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Cas:542-18-7
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryISO Certification Technology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure
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inquiryChlorocyclohexane Manufacturer Factory CAS 542-18-7 Cyclohexyl chloride Chlorocyclohexane Manufacturer High quality Best price In stock factory CAS 542-18-7 Chlorocyclohexane COA TDS price MSDS highly quality and immedaite delivery Chlo
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inquiryTIANFUCHEM--542-18-7--Chlorocyclohexane factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relat
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inquiryProduct Description Name Chlorocyclohexane CAS 542-18-7 Assay 99% Appearance
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryProduct information Product name: Chlorocyclohexane Synonyms: Cyclohexyl chloride; Chlorhexamethylene; 1-Chlorocyclohexane CAS#: 542-18-7 EINECS#: 208-806-6 Molecular Formula: C6H11Cl Molecular Weight: 118.6045 Description Melti
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inquiryChlorocyclohexane CAS:542-18-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Detail Minimum Order Qty. 10 Gram
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryadvantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product name: Chlorocyclohexane CAS No.:542-18-7 Molecule Formula:C6H11Cl Molecule Weight:118.60 Purity: 99.0% Package: 200kg/drum Description:Colorless clear liquid Manufacture Standards:Enterprise Standard TESTIN
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inquiryChlorocyclohexane Chemical Properties Melting point -44 °C (lit.) Boiling point 142 °C (lit.) density 1 g/mL at 25 °C (lit.) vapor pressure 7 hPa (20 °C) refractive index n20/D 1.462(lit.) Fp 84 °F storage
Cas:542-18-7
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquirynonafluoro-tert-butanesulfenyl chloride
cyclohexane
A
nonafluoro-tert-butanethiol
B
cyclohexyl chloride
Conditions | Yield |
---|---|
A 100% B 100% | |
A 100% B 100% |
Conditions | Yield |
---|---|
With bismuth(III) chloride In tetrachloromethane for 0.0833333h; Heating; | 99% |
With 1,2,3-Benzotriazole; thionyl chloride In dichloromethane at 20℃; Substitution; | 92% |
With triphenylphosphine; zinc(II) chloride; diethylazodicarboxylate In tetrahydrofuran for 2h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With bismuth(III) chloride In 1,2-dichloro-ethane for 0.25h; Heating; | 98% |
Conditions | Yield |
---|---|
With hydrogenchloride; tetrabutyl-ammonium chloride; sodium chloride In water at 20℃; for 5h; Reagent/catalyst; | 97% |
With hydrogenchloride; potassium chloride; tetrabutyl-ammonium chloride In water at 20℃; Irradiation; Green chemistry; | 95% |
With sodium hypochlorite In water; acetone at 20℃; for 2h; Reagent/catalyst; Solvent; Time; Inert atmosphere; | 93% |
cyclohexane
dichlorofluoromethanesulphenyl chloride
A
cyclohexyl chloride
B
bis(dichlorofluoromethyl)disulfane
C
Dichlorfluormethyl-cyclohexylsulfid
Conditions | Yield |
---|---|
A 63.6% B 97% C 3% | |
A 63.6% B 97% C 3% |
Conditions | Yield |
---|---|
With ethanol; trichlorovinylsilane; tin(IV) chloride for 1h; Ambient temperature; | 90% |
With dichloromethane; RhCl(PPh3)3 | 72% |
With chloro-trimethyl-silane; water for 15h; Ambient temperature; | 70% |
Conditions | Yield |
---|---|
With hydrogenchloride at 105℃; for 3h; | 90% |
With boron trichloride In hexane at 0℃; for 0.0833333h; | 78% |
With diethylaluminium chloride In hexane at -78℃; for 0.166667h; | 74 % Chromat. |
Conditions | Yield |
---|---|
With CPT | A n/a B 90% |
chlorodifluoromethansulfenylchloride
cyclohexane
A
cyclohexyl chloride
B
bis(chlorodifluoromethyl)disulfane
C
(Chloro-difluoro-methylsulfanyl)-cyclohexane
D
benzyl chloro-difluoromethyl sulfide
Conditions | Yield |
---|---|
A 39.4% B 88.4% C 11.6% D 65% | |
A 39.4% B 88.4% C 11.6% D 65% |
cyclohexyl chloride
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; tetrachloromethane In water; tert-butyl alcohol for 4h; Irradiation; | 86% |
heptafluoro-propane-1-sulphenic acid chloride
cyclohexane
A
bis(perfluoro-n-propyl)disulfane
B
cyclohexyl chloride
C
heptafluoro-n-propyl cyclohexyl sulfide
Conditions | Yield |
---|---|
A 85.7% B 43.2% C 14.3% | |
A 85.7% B 43.2% C 14.3% | |
for 0.1h; Mechanism; Irradiation; effect of bis(trifluoromethyl) disulfide; |
2-methoxycyclohexane
A
cyclohexyl chloride
B
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With phenylacetyl chloride; zinc In Petroleum ether at 28℃; for 4h; Yields of byproduct given; | A 84% B n/a |
2-methoxycyclohexane
phenylacetyl chloride
A
cyclohexyl chloride
B
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With zinc In Petroleum ether at 28℃; for 4h; Yields of byproduct given; | A n/a B 84% |
Conditions | Yield |
---|---|
With 1-chloro-1-(dimethylamino)-2-methyl-1-propene In dichloromethane 1.) 0 deg C; 2.) rt., 3h; | A 18 % Spectr. B 82% |
With hydrogenchloride | |
With aluminium trichloride Erwaermen auf dem Dampfbad; |
A
2-methyl-1,2-benzisothiazole-3(2H)-one
B
cyclohexyl chloride
D
cyclohexene
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane for 1h; Mechanism; Product distribution; Heating; also pyrolysis in toluene, 110 deg C, 20 h, without SOCl2; further o-(N-methylcarbamoyl)phenyl sulphoxides; | A 81% B 11% C 16% D 67% |
With thionyl chloride In dichloromethane for 1h; Heating; | A 81% B 11% C 16% D 67% |
(1R,2R)-1-Chloro-2-iodo-cyclohexane
cyclohexyl chloride
Conditions | Yield |
---|---|
With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; tri-n-butyl-tin hydride In tetrahydrofuran for 0.25h; Ambient temperature; | 80% |
cyclohexane
benzyloxychlorocarbene
A
cyclohexyl chloride
B
benzyl chloride
C
cyclohexanol
Conditions | Yield |
---|---|
at 25℃; Photolysis; | A 9% B 80% C 11% |
Conditions | Yield |
---|---|
In benzene at 30℃; Kinetics; Solvent; Temperature; Inert atmosphere; Schlenk technique; | A n/a B 70% |
cyclohexane
1-Phenylethanol
A
cyclohexyl chloride
B
tert-butylamine hydrochloride
C
acetophenone
Conditions | Yield |
---|---|
With N,N-dichloro-t-butylamine at 20℃; for 1h; Irradiation; | A 68% B n/a C n/a |
Conditions | Yield |
---|---|
With dichloromethylsilane; iron(III) chloride In 1,2-dimethoxyethane for 6h; Heating; | 66% |
Multi-step reaction with 2 steps 1: diethyl ether; sodium; alcohol / Reagens 4: Kaliumcarbonat 2: fuming hydrochloric acid / 100 °C View Scheme | |
Stage #1: cyclohexanone With iron(III) chloride In ethyl acetate at 20℃; for 0.0166667h; Stage #2: With dimethylmonochlorosilane In ethyl acetate at 20℃; |
cyclohexane
heptafluoropropane-2-sulphenic acid chloride
A
cyclohexyl chloride
B
bis(perfluoroisopropyl) disulfide
C
heptafluoropropane-2-thiol
D
Heptafluorisopropylcyclohexylsulfid
Conditions | Yield |
---|---|
A 37.7% B 65% C n/a D 0.5% | |
A 37.7% B 65% C n/a D 0.5% |
Benzotrichlorid
cyclohexanol
A
benzylidene dichloride
B
cyclohexyl chloride
Conditions | Yield |
---|---|
With TOP; phenylsilane In neat (no solvent) at 100℃; for 24h; Appel Halogenation; Inert atmosphere; | A n/a B 57% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; (FeCl2(C6H6N2CO)(CH3)2(C5H4N)2(C(O)OCH3)2); tetrabutyl-ammonium chloride In acetonitrile at 25℃; for 0.583333h; Inert atmosphere; chemoselective reaction; | A 5.1% B 55.4% |
With [FeIV(1,1-di(pyridin-2-yl)-N,N-bis(quinolin-2-ylmethyl)methanamine)(O)]2+; [FeII(1,1-di(pyridin-2-yl)-N,N-bis(quinolin-2-ylmethyl)methanamine)(Cl)]Cl In acetonitrile at 25℃; for 0.5h; Inert atmosphere; Glovebox; | A 52% B n/a |
With 5,10,15,20-tetraphenyl-21 H,23-H-porphine manganese(III)chloride; iodosylbenzene In dichloromethane; water for 12h; | A 18% B 30% |
Trifluoromethylsulfenyl chloride
cyclohexane
A
Bis(trifluoromethyl)disulfid
B
cyclohexyl(trifluoromethyl)sulfane
C
cyclohexyl chloride
Conditions | Yield |
---|---|
byproducts: HCl; Irradiation (UV/VIS); | A 35% B 45% C 28% |
byproducts: HCl; Irradiation (UV/VIS); | A 35% B 45% C 28% |
for 0.2h; Mechanism; Irradiation; effect of bis(heptafluoro-n-propyl) disulfide; |
tetraethylammonium chloride
3-chloro-benzenecarboperoxoic acid
A
cyclohexyl chloride
B
3-chloro-benzoic acid ethyl ester
Conditions | Yield |
---|---|
With cyclohexane In acetonitrile at 20℃; for 3h; Yields of byproduct given; | A n/a B 38% |
cyclohexane
A
cyclohexyl chloride
B
cyclohexanone
C
cyclohexanol
Conditions | Yield |
---|---|
With chloroform; pyrimido<5,4-g>pteridine N-oxide for 3h; Product distribution; Mechanism; Irradiation; | A 11% B 12% C 37% |
With [oxoiron(IV)(tris-(quinolyl-2-methyl)amine)(chloride)](1+) In [D3]acetonitrile at -40℃; Reagent/catalyst; | A 35% B 3% C 7% |
With barium hexaferrite; acetic acid; magnesium chloride In dichloromethane at 23℃; for 2h; Product distribution; Further Variations:; Reagents; | A 31% B 13% C 10% |
Conditions | Yield |
---|---|
With potassium permanganate; aluminium trichloride In acetonitrile for 0.5h; | A 35% B 15% |
With [oxoiron(IV)(tris(pyridyl-2-methyl)amine)(chloride)](triflate) In [D3]acetonitrile at 25℃; Inert atmosphere; | A 11% B 2% |
With cis-VI(6,6'-Cl2bpy)2O2> In tetrachloromethane; acetonitrile at 20℃; for 0.5h; Oxidation; | A 0.5 % Chromat. B 50 % Chromat. |
With peracetic acid; triethylamine hydrochloride; acetic acid In acetonitrile at 22℃; Inert atmosphere; sealed system; |
tetrachloromethane
cyclohexene
A
cyclohexyl chloride
trans-1-trichloromethyl-2-chlorocyclohexane
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride; water at 150℃; for 6h; Autoclave; | A n/a B 25% C 25% |
cyclohexane
A
cyclohexyl chloride
B
tert-butyl cyclohexyl peroxide
C
cyclohexanone
D
cyclohexanol
Conditions | Yield |
---|---|
With Co(III)(BPI)(OAc)(OO-tBu) at 60℃; for 2h; Product distribution; stoichiometric oxidation by various cobalt(III)alkylperoxy complexes, solvents; | A n/a B 18% C 24% D 18% |
tert.-butylhydroperoxide
cyclohexane
acrylonitrile
A
cyclohexyl chloride
B
2-Chlor-3-cyclohexylpropiononitril
C
2-tert-Butylperoxy-3-cyclohexyl-propionitrile
Conditions | Yield |
---|---|
With acetic acid; ferric nitrate; copper dichloride In pyridine at 60℃; Product distribution; Mechanism; further with LiCl; | A 15.8% B 8.7% C 3.1% |
Conditions | Yield |
---|---|
With hydrogen bromide; ferric(III) bromide In dichloromethane at 25℃; for 0.3h; | 99% |
With hydrogen bromide at 105℃; for 4h; | 90% |
With ferric(III) bromide; hydrogen bromide In dichloromethane at 25℃; for 2h; | |
With hydrogen bromide; cetyltributylphosphonium bromide at 105℃; for 7h; | 80 % Chromat. |
With ferric(III) bromide; hydrogen bromide In dichloromethane at 25℃; for 0.3h; Product distribution; Mechanism; other alkyl chlorides; other hydrogen halide; also without HBr; var. reaction conditions; | 99 % Chromat. |
cyclohexyl chloride
N-<(S)-1-phenylethyl>-2-pyridinecarboxamide
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; ethylmagnesium bromide; manganese(ll) chloride In tetrahydrofuran at 60℃; for 14h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; chemoselective reaction; | 99% |
cyclohexyl chloride
4-methoxyphenyl magnesium bromide
4-cyclohexylanisole
Conditions | Yield |
---|---|
With iron(III) chloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0 - 40℃; for 1.66667h; | 98% |
Stage #1: cyclohexyl chloride With [1,3-bis(3,5-di-tert-butyl-2-hydroxybenzyl)benzimidazolium][FeCl4] In diethyl ether at 0℃; for 0.0333333h; Schlenk technique; Inert atmosphere; Stage #2: 4-methoxyphenyl magnesium bromide In diethyl ether at 0 - 30℃; for 2h; Temperature; Schlenk technique; Inert atmosphere; | 86% |
With iron(III) chloride; triethylamine In diethyl ether for 0.5h; Grignard cross-coupling reaction; Heating; |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 4h; Reagent/catalyst; Inert atmosphere; UV-irradiation; | 98% |
Conditions | Yield |
---|---|
With aluminum (III) chloride at 0 - 20℃; for 4h; Friedel-Crafts Alkylation; | 95% |
With aluminum (III) chloride at 3 - 20℃; |
cyclohexyl chloride
4-flourophenylmagnesium bromide
1-cyclohexyl-4-fluorobenzene
Conditions | Yield |
---|---|
With iron(III) chloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0 - 40℃; for 1.66667h; | 95% |
Stage #1: cyclohexyl chloride With [1,3-bis(3,5-di-tert-butyl-2-hydroxybenzyl)benzimidazolium][FeCl4] In diethyl ether at 0℃; for 0.0333333h; Schlenk technique; Inert atmosphere; Stage #2: 4-flourophenylmagnesium bromide In diethyl ether at 0 - 30℃; for 2h; Temperature; Schlenk technique; Inert atmosphere; | 78% |
cyclohexyl chloride
1-(4-butoxyphenyl)-1-cyclohexyl-3-[4-(2,5-dimethylphenyl)piperazin-1-yl]-2-phenylpropan-1-one
Conditions | Yield |
---|---|
Stage #1: cyclohexyl chloride With magnesium In diethyl ether Stage #2: With 1-(4-butoxyphenyl)-3-[4-(2,5-dimethylphenyl)piperazin-1-yl]-2-phenylpropan-1-one In diethyl ether for 6h; Heating; | 95% |
Conditions | Yield |
---|---|
With zinc perchlorate In neat (no solvent) at 80℃; for 3h; Ritter Amidation; | 94% |
With iron(II) chloride tetrahydrate In neat (no solvent) at 80℃; for 4h; Ritter Amidation; | 94% |
N-(2-phenylethyl)pyridine-2-carboxamide
cyclohexyl chloride
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; ethylmagnesium bromide; manganese(ll) chloride In tetrahydrofuran at 60℃; for 14h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 94% |
Conditions | Yield |
---|---|
With copper(l) iodide; C21H23ClNiP2S; caesium carbonate; sodium iodide In dimethyl sulfoxide at 50℃; for 12h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere; | 94% |
2-cyclohex-1-enyl-pyridine
cyclohexyl chloride
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; neopentylmagnesium bromide; cobalt(II) bromide; 1,3-diisopropyl-1H-benzo[d]imidazol-3-ium bromide In tetrahydrofuran at 0 - 20℃; for 6h; Catalytic behavior; Reagent/catalyst; Temperature; Schlenk technique; | 92% |
cyclohexyl chloride
N-butyl-pyridine-2-carboxylic acid amide
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; ethylmagnesium bromide; manganese(ll) chloride In tetrahydrofuran at 60℃; for 14h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 92% |
cyclohexyl chloride
1-phenyl-3-piperidino-propan-1-one; hydrochloride
trihexylphenidyl hydrochloride
Conditions | Yield |
---|---|
Stage #1: cyclohexyl chloride With iodine; magnesium In 1,2-dimethoxyethane; tert-butyl methyl ether at 45 - 55℃; for 2h; Sealed tube; Inert atmosphere; Large scale; Stage #2: 1-phenyl-3-piperidino-propan-1-one; hydrochloride In 1,2-dimethoxyethane; tert-butyl methyl ether at 5 - 10℃; for 2h; Solvent; Sealed tube; Inert atmosphere; Large scale; | 90.5% |
Stage #1: cyclohexyl chloride With magnesium In tetrahydrofuran; ethyl bromide at 45 - 65℃; for 3h; Stage #2: 1-phenyl-3-piperidino-propan-1-one; hydrochloride In tetrahydrofuran; ethyl bromide at 65℃; for 4h; Stage #3: With hydrogenchloride In tetrahydrofuran; ethyl bromide; water at 65℃; for 0.8h; Temperature; | 70.3% |
Conditions | Yield |
---|---|
With hydrogen iodide; cetyltributylphosphonium bromide at 105℃; for 7h; | 90% |
With hydrogen iodide at 105℃; for 2.5h; | 85% |
With hydrogen iodide |
cyclohexyl chloride
(-)-(2S)-trifluoromethanesulfonyloxy-propionic acid tert-butyl ester
(+)-(2S)-cyclohexyl-propionic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: cyclohexyl chloride With magnesium In tetrahydrofuran Inert atmosphere; Stage #2: (-)-(2S)-trifluoromethanesulfonyloxy-propionic acid tert-butyl ester With zinc(II) chloride In tetrahydrofuran at 0℃; for 3h; Inert atmosphere; optical yield given as %ee; enantiospecific reaction; | 90% |
Conditions | Yield |
---|---|
With aluminum (III) chloride at 0 - 20℃; for 4h; Friedel-Crafts Alkylation; | 90% |
With aluminum (III) chloride at 0 - 20℃; for 5h; | 90% |
cyclohexyl chloride
para-methylphenylmagnesium bromide
1-cyclohexyl-4-methylbenzene
Conditions | Yield |
---|---|
Stage #1: cyclohexyl chloride With [1,3-bis(3,5-di-tert-butyl-2-hydroxybenzyl)benzimidazolium][FeCl4] In diethyl ether at 0℃; for 0.0333333h; Schlenk technique; Inert atmosphere; Stage #2: para-methylphenylmagnesium bromide In diethyl ether at 0 - 30℃; for 2h; Temperature; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 89% |
With C33H49N2O2(1+)*Cl4Fe(1-) In diethyl ether Reagent/catalyst; Grignard Reaction; | 77% |
With butylmethylimidazolium tetrachloroferrate In diethyl ether at 0 - 20℃; | 75% |
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina In 2-methyltetrahydrofuran at 90℃; for 12h; Inert atmosphere; chemoselective reaction; | 89% |
carbon dioxide
cyclohexyl chloride
aniline
O-cyclohexyl N-phenylcarbamate
Conditions | Yield |
---|---|
With choline chloride * 2ZnCl2 at 20℃; under 760.051 Torr; for 2h; Green chemistry; | 89% |
Conditions | Yield |
---|---|
With oxygen; kieselguhr; copper(l) chloride In hexane for 3h; Oxidation; Heating; | 88% |
Stage #1: cyclohexyl chloride With sodium hydroxide In water at 45 - 50℃; for 2.5h; Stage #2: With quinolinium chlorochromate(VI) In water for 18h; | 37% |
With pumice stone; vanadia at 350℃; beim Leiten im Gemisch mit Luft und Wasserdampf; |
cyclohexyl chloride
Conditions | Yield |
---|---|
Stage #1: cyclohexyl chloride With naphthalene; lithium In tetrahydrofuran at -78℃; for 3h; Stage #2: (2SP,4R,5S)-(-)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxazaphospholidine borane In tetrahydrofuran at -78℃; Further stages.; | 88% |
Stage #1: cyclohexyl chloride With lithium In Petroleum ether for 5h; Heating; Stage #2: (2SP,4R,5S)-(-)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxazaphospholidine borane In tetrahydrofuran; Petroleum ether at -78 - 0℃; | 87% |
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