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HUBEI RISON CHEMICAL CO.,LTD.

Founded in 2005, Wuhan Rison Trading co.,ltd is engaged in supplying various speciality chemicals, which are used for electroplating, pharmaceuticals, Oled, paint ,plastic, rubber and other industry. Our customers got to used to request package produ

N,N-Dimethylsulfamoyl chloride CAS:13360-57-1

Cas:13360-57-1

Min.Order:1 Metric Ton

Negotiable

Type:Other

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Dimethylsulfamoy Chloride supplier in China

Cas:13360-57-1

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:10 Kilogram

FOB Price: $20.0

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Dimethylsulphamoyl chloride

Cas:13360-57-1

Min.Order:1

Negotiable

Type:Other

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Dimethylsulfamoyl chloride Basic information Product Name: Dimethylsulfamoyl chloride Synonyms: dimethylamidosulfonylchloride;dimethylaminosulfonylchloride;dimethyl-sulfamoylchlorid;Sulf

TIANFU-CHEM CAS:13360-57-1 Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name: Dimethylsulfamoyl chloride Synonyms: dimethylamidosulfonylchloride;dimethylaminosulfonylchloride;dimethyl-sulfamoylchlorid;Sulfamoylchloride,dimethyl-;DIMETHYLSULFAMOYL CHLORIDE;DIMETHYLAMINOS

Dimethylsulfamoyl chloride CAS: 13360-57-1

Cas:13360-57-1

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Sulfamoyl chloride,N,N-dimethyl- 13360-57-1

Cas:13360-57-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Dimethylsulfamoyl chloride CAS: 13360-57-1 MF: C2H6ClNO2S MW: 143.59 EINECS: 236-412-4 Mol File: 13360-57-1.mol Dimethylsulfamoyl chloride Structure Dimethylsulfamoyl chloride Chemical Properties Melting point -1

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Dimethylsulfamoyl chloride 99%

Cas:13360-57-1

Min.Order:1 Kilogram

FOB Price: $89.0 / 98.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Dimethylsulfamoyl chloride CAS:13360-57-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi

Dimethylsulfamoyl chloride CAS:13360-57-1

Cas:13360-57-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Sulfamoyl chloride,N,N-dimethyl-

Cas:13360-57-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Sulfamoyl chloride,N,N-dimethyl-

Cas:13360-57-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Triumph International Development Limilted

Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h

N,N-Dimethylsulfamoyl chloride 13360-57-1

Cas:13360-57-1

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Dimethylsulfamoy Chloride

Cas:13360-57-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

N-Dimethylaminosulfonyl chloride

Cas:13360-57-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Dimethylsulfamoy Chloride

Cas:13360-57-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: N,N-Dimethylsulfamoyl Chloride CAS No.: 13360-57-1 Molecule Formula:C2H6ClNO2S Molecule Weight:143.59 Purity: 99.0% Package: 250kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard

Lower Price N,N-Dimethylsulfamoyl Chloride

Cas:13360-57-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

N,N-Dimethylsulfamoyl chloride

Cas:13360-57-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Synthetic route

N,N-dimethylammonium chloride

N,N-dimethylammonium chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

dimethylchloroamine
1585-74-6

dimethylchloroamine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfur dioxide In tetrachloromethane 1.) 0 deg C, 1.5 h, 2.) up to r.t., overnight;70%
dimethyl amine
124-40-3

dimethyl amine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride
With sulfuryl dichloride; triethylamine In 1,4-dioxane; chloroform at 0 - 20℃;
N,N-Dimethylcarbamoyl chloride
79-44-7

N,N-Dimethylcarbamoyl chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With chlorosulphuric acid
With sulfur trioxide
Carbamidsaeure-methylester-N-sulfonsaeure-dimethylamid
89168-09-2

Carbamidsaeure-methylester-N-sulfonsaeure-dimethylamid

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride
C5H15N2O2S(1+)*Cl(1-)
29777-18-2

C5H15N2O2S(1+)*Cl(1-)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
at 60℃;
C2H6NO2S(1-)*Na(1+)

C2H6NO2S(1-)*Na(1+)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With chlorine In tetrachloromethane
C2H6NO3S(1-)*Na(1+)
41955-27-5

C2H6NO3S(1-)*Na(1+)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With trichlorophosphate In 1,2-dichloro-ethane at 80℃; for 18h;
antimony (V) pentachloride

antimony (V) pentachloride

N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In acetonitrile44.2 g (87%)
With sulfuryl dichloride In acetonitrile44.2 g (87%)
With sulfuryl dichloride In acetonitrile44.2 g (87%)
dipropylchloroborane
22086-53-9

dipropylchloroborane

tetramethylsulfamide
3768-63-6

tetramethylsulfamide

A

(dimethylamino)di-n-propylborane
13113-78-5

(dimethylamino)di-n-propylborane

B

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

dibutylchloroborane
1730-69-4

dibutylchloroborane

tetramethylsulfamide
3768-63-6

tetramethylsulfamide

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4,4-ethylenedioxy-piperidine
177-11-7

4,4-ethylenedioxy-piperidine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1,4-dioxa-8-azaspiro[4.5]decane-8-sulfonamide
877796-41-3

N,N-dimethyl-1,4-dioxa-8-azaspiro[4.5]decane-8-sulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 1h;100%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-t-Butoxycarbonylpiperazine
57260-71-6

1-t-Butoxycarbonylpiperazine

(S)-6'-chloro-N-((R)-hept-6-en-3-ylsulfonyl)-5-((2-((S)-1-hydroxyallyl)-2-methylcyclobutyl)methyl)-3',4,4',5-tetrahydro-2H,2’H-spiro[benzo[b][1,4]oxazepine-3,1’-naphthalene]-7-carboxamide
253176-45-3

(S)-6'-chloro-N-((R)-hept-6-en-3-ylsulfonyl)-5-((2-((S)-1-hydroxyallyl)-2-methylcyclobutyl)methyl)-3',4,4',5-tetrahydro-2H,2’H-spiro[benzo[b][1,4]oxazepine-3,1’-naphthalene]-7-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; for 12h;92%
With triethylamine at 0 - 20℃; for 4h; Inert atmosphere;89%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-t-Butoxycarbonylpiperazine
57260-71-6

1-t-Butoxycarbonylpiperazine

piperazine-1-sulfonic acid dimethylamide
98961-97-8

piperazine-1-sulfonic acid dimethylamide

Conditions
ConditionsYield
Stage #1: dimethylamino sulfonyl chloride; 1-t-Butoxycarbonylpiperazine With triethylamine In tetrahydrofuran at 0℃; for 1h;
Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; for 48h;
Stage #3: With sodium hydroxide In dichloromethane; water
100%
N,N-diethyl-4-[7-hydroxy-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-1-yl]benzamide
857252-49-4

N,N-diethyl-4-[7-hydroxy-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-1-yl]benzamide

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-{4-[(diethylamino)carbonyl]phenyl}-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-7-yl dimethylsulfamate
857252-50-7

1-{4-[(diethylamino)carbonyl]phenyl}-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-7-yl dimethylsulfamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 22h;100%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

(2S,4S)-2-aminomethyl-1-p-methoxybenzyloxycarbonyl-4-tritylthiopyrrolidine
148016-92-6

(2S,4S)-2-aminomethyl-1-p-methoxybenzyloxycarbonyl-4-tritylthiopyrrolidine

(2S,4S)-1-p-methoxybenzyloxycarbonyl-2-N,N-dimethylsulfamoylaminomethyl-4-tritylthiopyrrolidine

(2S,4S)-1-p-methoxybenzyloxycarbonyl-2-N,N-dimethylsulfamoylaminomethyl-4-tritylthiopyrrolidine

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
2-fluorophenol
367-12-4

2-fluorophenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C8H10FNO3S
1201594-21-9

C8H10FNO3S

Conditions
ConditionsYield
Stage #1: 2-fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 23℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane at 23℃; for 11h;
100%
salicylonitrile
611-20-1

salicylonitrile

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C9H10N2O3S
1263387-24-1

C9H10N2O3S

Conditions
ConditionsYield
Stage #1: salicylonitrile With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 11h;
100%
4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole
1288963-67-6

4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

2-(3,5-dimethylisoxazol-4-yl)-3-(4-methoxyphenyl)-N,N-dimethyl-1H-indole-1-sulfonamide
1288963-72-3

2-(3,5-dimethylisoxazol-4-yl)-3-(4-methoxyphenyl)-N,N-dimethyl-1H-indole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole With sodium hydride In n-heptane; N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In n-heptane; N,N-dimethyl-formamide at 0 - 20℃; for 2h;
100%
Stage #1: 4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 0 - 20℃; for 2h;
Stage #3: With water In N,N-dimethyl-formamide
100%
2-(3-amino-phenyl)-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester
1343453-37-1

2-(3-amino-phenyl)-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

ethyl 2-(3-(N,N-dimethylsulfamoylamino)phenyl)-3,3-dimethyl-1,2,3,4-tetrahydroquinoline-6-carboxylate
1343454-35-2

ethyl 2-(3-(N,N-dimethylsulfamoylamino)phenyl)-3,3-dimethyl-1,2,3,4-tetrahydroquinoline-6-carboxylate

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 25℃; for 16h;100%
With pyridine In dichloromethane at 0 - 25℃; for 16h;
3-methoxy-4-hydroxybenzonitrile
4421-08-3

3-methoxy-4-hydroxybenzonitrile

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-cyano-2-methoxyphenyl N,N-dimethylsulfamate
1432739-31-5

4-cyano-2-methoxyphenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 3-methoxy-4-hydroxybenzonitrile With dmap; triethylamine In dichloromethane at 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In dichloromethane at 20℃; for 16h;
100%
4-chloro-phenol
106-48-9

4-chloro-phenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-chlorophenyl N,N-dimethylsulfamate
1135-05-3

4-chlorophenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 4-chloro-phenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 16h;
100%
Stage #1: 4-chloro-phenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 10h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃;
83%
2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride

2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

2,4-dichloro-N,N-dimethyl-5,8-dihydropyrido[3,4-d]pyrimidine-7(6H)-sulfonamide

2,4-dichloro-N,N-dimethyl-5,8-dihydropyrido[3,4-d]pyrimidine-7(6H)-sulfonamide

Conditions
ConditionsYield
Stage #1: 2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride With triethylamine In dichloromethane
Stage #2: dimethylamino sulfonyl chloride In dichloromethane
100%
NH-pyrazole
288-13-1

NH-pyrazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1H-pyrazole-1-sulfonamide
133228-21-4

N,N-dimethyl-1H-pyrazole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: NH-pyrazole With sodium hydride In tetrahydrofuran at 20℃; for 1h;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran for 1.5h;
99%
Stage #1: NH-pyrazole With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere;
99%
With sodium hydride In tetrahydrofuran; mineral oil for 1.33333h; Inert atmosphere;91%
methoxybenzene
100-66-3

methoxybenzene

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-4-methoxybenzenesulfonamide
59907-37-8

N,N-dimethyl-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
indium(III) triflate In 1,2-dichloro-ethane at 100℃; for 24h;99%
4-hydroxy-benzaldehyde
123-08-0

4-hydroxy-benzaldehyde

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-formylphenyl N,N-dimethylsulfamate

4-formylphenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
With N,N-dimethyl-cyclohexanamine at 90 - 95℃; for 3h;99%
With N-ethyl-N,N-diisopropylamine at 90℃; for 2.5h;
4-Fluorophenol

4-Fluorophenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-fluorophenyl N,N-dimethylsulfamate
1259092-05-1

4-fluorophenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 16h;
99%
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.25h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; Inert atmosphere;
91%
With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 11h; Inert atmosphere;
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 12h;
4-ethoxycarbonylpyrazole
37622-90-5

4-ethoxycarbonylpyrazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

ethyl 1-(N,N-dimethylsulfamoyl)-1H-pyrazole-4-carboxylate

ethyl 1-(N,N-dimethylsulfamoyl)-1H-pyrazole-4-carboxylate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In acetonitrile for 1h; Inert atmosphere;99%
Stage #1: 4-ethoxycarbonylpyrazole With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.333333h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran; mineral oil at 25℃; for 22h; Inert atmosphere;
91%
methyl 3-(acetylamino)-1H-pyrazole-5-carboxylate
1202657-29-1

methyl 3-(acetylamino)-1H-pyrazole-5-carboxylate

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C9H14N4O5S

C9H14N4O5S

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In acetonitrile at 0 - 20℃; for 18h;99%
C17H19NO4

C17H19NO4

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C23H34N4O10S3

C23H34N4O10S3

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 10h;98.2%
methylamine
74-89-5

methylamine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N,N′-trimethylsulfamide
76820-42-3

N,N,N′-trimethylsulfamide

Conditions
ConditionsYield
In tetrahydrofuran98%
With potassium carbonate In tetrahydrofuran; dichloromethane at 0 - 25℃; for 2h;97%
In water; benzene at 50℃; for 5h;87%
With toluene
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethylsulfamide
3984-14-3

N,N-dimethylsulfamide

Conditions
ConditionsYield
With ammonia In methanol at 60℃; for 16h; Sealed tube;98%
With ammonium hydroxide at 0℃; for 3h;94%
With ammonium hydroxide at 0℃; ice-bath;76%
1H-imidazole
288-32-4

1H-imidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1H-imidazole-1-sulfonamide
78162-58-0

N,N-dimethyl-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
With triethylamine In toluene at 20℃; for 8h;98%
With triethylamine In benzene for 16h; Ambient temperature;95%
With triethylamine In diethyl ether at 20℃; for 16h;94.75%
1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose
17073-95-9

1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1,6-anhydro-2-O-(N,N-dimethylsulfamoyl)-3,4-O-isopropylidene-β-D-talopyranose
98815-77-1

1,6-anhydro-2-O-(N,N-dimethylsulfamoyl)-3,4-O-isopropylidene-β-D-talopyranose

Conditions
ConditionsYield
With 1H-imidazole; sodium hydride In tetrahydrofuran for 2h; Heating;98%
α-naphthol
90-15-3

α-naphthol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

naphthalen-1-yl N,N-dimethylsulfamate
1144-13-4

naphthalen-1-yl N,N-dimethylsulfamate

Conditions
ConditionsYield
With sodium hydride In 1,2-dimethoxyethane at 23℃; for 17h; Inert atmosphere;98%
Stage #1: α-naphthol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 23℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 23℃; for 11h;
95%
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In benzene at 50℃; for 6h;94%
4(5)-(4-tolyl)-1H-imidazole
670-91-7

4(5)-(4-tolyl)-1H-imidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-(dimethylsulfamoyl)-5-p-tolylimidazole

1-(dimethylsulfamoyl)-5-p-tolylimidazole

Conditions
ConditionsYield
With potassium carbonate In ethyl acetate at 77℃; for 6h; Temperature;98%
C17H20N6

C17H20N6

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C21H30N8O4S2

C21H30N8O4S2

Conditions
ConditionsYield
Stage #1: C17H20N6 With sodium hydroxide In N,N-dimethyl-formamide for 0.5h; Cooling;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 220℃; for 4h; Autoclave;
97.6%
4-iodoimidazole
71759-89-2

4-iodoimidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-iodo-N,N-dimethyl-1H-imidazole-1-sulfonamide
135773-25-0

4-iodo-N,N-dimethyl-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 4-iodoimidazole; dimethylamino sulfonyl chloride With sodium hydroxide In tetrahydrofuran at 8 - 20℃;
Stage #2: In n-heptane at 70℃; for 4h;
97.3%
With triethylamine In acetonitrile at 20℃; for 2h;80%
With triethylamine In dichloromethane for 60h; Heating;60%
With triethylamine In dichloromethane at 20℃; for 26h; Inert atmosphere;58%
2-methyl-propan-1-ol
78-83-1

2-methyl-propan-1-ol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

isobutyl N,N-dimethylsulfamate
66950-72-9

isobutyl N,N-dimethylsulfamate

Conditions
ConditionsYield
With sodium hydride In 1,2-dimethoxyethane97%
(+/-)-(1S*,6S*,8R*,9R*,10S*,11S*)-2,2-Dimethoxy-10,11-epoxy-6-methyl-12-oxatricyclo<6.3.1.01,6>dodecan-9-ol

(+/-)-(1S*,6S*,8R*,9R*,10S*,11S*)-2,2-Dimethoxy-10,11-epoxy-6-methyl-12-oxatricyclo<6.3.1.01,6>dodecan-9-ol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C16H27NO7S

C16H27NO7S

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran 1.) r.t., 5 min, 2.) r.t., 1 h;97%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

3,4-bis(trimethylsilyl)-1H-pyrrole
195820-65-6

3,4-bis(trimethylsilyl)-1H-pyrrole

N-N-dimethyl 3,4-bis(trimethylsilyl)-1H-pyrrole-1-sulfonamide
278167-17-2

N-N-dimethyl 3,4-bis(trimethylsilyl)-1H-pyrrole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 3,4-bis(trimethylsilyl)-1H-pyrrole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 2h; Metallation;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 0 - 20℃; for 2h; Substitution; Further stages.;
97%
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