hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:101-41-7
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiry1. Quality Our products meet MSDS safe standard and we have ISO and other certificate so yan can get high quality products from our company. 2. Price We are the company which is the joint of trade and industry so we cao provide the competiti
Cas:101-41-7
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:101-41-7
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:101-41-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTIANFUCHEM--101-41-7--Methyl phenylacetate in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relatio
Cas:101-41-7
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryAppearance:colorless liquid Storage:Store below +30°C. Package:200kg/Drum Application:Chemicals Transportation:Express/Sea/Air Port:Any port in China
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Liquid Storage:Store in sealed containers at cool & dry plac
Cas:101-41-7
Min.Order:100 Gram
Negotiable
Type:Other
inquiryHanways chempharm is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The marketing department is located in Wuhan. We have two GMP facilities in Hubei Pr
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $200.0 / 400.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:101-41-7
Min.Order:10 Gram
FOB Price: $0.12
Type:Trading Company
inquiryProduct Name: Methyl phenylacetate CAS: 101-41-7 MF: C9H10O2 MW: 150.17 EINECS: 202-940-9 Mol File: 101-41-7.mol Methyl phenylacetate Structure Methyl phenylacetate Chemical Properties Melting point 107-115 °C Boiling poin
Cas:101-41-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:101-41-7
Min.Order:25 Kilogram
FOB Price: $135.0 / 156.0
Type:Trading Company
inquiryMethyl phenylacetate CAS:101-41-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:101-41-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful d
Cas:101-41-7
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:101-41-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Detail Minimum Order Qty. 10 Gram
Cas:101-41-7
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/A
Cas:101-41-7
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Methyl phenylacetate CAS 101-41-7 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $50.0 / 100.0
Type:Trading Company
inquiryMethyl phenylacetate CAS 101-41-7 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality contr
Cas:101-41-7
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:101-41-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:101-41-7
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Benzene methyl acetate w
1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:101-41-7
Min.Order:1 Liter
FOB Price: $4.5 / 5.0
Type:Trading Company
inquiryConditions | Yield |
---|---|
With hydrogenchloride for 1h; Heating; | 100% |
With sulfuric acid for 4h; Reflux; | 100% |
With sulfuric acid Heating; | 99% |
Conditions | Yield |
---|---|
With tert-butylamine for 21h; Heating; | 100% |
With indium; iodine for 5.5h; transesterification; Heating; | 86% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide for 5h; Ambient temperature; |
Conditions | Yield |
---|---|
With tert-butylamine; lithium bromide for 0.25h; Heating; | 100% |
With indium; iodine for 12h; transesterification; Heating; | 88% |
In acetonitrile Ambient temperature; Et4NClO4 electrolyte, glassy carbon cathode, Pt anode, -1,7 V potential; | 43% |
With PCS-DBU In water at 60℃; Rate constant; Mechanism; other quaternary ammonium resins, other temperatures, other reaction time; |
methanol
carbon monoxide
benzyl bromide
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; C52H46O2P2Pd2; triphenylphosphine at 60℃; for 2h; Conversion of starting material; | 100% |
With N-ethyl-N,N-diisopropylamine; C26H24BrOPPd; triphenylphosphine at 28 - 60℃; under 760.051 - 2587.76 Torr; for 2h; Conversion of starting material; | 99% |
With N-ethyl-N,N-diisopropylamine; C43H37BrOP2Pd; triphenylphosphine at 60℃; for 2h; Conversion of starting material; | 99% |
Methyl formate
carbon monoxide
benzyl bromide
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With potassium iodide; <1,5-HDRhCl>2 under 5171.5 Torr; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With tert-butylamine for 2h; Heating; | 100% |
(EtO)3TiO(CH2)2OTi(OEt)3 for 72h; Heating; | 91% |
scandium tris(trifluoromethanesulfonate) at 64℃; for 10h; | 91% |
With Rhizobium meliloti cyclosophoraoses at 60℃; Kinetics; Enzyme kinetics; Further Variations:; Reaction partners; reaction time; |
Conditions | Yield |
---|---|
With lithium perchlorate; methyl iodide Ambient temperature; anodic oxidation at constant current; | 100% |
With poly[4-(diacetoxyiodo)styrene]; sulfuric acid In acetonitrile at 60℃; for 0.5h; | 80% |
With lead(IV) acetate; perchloric acid at 50℃; for 2h; | 46% |
With LiCO4*H2O; methyl iodide Product distribution; Mechanism; Ambient temperature; anodic oxidation at constatnt current; |
Conditions | Yield |
---|---|
With potassium hydroxide In diethyl ether at 0℃; Inert atmosphere; | 100% |
carbonic acid dimethyl ester
1-phenyl-acetone
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With Novozym 435; acylase I from Aspergillus melleus; amano lipase AK from pseudomonas fluorescens; lipase from wheat germ; papaine In toluene at 40℃; for 48h; Mechanism; Enzymatic reaction; | 100% |
Conditions | Yield |
---|---|
With acid | 99% |
bromo-phenyl-acetic acid methyl ester
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With ammonium chloride; zinc In ethanol at 80℃; for 0.00833333h; microwave irradiation; | 99% |
With indium; acetic acid In methanol at 20℃; for 1h; | 97.6% |
With dimethyl-3-pyrenylpropyl tin hydride; 2,2'-azobis(isobutyronitrile) In benzene for 1h; Heating; | 89% |
With 2,2'-azobis(isobutyronitrile); dimethyl(3-(pyren-1-yl)propyl)stannane In benzene for 1h; Heating; | 89% |
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene 1.) 10-20 deg C, 2.) room temperature, 10 min; | 80% |
phenylacetic acid
carbonic acid dimethyl ester
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 160℃; under 15001.2 Torr; for 0.2h; microwave irradiation; | 99% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene for 6h; Heating; | 98% |
With sulfuric acid at 80 - 85℃; for 5.5h; Neat (no solvent); | 97.09% |
(2-Iodo-1,1-dimethoxy-ethyl)-benzene
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In methanol at 20℃; for 5h; | 98% |
In methanol for 4h; | 98% |
4-[(methoxycarbonyl)methyl]phenyl mesylate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With ammonium acetate; magnesium; palladium on activated charcoal In methanol at 20℃; for 12h; | 98% |
With hydrogen; diethylamine; palladium on activated charcoal In methanol at 20℃; for 4h; | 89% |
With ammonium acetate; methanol; magnesium; palladium on activated charcoal at 20℃; for 12h; | 98 % Spectr. |
Conditions | Yield |
---|---|
With sulfuric acid; acetonitrile at 80 - 85℃; for 16 - 18h; | 98% |
methanol
phenyl-acetic acid phenethyl ester
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III) at 146.84℃; for 6h; Reagent/catalyst; | 96.6% |
methanol
Benzyl-phenylacetyl-carbamic acid tert-butyl ester
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With sodium methylate at 0℃; for 0.416667h; | 96% |
methyl O-acetylmandalate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide In tetrahydrofuran at 20 - 22℃; for 0.0166667h; | 96% |
With sodium tetrahydroborate; nickel dichloride In methanol for 0.333333h; Ambient temperature; | 76% |
trimethyl orthoselenophenylacetate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With mercury dichloride; mercury(II) oxide In methanol; water for 5h; Heating; | 96% |
methanol
acetophenone
trimethyl orthoformate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With bromine; silver nitrate for 108h; other oxidants; | 96% |
methanol
1-[1-methoxy-2-phenylethenyl]-1H-1,2,3-benzotriazole
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With hydrogenchloride Heating; | 96% |
methanol
tert-butyldimethylsilyl 2-phenylethanoate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: methanol; tert-butyldimethylsilyl 2-phenylethanoate; carbon tetrabromide at 20℃; for 0.5h; Irradiation; Stage #2: at 20℃; for 2h; | 96% |
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol at 20℃; for 12h; | 96% |
Conditions | Yield |
---|---|
In methanol; water | 95.4% |
methanol
phenylacetylene
A
phenylacetic acid
B
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII) for 48h; Yields of byproduct given; | A n/a B 95% |
Conditions | Yield |
---|---|
In benzene at 20℃; for 18h; Elimination; addition; Irradiation; | A 95% B 72% |
methyl 2-(dimethyl(oxo)-λ6-sulfaneylidene)-2-phenylacetate
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With water; isopropyl alcohol for 2h; Reflux; | 95% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal at 25℃; for 4h; | 94% |
With potassium hydrogensulfate at 65℃; for 14h; | 93% |
unter Einleiten von Borfluorid und Erwaermen des Reaktionsgemisches; |
Conditions | Yield |
---|---|
With triethylamine; dmap In dichloromethane at 0℃; for 1h; | 94% |
With dmap; triethylamine 1.) CH2Cl2, 0 deg C, 5 min, 2.) 0 deg C, 1 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
In acetonitrile at 35℃; under 8000 Torr; for 72h; | 100% |
In acetonitrile at 35℃; under 6000480 Torr; for 72h; | 100% |
With 14C2H2F3O(1-)*6C4H8O*La2Na8(14+) at 80℃; for 6h; Inert atmosphere; | 99% |
chloro-trimethyl-silane
benzeneacetic acid methyl ester
(1-methoxy-2-phenylvinyloxy)trimethylsilane
Conditions | Yield |
---|---|
With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 100% |
Stage #1: benzeneacetic acid methyl ester With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2.1h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran at 20℃; Inert atmosphere; | 100% |
Stage #1: benzeneacetic acid methyl ester With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at 20℃; | 91% |
Conditions | Yield |
---|---|
In acetonitrile at 35℃; under 6000480 Torr; for 72h; | 100% |
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Reagent/catalyst; Green chemistry; | 99% |
With magnesium chloride In tetrahydrofuran at 20℃; for 16h; | 98% |
With potassium tert-butylate at 219℃; for 0.05h; microwave irradiation; | 63% |
With bis(bis(trimethylsilyl)amido)tin(II) 1) hexane, r.t., 10 min; Yield given. Multistep reaction; |
piperidine
benzeneacetic acid methyl ester
2-phenyl-1-(1-piperidinyl)ethanone
Conditions | Yield |
---|---|
In acetonitrile at 35℃; under 6000480 Torr; for 72h; | 100% |
In acetonitrile at 45℃; under 6000480 Torr; for 72h; | 100% |
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 99% |
2-iodo-propane
benzeneacetic acid methyl ester
2-phenyl-3-methylbutyric acid methyl ester
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -78℃; | 100% |
With 2-pyrrolidinon In N,N-dimethyl-formamide Flow reactor; | 16% |
With 1) EGB.2 1) -78 deg C, 2) -78 deg C, 15 min; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With tert-butylamine; lithium bromide for 6h; Heating; | 100% |
With tetrachlorosilane for 8h; Heating; | 91% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide for 1h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With bis(tri-n-butyltin)oxide In toluene for 0.333333h; Product distribution; Irradiation; var. carboxylic ester, organotin oxide and hydroxide, solvent, time of temp. or microwave irrad.; | 100% |
With bis(tri-n-butyltin)oxide In neat (no solvent) at 200℃; for 0.5h; | 100% |
With aluminium trichloride; dodecyl methyl sulfide at 0 - 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; silica gel In hexane for 3h; Heating; | 100% |
With methanol; sodium tetrahydroborate In diethyl ether at 20℃; for 38h; Reduction; | 96% |
With sodium tetrahydroborate In diethylene glycol dimethyl ether at 104℃; | 95% |
benzeneacetic acid methyl ester
cyanomethyl bromide
β-(carbomethoxy)-β-phenylpropionitrile
Conditions | Yield |
---|---|
Stage #1: benzeneacetic acid methyl ester With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Inert atmosphere; Stage #2: cyanomethyl bromide In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; | 100% |
Stage #1: benzeneacetic acid methyl ester With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: cyanomethyl bromide In tetrahydrofuran at -78 - 20℃; | 77% |
Stage #1: benzeneacetic acid methyl ester With lithium diisopropyl amide In tetrahydrofuran; ethylbenzene; toluene at -78℃; for 1h; Inert atmosphere; Stage #2: cyanomethyl bromide In tetrahydrofuran; ethylbenzene; toluene at -78℃; Inert atmosphere; | 69% |
ethanolamine
benzeneacetic acid methyl ester
N-(2-hydroxyethyl)-2-phenylacetamide
Conditions | Yield |
---|---|
With N,N'-Mes2imidazol-2-ylidene In tetrahydrofuran at 23℃; for 8h; | 100% |
With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine In acetonitrile at 20℃; for 15h; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 99% |
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 99% |
cyclopentylmethyl Iodide
benzeneacetic acid methyl ester
3-cyclopentyl-2-phenylpropionic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: benzeneacetic acid methyl ester With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.75h; Inert atmosphere; Stage #2: cyclopentylmethyl Iodide In tetrahydrofuran at -78 - 25℃; Inert atmosphere; | 100% |
2,2'-iminobis[ethanol]
benzeneacetic acid methyl ester
N,N-bis(2-hydroxyethyl)-2-phenylacetamide
Conditions | Yield |
---|---|
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 99% |
at 100 - 150℃; |
1-amino-2-propene
benzeneacetic acid methyl ester
N-Allyl-2-phenylethanamide
Conditions | Yield |
---|---|
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 99% |
isopropyl alcohol
benzeneacetic acid methyl ester
isopropyl phenylacetate
Conditions | Yield |
---|---|
With tert-butylamine; lithium bromide for 33h; Heating; | 99% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide for 4h; Ambient temperature; | 94% |
With indium; iodine for 6h; transesterification; Heating; | 90% |
Conditions | Yield |
---|---|
With C16H25N3O2S In n-heptane for 48h; Reflux; Molecular sieve; Inert atmosphere; | 99% |
With 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; 4-pyrrolidin-1-ylpyridine In octane for 6h; Reflux; | 98% |
With SO3H and NH2+ functional carbon-based solid acid at 80℃; for 6h; | 92% |
Conditions | Yield |
---|---|
With diisopropylamine; lithium diisopropyl amide In tetrahydrofuran; hexane -78 deg C, 1 h; -78 deg C to room temp., 35 min; | 99% |
dimethyl amine
benzeneacetic acid methyl ester
N,N-dimethyl-2-phenylacetamide
Conditions | Yield |
---|---|
With magnesium chloride In tetrahydrofuran at 20℃; for 24h; | 99% |
Conditions | Yield |
---|---|
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 99% |
With potassium tert-butylate at 105℃; for 0.05h; microwave irradiation; | 97% |
With trimethylaluminum In tetrahydrofuran; toluene at 125℃; for 0.0333333h; | 84% |
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