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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
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inquiryAppearance:Colorless to sltly yellow liquid Storage:room temperature Package:200kg/Drum Application:2-Phenylethyl 2-Phenylacetate is an antimicrobial spray applied freshening compounds for fabric. Transportation:Express/Sea/Air Port:Any port in Ch
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inquiryPhenethyl phenylacetate CAS:102-20-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryName phenethyl phenyl acetate Synonyms 2-phenylethyl 2-phenylacetate CAS Registry Number 102-20-5 EINECS 203-013-1 Appearance:Colorl
Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Conditions | Yield |
---|---|
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | A 4% B 99% |
With pyridine; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 25℃; for 3h; | A 58.7% B 41.3% |
With oxygen at 120℃; for 5h; Neat (no solvent); | |
With pyridine; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 22℃; for 3h; Catalytic behavior; Time; | A 71 %Chromat. B 23 %Chromat. |
With 2,6-dimethylpyridine; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 22℃; for 3h; Catalytic behavior; Time; | A 12 %Chromat. B 86 %Chromat. |
Conditions | Yield |
---|---|
With potassium hydroxide | 98.6% |
With C10H10Zr(2+)*2CF3O3S(1-)*C4H8O at 80℃; for 24h; Sealed tube; | 95% |
With silica gel-immobilized perchloric acid at 80℃; for 6h; Fischer esterification; Inert atmosphere; Neat (no solvent); | 94% |
Conditions | Yield |
---|---|
With periodic acid; pyridinium chlorochromate In acetonitrile at 0 - 20℃; for 2h; | 94% |
With sodium bromite In water; acetic acid for 10h; Ambient temperature; | 91% |
With peracetic acid; sodium bromide In ethyl acetate at 39.9℃; for 2h; | 86% |
2-phenylethanol
tert-butylamine
A
phenyl-acetic acid phenethyl ester
B
2-methyl-N-phenethylpropan-2-amine
Conditions | Yield |
---|---|
With 3 A molecular sieve; potassium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; [Ru(p-cumene)Cl2]2 In toluene at 110℃; for 24h; Product distribution; Further Variations:; Catalysts; | A 7% B 88% |
With 3 A molecular sieve; potassium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; [Ru(p-cumene)Cl2]2 In toluene at 110℃; for 24h; | A 61% B n/a |
Conditions | Yield |
---|---|
With Rh(PhBP3)(H)2(NCMe); hydrogen In toluene at 20℃; under 760.051 Torr; for 0.166667h; Tishchenko reaction; | 85% |
2-phenylethanol
phenylacetylene
A
phenylacetic acid
B
phenyl-acetic acid phenethyl ester
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII) for 48h; | A 50% B 47% |
Conditions | Yield |
---|---|
With [RuCl2(p-cymene)(iPr2-imy)]; potassium hydroxide; tricyclohexylphosphine In 1,3,5-trimethyl-benzene at 163℃; for 18h; Inert atmosphere; | A 48% B 7% |
2-phenylethanol
di-n-propylamine
A
phenyl-acetic acid phenethyl ester
B
2-phenyl-N,N-dipropylacetamide
Conditions | Yield |
---|---|
With C15H22Cl2N2Ru; potassium tert-butylate In toluene for 24h; Inert atmosphere; Reflux; | A 21% B 44% |
2-phenylethanol
dibenzylamine
A
phenyl-acetic acid phenethyl ester
B
N,N-dibenzyl-2-phenylacetamide
Conditions | Yield |
---|---|
With C15H22Cl2N2Ru; potassium tert-butylate In toluene for 24h; Inert atmosphere; Reflux; | A 19% B 40% |
Conditions | Yield |
---|---|
With rhenium-catalyst at 149℃; under 117681 Torr; Hydrogenation; | |
With tin(II) trifluoromethanesulfonate; tris(2,4-pentanedionato)ruthenium(III); hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In water; toluene at 160℃; under 45004.5 Torr; for 48h; Reagent/catalyst; Autoclave; | A 49 %Chromat. B 20 %Chromat. |
Conditions | Yield |
---|---|
With sulfuric acid bei der elektrolytischen Reduktion an einer Bleikathode; | |
With tin(II) trifluoromethanesulfonate; tris(2,4-pentanedionato)ruthenium(III); hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In toluene at 160℃; under 45004.5 Torr; for 48h; Reagent/catalyst; Autoclave; | 26 %Chromat. |
Conditions | Yield |
---|---|
With triphenylstannane |
Ethyl 2-phenylethanoate
A
Phenylessigsaeurehexylester
B
phenyl-acetic acid phenethyl ester
C
phenylacetic acid octyl ester
Conditions | Yield |
---|---|
Product distribution; competition reaction with n-hexanol, n-octanol and phenylethanol; selectivity of catalysis with SiO2, also mod. with Ph-CH<(EtO)3SiO>-P(O)(OEt)(OHex) or H2SO4; |
diethyl ether
phenylacetyl chloride
benzene
A
phenyl-acetic acid phenethyl ester
Conditions | Yield |
---|---|
at 70℃; bei der Elektrolyse an einer Bleikathode.Diazotization; |
Conditions | Yield |
---|---|
at 150℃; under 117681 Torr; Hydrogenation; |
2-phenylethanol
sulfuric acid
A
phenyl-acetic acid phenethyl ester
B
benzaldehyde
C
acetic acid
D
benzoic acid
2-phenylethanol
benzyl alcohol
A
benzyl 2-phenylacetate
B
benzoic acid benzyl ester
C
2-Phenylethyl benzoate
D
phenyl-acetic acid phenethyl ester
Conditions | Yield |
---|---|
With magnesium nitride; [RuCl2(p-cymene)(iPr2-imy)]; potassium tert-butylate; tricyclohexylphosphine tetrafluoroborate In toluene at 110℃; for 24h; Schlenk technique; Inert atmosphere; |
1-Phenylethanol
2-phenylethanol
A
phenyl-acetic acid phenethyl ester
B
acetophenone
Conditions | Yield |
---|---|
With magnesium nitride; [RuCl2(p-cymene)(iPr2-imy)]; potassium tert-butylate; tricyclohexylphosphine tetrafluoroborate In toluene at 110℃; for 24h; Schlenk technique; Inert atmosphere; |
phenylacetic acid
1,1-diphenylethanol
2-phenylethanol
4-nitrobenzaldehdye
4-methoxy-benzaldehyde
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
A
1,1-Diphenylethylene
B
4-methoxy-N-(4-nitrobenzylidene)aniline
C
p-methoxybenzaldehyde neopentyl glycol acetal
D
phenyl-acetic acid phenethyl ester
E
N-(4-methoxy benzylidene)-4-methoxyaniline
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 75 %Spectr. C 72 %Spectr. D 59 %Spectr. E 5 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2-phenylethanol
4-chlorobenzaldehyde
4-nitrobenzaldehdye
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
A
1,1-Diphenylethylene
B
4-methoxy-N-(4-nitrobenzylidene)aniline
C
2-(4-chlorophenyl)-5,5-dimethyl-1,3-dioxane
D
5,5-dimethyl-2-(4-nitro-phenyl)-[1,3]dioxane
E
N-(4-chlorobenzylidene)-4-methoxyaniline
F
phenyl-acetic acid phenethyl ester
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 52 %Spectr. C 52 %Spectr. D 48 %Spectr. E 43 %Spectr. F 99 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
4-chloro-aniline
2,2-Dimethyl-1,3-propanediol
2,4-Dimethoxybenzaldehyde
A
1,1-Diphenylethylene
B
phenyl-acetic acid phenethyl ester
C
2-(2,4-dimethoxyphenyl)-5,5-dimethyl-1,3-dioxane
D
4-chloro-N-(2,4-dinitrobenzylidene)aniline
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 99 %Spectr. C 74 %Spectr. D 83 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
phenylboronic acid
A
1,1-Diphenylethylene
B
N-(2,4-dinitrobenzylidene)-4-methoxyaniline
C
phenyl-acetic acid phenethyl ester
D
5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 98 %Spectr. B 93 %Spectr. C 99 %Spectr. D 99 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
pentafluorophenylboronic acid
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
A
1,1-Diphenylethylene
B
N-(2,4-dinitrobenzylidene)-4-methoxyaniline
C
phenyl-acetic acid phenethyl ester
D
(2,3,4,5,6-pentafluorophenyl)-5,5-dimethyl-1,3,2-dioxaborinane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 97 %Spectr. C 99 %Spectr. D 74 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
2,4-Dimethoxybenzaldehyde
A
1,1-Diphenylethylene
B
N-(2,4-dinitrobenzylidene)-4-methoxyaniline
C
phenyl-acetic acid phenethyl ester
D
2-(2,4-dimethoxyphenyl)-5,5-dimethyl-1,3-dioxane
E
N-(2,4-dimethoxybenzylidene)-4-methoxyaniline
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 84 %Spectr. C 96 %Spectr. D 77 %Spectr. E 9 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
2,2-Dimethyl-1,3-propanediol
aniline
2,4-Dimethoxybenzaldehyde
A
1,1-Diphenylethylene
B
phenyl-acetic acid phenethyl ester
C
2-(2,4-dimethoxyphenyl)-5,5-dimethyl-1,3-dioxane
D
1-(2,4-dinitrophenyl)-N-phenylmethanimine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 98 %Spectr. C 80 %Spectr. D 86 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
cyclohexylamine
2,2-Dimethyl-1,3-propanediol
2,4-Dimethoxybenzaldehyde
A
1,1-Diphenylethylene
B
phenyl-acetic acid phenethyl ester
C
2-(2,4-dimethoxyphenyl)-5,5-dimethyl-1,3-dioxane
D
N-(2,4-dinitrobenzylidene)cyclohexanamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 43 %Spectr. C 95 %Spectr. D 72 %Spectr. |
phenylacetic acid
1,1-diphenylethanol
2,4-dinitrobenzaldehyde
2-phenylethanol
benzaldehyde
4-methoxy-aniline
2,2-Dimethyl-1,3-propanediol
A
1,1-Diphenylethylene
B
5,5-dimethyl-2-phenyl-[1,3]dioxane
C
N-(2,4-dinitrobenzylidene)-4-methoxyaniline
D
phenyl-acetic acid phenethyl ester
E
[4-(benzylideneamino)phenyl]methanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 48h; Inert atmosphere; Reflux; Dean-Stark; | A 99 %Spectr. B 79 %Spectr. C 92 %Spectr. D 98 %Spectr. E 5 %Spectr. |
methanol
phenyl-acetic acid phenethyl ester
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III) at 146.84℃; for 6h; Reagent/catalyst; | 96.6% |
Conditions | Yield |
---|---|
With triiron dodecarbonyl; 1,1,3,3-Tetramethyldisiloxane In toluene at 100℃; for 2h; Inert atmosphere; Schlenk technique; | 85% |
phenyl-acetic acid phenethyl ester
allyl bromide
phenethyl 2-phenylpent-4-enoate
Conditions | Yield |
---|---|
With caesium hydroxide monohydrate; 2,7-bis[O(9)-allylhydrocinchonidinium-N-methyl]naphthalene dibromide In dichloromethane at -40℃; for 23h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 77% |
phenyl-acetic acid phenethyl ester
2-phenylethyl 2-oxo-2-phenylacetate
Conditions | Yield |
---|---|
Stage #1: phenyl-acetic acid phenethyl ester With tert.-butylhydroperoxide; copper(II) oxide In water at 110℃; for 4.5h; Stage #2: With pyridine In water at 50℃; for 4h; | 61% |
phenyl-acetic acid phenethyl ester
styrene
Conditions | Yield |
---|---|
at 315 - 320℃; |
Conditions | Yield |
---|---|
at 315 - 320℃; |
phenyl-acetic acid phenethyl ester
benzylmagnesium chloride
tribenzylcarbinol
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 315 - 320 °C 2: peroxybenzoic acid; chloroform / 0 °C View Scheme |
phenyl-acetic acid phenethyl ester
2-phenyl-acrylic Acid Phenethyl Ester
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium carbonate; paraformaldehyde In diethyl ether; toluene | 1.48 g (60%) |
phenyl-acetic acid phenethyl ester
allyl bromide
(+/-)-phenethyl 2-phenylpent-4-enoate
Conditions | Yield |
---|---|
With caesium hydroxide monohydrate; tetrabutylammomium bromide In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: phenyl-acetic acid phenethyl ester With iron (II) stearate; ethylenediamine In toluene at 20℃; for 0.0833333h; Inert atmosphere; Schlenk technique; Stage #2: In toluene at 100℃; for 20h; Inert atmosphere; Schlenk technique; | 84 %Chromat. |
Stage #1: phenyl-acetic acid phenethyl ester With C33H58FeN3PSi2; phenylsilane In toluene at 20℃; for 4h; Inert atmosphere; Glovebox; Green chemistry; Stage #2: With sodium hydroxide In toluene for 1h; Green chemistry; |
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