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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Name:4-Hydroxy-3-methoxybenzonitrile CAS:4421-08-3 Grade:For chemical industry, scientific research and export Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryProduct name: 4-Hydroxy-3-Methoxybenzonitrile CAS No.:4421-08-3 Molecule Formula:C8H7NO2 Molecule Weight:149.15 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiry4-Hydroxy-3-methoxybenzonitrile Chemical Properties Melting point 85-87 °C (lit.) Boiling point 270.21°C (rough estimate) density 1.2517 (rough estimate) refractive index 1.5320 (estimate) pka 7.84±0.18(Predicted) CA
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiry4-Hydroxy-3-methoxybenzonitrileAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Hebei Tecxiang Chemical Co., Ltd. is an enterprise specializing in the research and development, production and trade of pharmaceutical intermediates, apis and chemical raw materials and formula technology. Our company has extensive experience in the
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inquiryTAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry4-Hydroxy-3-methoxybenzonitrile cas 4421-08-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryBest quality with low priceAppearance:beige crystalline powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiryreagent grade ex stockAppearance:white or off-white crystalline powder Storage:Keep away of light,cool place Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:by Fedex, ship or plane
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inquiryHangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:5g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
With phenoxyamine hydrochloride In methanol; aq. phosphate buffer; water-d2 at 60℃; for 8h; pH=6.5; | 99% |
With iron(III) chloride; hydroxylamine hydrochloride In N,N-dimethyl-formamide for 3h; Reagent/catalyst; Reflux; | 98% |
With copper(II) oxide; hydroxylamine hydrochloride In neat (no solvent) for 0.0194444h; Mechanism; Reagent/catalyst; Microwave irradiation; Green chemistry; | 98% |
Conditions | Yield |
---|---|
With iron(III) chloride; silica gel In neat (no solvent) at 110℃; for 1.5h; Catalytic behavior; Concentration; Temperature; Green chemistry; | 98% |
With silica gel for 0.0166667h; microwave irradiation; | 95% |
With hydroxylamine hydrochloride; phosphorus pentoxide; silica gel for 0.0166667h; microwave irradiation; | 95% |
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
at 100℃; for 8h; Beckmann rearrangement; | 92% |
2-methoxy-4-iodophenol
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; copper(II) acetate monohydrate In water at 180℃; for 22h; | 86% |
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 130℃; for 10h; Schlenk technique; | 86% |
veratronitrile
A
3-methoxy-4-hydroxybenzonitrile
B
2-methoxy-5-cyanophenol
Conditions | Yield |
---|---|
With sodium methylate; 1-dodecylthiol In N,N-dimethyl-formamide at 100℃; for 1h; | A 83% B 17% |
Conditions | Yield |
---|---|
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 110℃; under 2250.23 Torr; for 15h; Autoclave; Green chemistry; | 83% |
(E)-4-hydroxy-3-methoxybenzaldehyde oxime
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
at 120℃; for 2.5h; Beckmann rearrangement; Heating; | 73% |
2-(2-methoxy-4-cyanophenoxy)-acetic acid
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
Stage #1: 2-(2-methoxy-4-cyanophenoxy)-acetic acid With triethylamine In N,N-dimethyl-formamide; toluene for 3h; Curtius rearrangement; Heating; Stage #2: With potassium hydroxide; glycerol In ethanol; N,N-dimethyl-formamide; toluene for 2h; Heating; Further stages.; | 70% |
methyl 3,4-dimethoxybenzoate
A
3,4-dihydroxybenzonitrile
B
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran at 185℃; for 24h; | A 63% B 23% |
Conditions | Yield |
---|---|
With iron(III) trifluoromethanesulfonate; sodium nitrite In dimethyl sulfoxide at 50℃; for 10h; Inert atmosphere; Sealed tube; | 62% |
2-methoxy-4-iodophenol
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; copper(II) acetate monohydrate In water at 20 - 140℃; Microwave irradiation; | 59% |
methyl 3,4-dimethoxybenzoate
A
3-methoxy-4-hydroxybenzonitrile
B
2-methoxy-5-cyanophenol
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran at 110℃; for 24h; | A 55% B 18% |
veratronitrile
A
3,4-dihydroxybenzonitrile
B
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With 1,3-dimethyl-2-imidazolidinone; sodium hexamethyldisilazane In tetrahydrofuran at 185℃; for 12h; further reagent: LDA; | A 53% B 28% |
4-bromoguaiacol
P-toluenesulfonyl cyanide
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
Stage #1: 4-bromoguaiacol; P-toluenesulfonyl cyanide With potassium phosphate; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In acetone for 0.25h; Inert atmosphere; Sealed tube; Stage #2: With 1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)-2-trisilanol In acetone for 12h; Inert atmosphere; Irradiation; | 41% |
4-cyano-2-methoxyphenyl acetate
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With potassium hydroxide | |
With hydrogenchloride | |
With potassium hydroxide In ethanol for 0.333333h; Heating; Yield given; |
4-(benzyloxy)-3-methoxybenzonitrile
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal |
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; FeOO280 In toluene for 6h; Condensation; dehydration; Heating; | A 43 % Chromat. B 57 % Chromat. |
With hydroxylamine hydrochloride; titanium(IV) oxide for 0.00833333h; Microwave irradiation; Neat (no solvent); |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (NH2OH)2*H2SO4; sodium acetate / ethanol / Heating 2: SOCl2 / benzene / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 89 percent / aq. NaOH; hydroxylamine hydrochloride / ethanol / 0 - 20 °C 2: 85 percent / phthalic anhydride / 0.08 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NH2OH*HCl; Et3N / CHCl3 / 0 - 20 °C 2: bis(trichloromethyl) carbonate / CHCl3 / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) NH2OH*HCl, Py, (ii) DCC, CuSO4*5H2O, Et3N 2: H2 / Pd-C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; ammonia In water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: laccase from Trametesversicolor; oxygen / dimethyl sulfoxide / 16 h / 30 °C / pH 4.7 / Enzymatic reaction 2: hydroxylamine hydrochloride / acetonitrile / 4 h / Reflux View Scheme |
4-((2-(1H-tetrazol-5-yl)hydrazono)methyl)-2-methoxyphenol
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: laccase from Trametesversicolor; oxygen / ethanol / 2 h / 30 °C / pH 4.7 / Enzymatic reaction 2: hydroxylamine hydrochloride / acetonitrile / 4 h / Reflux View Scheme |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-Bromosuccinimide 2: N,N-dimethyl-formamide View Scheme |
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With sodium azide; zinc dibromide In water; isopropyl alcohol at 80℃; for 24h; | 100% |
With ammonium azide; ammonium chloride; lithium chloride In N,N-dimethyl-formamide at 120 - 130℃; for 24h; | 40% |
3-methoxy-4-hydroxybenzonitrile
benzyl bromide
4-(benzyloxy)-3-methoxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 18h; | 100% |
Stage #1: 3-methoxy-4-hydroxybenzonitrile With potassium carbonate In acetonitrile at 20℃; for 0.166667h; Stage #2: benzyl bromide In acetonitrile for 5h; Reflux; | 96.8% |
3-methoxy-4-hydroxybenzonitrile
tert-butyldimethylsilyl chloride
4-(tert-butyldimethylsilyloxy)-3-methoxybenzonitrile
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 2h; Inert atmosphere; | 100% |
3-methoxy-4-hydroxybenzonitrile
dimethylamino sulfonyl chloride
4-cyano-2-methoxyphenyl N,N-dimethylsulfamate
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-hydroxybenzonitrile With dmap; triethylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: dimethylamino sulfonyl chloride In dichloromethane at 20℃; for 16h; | 100% |
ethyl bromide
3-methoxy-4-hydroxybenzonitrile
4-ethoxy-3-methoxybenzonitrile
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-hydroxybenzonitrile With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.583333h; Stage #2: ethyl bromide In N,N-dimethyl-formamide at 0 - 20℃; | 100% |
With potassium carbonate In acetone Reflux; |
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With laccase from Trametesversicolor; oxygen In aq. acetate buffer at 30℃; for 2h; pH=4.7; Reagent/catalyst; Enzymatic reaction; | 99% |
With laccase from Trametes versicolor; oxygen In acetone at 20℃; for 24h; pH=5; Green chemistry; Enzymatic reaction; | 95% |
With laccase from Trametes versicolor; oxygen In acetone at 20℃; for 24h; pH=5; Enzymatic reaction; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; Williamson Ether Synthesis; Inert atmosphere; | 99% |
trifluoromethylsulfonic anhydride
3-methoxy-4-hydroxybenzonitrile
3-methoxy-4-O-trifluoromethylsulfonylbenzonitrile
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -78 - 20℃; for 14h; Inert atmosphere; | 98.4% |
With pyridine at 20 - 25℃; | 92% |
With pyridine at 20 - 25℃; for 1h; | 92% |
3-methoxy-4-hydroxybenzonitrile
ethyl iodide
4-ethoxy-3-methoxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 0 - 40℃; for 16h; | 98% |
With potassium hydroxide |
3-methoxy-4-hydroxybenzonitrile
3,4-dihydroxybenzonitrile
Conditions | Yield |
---|---|
With aluminium(III) iodide; diisopropyl-carbodiimide In acetonitrile at 80℃; for 18h; | 98% |
With aluminium(III) iodide; calcium oxide In acetonitrile at 80℃; for 18h; | 95% |
With aluminium(III) iodide In dimethyl sulfoxide; acetonitrile at 80℃; for 18h; | 95% |
3-methoxy-4-hydroxybenzonitrile
mechlorethamine hydrochloride
1,5-bis(4-cyano-2-methoxyphenoxy)-N-methyl-3-azapentane
Conditions | Yield |
---|---|
With potassium carbonate In 1-methyl-pyrrolidin-2-one at 115℃; for 3h; | 98% |
3-methoxy-4-hydroxybenzonitrile
3-(bromomethyl)benzonitrile
3-cyanobenzyl 4-cyano-2-methoxyphenyl ether
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-hydroxybenzonitrile With potassium carbonate In N,N-dimethyl-formamide for 0.5h; Stage #2: m-(bromomethyl)benzonitrile In N,N-dimethyl-formamide | 98% |
3-methoxy-4-hydroxybenzonitrile
2-(chloromethyl)-5-(4-fluorophenyl)-1,3,4-oxadiazole
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 20℃; | 98% |
3-methoxy-4-hydroxybenzonitrile
benzyl chloride
4-(benzyloxy)-3-methoxybenzonitrile
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-hydroxybenzonitrile With potassium carbonate In acetonitrile at 20℃; for 0.166667h; Stage #2: benzyl chloride In acetonitrile for 5h; Reflux; | 95.7% |
With potassium carbonate In acetone | 88% |
2-iodo-propane
3-methoxy-4-hydroxybenzonitrile
4-isopropoxy-3-methoxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 22h; Reflux; | 95% |
With potassium carbonate In acetone for 22h; Reflux; |
3-methoxy-4-hydroxybenzonitrile
3-methoxy-4-(4-(4-methyl-3-oxopiperazin-1-yl)cyclohexyloxy)benzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl acetamide at 120℃; for 3h; | 94% |
spiro[7-azoniabicyclo[2,2,1]heptane-7,4'-[1'-methyl-2'-oxo-4'-piperazinium]methanesulphonate]
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In ISOPROPYLAMIDE at 120℃; for 3h; | 94% |
1-chloro-4-pentyne
3-methoxy-4-hydroxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In 1-methyl-pyrrolidin-2-one at 65℃; for 24h; | 93% |
3-methoxy-4-hydroxybenzonitrile
chloromethyl methyl ether
3-methoxy-4-(methoxymethyloxy)benzonitrile
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h; | 92% |
With N-ethyl-N,N-diisopropylamine In dichloromethane | 80% |
1,1'-(Azodicarbonyl)dipiperidin
3-methoxy-4-hydroxybenzonitrile
4-(4-chlorophenyl)-5-(3-hydroxypropyl)-2-(2-methylimidazol-1-yl)oxazole
4-(4-chlorophenyl)-5-[3-(4-cyano-2-methoxyphenoxy)propyl]-2-(2-methyl-1-imidazolyl)oxazole
Conditions | Yield |
---|---|
With tributylphosphine In tetrahydrofuran | 92% |
3-methoxy-4-hydroxybenzonitrile
trifluoromethanesulfonic acid anhydride
3-methoxy-4-O-trifluoromethylsulfonylbenzonitrile
Conditions | Yield |
---|---|
With pyridine at 0 - 25℃; | 92% |
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-4-hydroxybenzonitrile With potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: 1-bromo-butane In water; N,N-dimethyl-formamide at 20 - 37℃; | 92% |
Stage #1: 3-methoxy-4-hydroxybenzonitrile With potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: 1-bromo-butane In water; N,N-dimethyl-formamide at 20 - 37℃; |
3-methoxy-4-hydroxybenzonitrile
2-(chloromethyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 20℃; | 92% |
3-methoxy-4-hydroxybenzonitrile
4-ethoxy-3-methoxybenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20 - 37℃; | 91.8% |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene at 50℃; for 1h; Oxidation; Diels-Alder cycloaddition; | 91% |
With [bis(acetoxy)iodo]benzene at 50℃; for 4h; Diels-Alder reaction; | 91% |
triisopropylsilyl chloride
3-methoxy-4-hydroxybenzonitrile
3-methoxy-4-(triisopropylsilyloxy)benzonitrile
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 91% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 91% |
3-methoxy-4-hydroxybenzonitrile
acetyl chloride
4-cyano-2-methoxyphenyl acetate
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran at 20℃; for 2h; | 91% |
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