifluoromethyl)sulfur(IV)

Conditions

Conditions	Yield
fluorination with F2/He (flow rate 1 mL/min F2 and 60 mL min He) in continuous flow reactor at -120°C (38 h);	90%
fluorination with F2/He (flow rate 1 mL/min F2 and 60 mL min He) in continuous flow reactor at -120°C (38 h);	90%
with N2 dild. F2 used;
with N2 dild. F2 used;

: {C6H5NiCO}2

: 372-64-5
Bis(trifluoromethyl)disulfid

: (C6H5NiSCF3)2

Conditions

Conditions	Yield
In pentane Irradiation (UV/VIS); medium-pressure mercury lamp, 25 h;	90%
In pentane Irradiation (UV/VIS); medium-pressure mercury lamp, 25 h;	90%

: 10170-69-1
dimanganese decacarbonyl

: 372-64-5
Bis(trifluoromethyl)disulfid

A: 21239-57-6
Mn2(CO)8(SCF3)2

B: 50979-57-2
CF3SMn(CO)5

Conditions

Conditions	Yield
In pentane Irradiation (UV/VIS); medium-pressure mercury lamp, -10°C, 24 h;	A 90% B n/a
In pentane Irradiation (UV/VIS); medium-pressure mercury lamp, -10°C, 24 h;	A 90% B n/a

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: 371-78-8
bis-(trifluoromethyl)sulfide

Conditions

Conditions	Yield
heating at 425-435°C, 3-4 d;	88%
Irradiation (UV/VIS); in quartztube, 13 d;	39%
Irradiation (UV/VIS); in quartztube, 13 d;	39%
Irradiation.UV-Licht;

: 372-64-5
Bis(trifluoromethyl)disulfid

: 82945-11-7, 6057-79-0, 57956-51-1
(Rp)-t-butyl(phenyl)phosphine oxide

: 128175-77-9
(-)-S-t-butyl(phenyl)-S-trifluoromethyl phosphinothioate

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 6h;	88%

: 12176-06-6
hydrido(tricarbonyl)(cyclopentadienyl)molybdenum

: 372-64-5
Bis(trifluoromethyl)disulfid

: [(η(5)-C5H5)Mo(CO)3SCF3]

Conditions

Conditions	Yield
In benzene byproducts: HSCF3; (N2 or in vacuum with Schlenk-technique); react. at 25°C for 2 d; chromy. on SiO2-column with benzene/cyclohexane;	87.3%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 98976-30-8, 57956-51-1, 6057-79-0, 82945-11-7
tert-Butylphenylphosphine oxide

: t-butyl(phenyl) S-trifluoromethyl phosphinothioate

Conditions

Conditions	Yield
In dichloromethane -85 to -80 deg C, 30 min, then 15-20 deg C, 5 h;	85%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 38432-39-2
2-diethylamino-1,3,2-dioxaphosphorinane

: O-(3-S-trifluoromethyl)propyl S-trifluoromethyl N,N-diethylamidophosphorothioate

Conditions

Conditions	Yield
In dichloromethane -85 to -80 deg C, 30 min, then 15-20 deg C, 5 h;	85%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 3,4,5-trimethoxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 3,4,5-trimethoxy-1,2-bis(trifluoromethylthio)benzene

Conditions

Conditions	Yield
With cesium fluoride In 1,2-dimethoxyethane at 85℃; for 24h; Inert atmosphere; Sealed tube;	84%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 3440-92-4
2-(diethylamino)-4-methyl-1,3,2-dioxaphospholane

: O-(1-methyl, 2-S-trifluoromethyl)ethyl S-trifluoromethyl N,N-diethylamidophosphorothioate

Conditions

Conditions	Yield
In dichloromethane -85 to -80 deg C, 30 min, then 15-20 deg C, 5 h;	83%

: 372-64-5
Bis(trifluoromethyl)disulfid

: C24H33F3O5SSi

: C22H24F6O2S2

Conditions

Conditions	Yield
With cesium fluoride In 1,2-dimethoxyethane at 110℃; for 48h; Inert atmosphere; Sealed tube;	83%

: 372-64-5
Bis(trifluoromethyl)disulfid

: (6-iodo-2,3,4-trimethoxyphenyl)dimethylsilane

A: C10H10F3IO3S

B: 3,4,5-trimethoxy-1,2-bis(trifluoromethylthio)benzene

Conditions

Conditions	Yield
With cesium fluoride In 1,2-dimethoxyethane at 110℃; for 37h; Inert atmosphere; Sealed tube;	A n/a B 82%

...Expand

: 372-64-5
Bis(trifluoromethyl)disulfid

: 3741-34-2
2-diethylamino-1,3,2-dioxaphospholane

: O-2-(S-trifluoromethyl)ethyl S-trifluoromethyl N,N-diethylamidophosphorothioate

Conditions

Conditions	Yield
In dichloromethane -85 to -80 deg C, 30 min, then 15-20 deg C, 5 h;	81%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 33757-50-5
4-methoxy-N-(8-quinolinyl)benzamide

: 1404616-69-8
N-(2,6-di(trifluoromethylthio)-4-methoxybenzoyl)-8-aminoquinoline

Conditions

Conditions	Yield
With copper diacetate In dimethyl sulfoxide at 100℃; for 5.75h;	81%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 104-94-9
4-methoxy-aniline

: 78914-94-0
4-methoxyphenyl trifluoromethylsulfide

Conditions

Conditions	Yield
Stage #1: 4-methoxy-aniline With tetrafluoroboric acid; tert.-butylnitrite In water; acetic acid at 20℃; for 0.0833333h; Green chemistry; Stage #2: Bis(trifluoromethyl)disulfid With sodium acetate In dimethyl sulfoxide at 20℃; for 8h; Inert atmosphere; Green chemistry;	81%
Stage #1: 4-methoxy-aniline With tetrafluoroboric acid; sodium nitrite In water at 0℃; for 0.666667h; Stage #2: Bis(trifluoromethyl)disulfid With tris(bipyridine)ruthenium(II) dichloride hexahydrate In dimethyl sulfoxide at 20℃; for 1h; Reagent/catalyst; Inert atmosphere; Irradiation;	131.2 mg

: 372-64-5
Bis(trifluoromethyl)disulfid

: 1-(trimethylsilyl)-5,6,7,8-tetrahydronaphthalen-2-yl trifluoromethanesulfonate

: 1,2-bis((trifluoromethyl)thio)-5,6,7,8-tetrahydronaphthalene

Conditions

Conditions	Yield
With cesium fluoride In 1,2-dimethoxyethane at 110℃; for 46h; Inert atmosphere; Sealed tube;	81%

: 372-64-5
Bis(trifluoromethyl)disulfid

: 121-45-9
phosphorous acid trimethyl ester

A: 421-16-9
methyl trifluoromethyl sulphide

B: 30295-39-7
O,O-dimethyl-S-trifluoromethyl phosphorthioate

Conditions

Conditions	Yield
In dichloromethane 1) -75 deg C, 2) 20 deg C, 50 min;	A n/a B 80%
In dichloromethane -75 to 20°C;	A n/a B 80%
In dichloromethane -75 to 20°C;	A n/a B 80%

...Expand

: (bis(triphenylphosphoranylidene)ammonium){CpMo(CO)3}

: 372-64-5
Bis(trifluoromethyl)disulfid

: [(η(5)-C5H5)Mo(CO)3SCF3]

Conditions

Conditions	Yield
In dichloromethane a soln. of Mo-complex and CF3SSCF3 was stirred under N2 at room temp. for 2 h (IR monitoring); solvent was removed by evapn. under a stream of N2, product purified by chromy. on Al2O3 and crystn.;	80%

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