Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:122-78-1
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:White or
Cas:122-78-1
Min.Order:1 Gram
Negotiable
Type:Manufacturers
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:122-78-1
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:122-78-1
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryProduct Name: Phenylacetaldehyde Synonyms: 2-PHENYLACETALDEHYDE;ALPHA-TOLUALDEHYDE;ALPHA-TOLUIC ALDEHYDE;FEMA 2874;α-Toluic aldehyde;PHENYLACETALDEHYDE;PHENYL ACETIC ALDEHYDE;Phenylaceta
Cas:122-78-1
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Other
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:122-78-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: Phenylacetaldehyde CAS: 122-78-1 MF: C8H8O MW: 120.15 EINECS: 204-574-5 Mol File: 122-78-1.mol Phenylacetaldehyde Structure Phenylacetaldehyde Chemical Properties Melting point −10 °C(lit.) Boiling poin
Phenylacetaldehyde CAS:122-78-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:122-78-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:122-78-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:122-78-1
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiryProduct Name: Phenylacetaldehyde Synonyms: 2-PHENYLACETALDEHYDE;ALPHA-TOLUALDEHYDE;ALPHA-TOLUIC ALDEHYDE;FEMA 2874;α-Toluic aldehyde;PHENYLACETALDEHYDE;PHENYL ACETIC ALDEHYDE;Phenylacetaldehyde solution CAS: 122-78-1 MF: C8H8O MW: 12
Cas:122-78-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:122-78-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:122-78-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $200.0
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:122-78-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:122-78-1
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:122-78-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:122-78-1
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Superior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used for active pha
Conditions | Yield |
---|---|
With trimethylaluminum; bis(3,5-di-t-butyl-2-hydroxyphenyl)sulfone; 1-phenylpropylene oxide In hexane; dichloromethane at -80℃; for 1h; Rearrangement; | 100% |
100% | |
With Cr-pillared montmorillonite In tetrahydrofuran for 0.25h; Solvent; Reagent/catalyst; Temperature; Time; Reflux; | 100% |
trimethyl(phenethyloxy)silane
phenylacetaldehyde
Conditions | Yield |
---|---|
With nitrogen dioxide at 20℃; for 0.166667h; | 100% |
With NTPPPODS In acetonitrile for 0.5h; Reflux; | 92% |
With phosphomolybdic acid In toluene for 0.833333h; Heating; | 90% |
N,N-dimethyl-2-[2-(phenyl)ethenyloxy]ethanamine
phenylacetaldehyde
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 1h; | 100% |
Conditions | Yield |
---|---|
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In water at 30℃; for 15h; | 100% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In water; acetonitrile | 95% |
With water at 120℃; for 0.5h; microwave irradiation; | 95% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water at 75℃; for 6h; | 100% |
With sodium periodate; C31H29Br2N3Ru*CH2Cl2 In water; ethyl acetate; acetonitrile at 25℃; for 0.5h; Inert atmosphere; Schlenk technique; | 96% |
Stage #1: allylbenzene With sodium periodate; C22H23N7Ru(2+)*F6P(1-)*CF3O3S(1-) In water; acetone at 20℃; for 2h; Stage #2: With sodium sulfite In dichloromethane; water for 0.166667h; Catalytic behavior; Reagent/catalyst; | 65% |
Conditions | Yield |
---|---|
In benzene | 100% |
In benzene | 100% |
In benzene |
Conditions | Yield |
---|---|
In benzene | 100% |
5'-benzylspiro[adamantane-2,3'-[1,2,4]trioxolane]
phenylacetaldehyde
Conditions | Yield |
---|---|
With iron(II) bromide In dichloromethane; acetonitrile at 35℃; for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
With C16H17MoN3O6S; dihydrogen peroxide; sodium hydrogencarbonate In water; acetonitrile at 60℃; for 4h; Catalytic behavior; Overall yield = 94.0 %; | A 99.1% B 0.9% |
With 4C17H18ClMoN3O5S2*2C2H6OS; dihydrogen peroxide; sodium hydrogencarbonate In water; acetonitrile at 60℃; for 4h; Catalytic behavior; Overall yield = 92.0 %; | A 99.2% B 0.8% |
With C20H18ClMoN3O4S2; dihydrogen peroxide; sodium hydrogencarbonate In water; acetonitrile at 60℃; for 4h; Catalytic behavior; Overall yield = 93.0 %; | A 99.4% B 0.6% |
Conditions | Yield |
---|---|
With titanium(IV) oxide; oxygen at 29.84℃; under 760.051 Torr; for 24h; Sealed tube; Irradiation; | 99% |
With oxygen; isobutyraldehyde In 1,2-dichloro-ethane at 40℃; for 5.5h; | 98% |
With oxygen In water at 25℃; under 760.051 Torr; for 1.5h; | 98% |
Conditions | Yield |
---|---|
With Halomonas elongata/Co imm pyridoxal phosphate In toluene at 37℃; for 0.25h; pH=7.5; Flow reactor; Enzymatic reaction; | 99% |
With immobilised amine transaminase from the moderate halophilic bacterium Halomonas elongata; sodium pyruvate In aq. phosphate buffer; dimethyl sulfoxide at 37℃; under 760.051 Torr; for 2h; pH=8; | 97% |
With oxygen; copper(I) bromide In chlorobenzene at 20℃; for 3h; | 93% |
styrene
phenylacetaldehyde
Conditions | Yield |
---|---|
With 2,6-dichloropyridine N-oxide; [Ru(2,6-Cl2tpp)Cl2] In chloroform at 60℃; for 12h; Product distribution / selectivity; | 99% |
With 2,6-dichloropyridine N-oxide; [Ru(2,6-Cl2tpp)Cl2] In chloroform-d1 at 60℃; for 12h; Product distribution / selectivity; | 99% |
Stage #1: styrene With ammonium iodide; water; sodium dodecyl-sulfate for 0.5h; Stage #2: With Oxone at 20℃; for 0.13h; Reagent/catalyst; regioselective reaction; | 93% |
Conditions | Yield |
---|---|
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | A 4% B 99% |
With pyridine; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 25℃; for 3h; | A 58.7% B 41.3% |
With oxygen at 120℃; for 5h; Neat (no solvent); | |
With pyridine; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 22℃; for 3h; Catalytic behavior; Time; | A 71 %Chromat. B 23 %Chromat. |
With 2,6-dimethylpyridine; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; iodine; sodium hydrogencarbonate In dichloromethane; water at 20 - 22℃; for 3h; Catalytic behavior; Time; | A 12 %Chromat. B 86 %Chromat. |
2-benzyl-1,3-dithiane
phenylacetaldehyde
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 1h; Micellar solution; | 98% |
With ammonium iodide; dihydrogen peroxide; sodium dodecyl-sulfate In water at 20℃; for 0.333333h; micellar medium; | 95% |
styrene oxide
acetone
A
2,2-dimethyl-4-phenyl-1,3-dioxolane
B
phenylacetaldehyde
Conditions | Yield |
---|---|
With Cr-pillared montmorillonite at 30℃; for 0.333333h; Time; | A 98% B 9% |
2-phenylethyl nitrite
phenylacetaldehyde
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In diethyl ether for 4h; Ambient temperature; | 97% |
phenylacetaldehyde
Conditions | Yield |
---|---|
With sulfuric acid In tetrahydrofuran for 10h; Heating; | 96% |
(2-phenylethane-1,1-diyl)bis(phenylsulfane)
phenylacetaldehyde
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 20 - 25℃; for 2h; Irradiation; | 95% |
Conditions | Yield |
---|---|
With 3-carboxypyridinium dichromate In acetonitrile at 20℃; for 0.166667h; | A 95% B n/a |
1,4-diphenylbut-2-ene
phenylacetaldehyde
Conditions | Yield |
---|---|
Stage #1: 1,4-diphenylbut-2-ene With oxygen at -20℃; for 2h; Green chemistry; Stage #2: With Lindlar's catalyst; hydrogen at 15℃; for 2h; Temperature; Reagent/catalyst; Green chemistry; | 94.4% |
2-iodo-1-phenylethan-1-ol
phenylacetaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-iodo-1-phenylethan-1-ol With ammonium iodide; water; sodium dodecyl-sulfate for 0.5h; Stage #2: With Oxone at 20℃; for 0.1h; regioselective reaction; | 94% |
With silver nitrate |
N-styrylmorpholine
phenylacetaldehyde
Conditions | Yield |
---|---|
With aq. acid for 1h; Ambient temperature; | 94% |
(E)-N-(2-phenylethenyl)morpholine
phenylacetaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 5h; Ambient temperature; | 94% |
With water In dimethylsulfoxide-d6 at 25℃; Equilibrium constant; Solvent; | |
Multi-step reaction with 2 steps 1: bismuth(lll) trifluoromethanesulfonate / chloroform-d1; [D3]acetonitrile / 22 °C 2: water / dimethylsulfoxide-d6 / 25 °C View Scheme | |
Multi-step reaction with 2 steps 1: bismuth(lll) trifluoromethanesulfonate / chloroform-d1; [D3]acetonitrile 2: water / chloroform-d1 / 25 °C View Scheme |
Conditions | Yield |
---|---|
With 6-(2,4,6-triphenyl-phenyl)-2-diphenylphosphino-pyridine; water; (η5-cyclopentadienyl) (η6-naphthalene)ruthenium hexafluorophosphate In acetone at 55℃; for 3h; | 94% |
With chloro(cyclopentadienyl)[bis(diphenylphosphino)methane]ruthenium; water In isopropyl alcohol at 100℃; for 12h; | 90% |
With 5,5′-bis(trifluoromethyl)-2,2′-bipyridine; lithium chloride In 1-methyl-pyrrolidin-2-one; water at 25℃; for 48h; Reagent/catalyst; Inert atmosphere; Autoclave; | 84% |
Conditions | Yield |
---|---|
With dimanganese decacarbonyl In toluene at 120℃; for 8h; Sealed tube; | 94% |
Conditions | Yield |
---|---|
With 1H-imidazole; dihydrogen peroxide; Mn(TDCPP)Cl In dichloromethane; acetonitrile for 2h; Ambient temperature; | A 93% B 1% C 1% |
With 1H-imidazole; dihydrogen peroxide In dichloromethane; acetonitrile at 20℃; | A 93% B 1% C 1% |
With 1H-imidazole; dihydrogen peroxide; Mn(TDCPP)(Cl) In dichloromethane; acetonitrile at 20℃; Product distribution; other catalysts; | A 93% B 1% C 1% |
{PPN}{HCr(CO)5}
phenylacetyl chloride
A
bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}
B
phenylacetaldehyde
Conditions | Yield |
---|---|
In tetrahydrofuran 1:1 molar ratio, THF, 25°C;; detected by NMR and IR spectra; and GC analysis,; | A n/a B 92% |
Conditions | Yield |
---|---|
With zinc dichromate trihydrate at 20℃; grinding; neat (no solvent); chemoselective reaction; | 92% |
Conditions | Yield |
---|---|
With sodium dodecyl-sulfate; [Ru(η5-C9H7)Cl(PPh3)2] In water at 60℃; for 24h; | A 91% B 7 % Chromat. |
[Ru(η5-C9H7)Cl(PPh3)2] In water; isopropyl alcohol at 90℃; for 48h; | A 69% B 17 % Chromat. |
With sodium hydroxide; lithium borohydride; dihydrogen peroxide; ethyl acetate Product distribution; different ratios; | A 22 % Chromat. B 78 % Chromat. |
phenylacetaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran at 20℃; for 2h; | 91% |
With hydrogenchloride In tetrahydrofuran; water at 30℃; for 4h; | 84 %Spectr. |
phenylacetaldehyde
α-bromophenylacetaldehyde
Conditions | Yield |
---|---|
With bromine In 1,4-dioxane at 0 - 20℃; for 0.583333h; | 100% |
With bromine In dichloromethane at -10 - 20℃; Heating / reflux; | 98.7% |
Stage #1: phenylacetaldehyde With polystyrene-supported 4-(phenylseleno)morpholine In dichloromethane for 5h; Heating; Stage #2: With bromine In dichloromethane at 0℃; for 1h; Stage #3: In dichloromethane for 1h; Heating; | 85% |
3-Phenylpropan-1-amine
phenylacetaldehyde
N-(2-phenylethyl)-3-phenylpropylamine
Conditions | Yield |
---|---|
Stage #1: 3-Phenylpropan-1-amine; phenylacetaldehyde In methanol at 64℃; for 3h; Borch Reduction; Stage #2: With sodium cyanoborohydride In methanol; ethanol at 20 - 64℃; for 5h; Borch Reduction; | 100% |
With sodium cyanoborohydride In methanol for 24h; Ambient temperature; |
phenylacetaldehyde
2-hydroxy-2-methylpropanenitrile
phenyl acetaldehyde cyanohydrin
Conditions | Yield |
---|---|
With potassium carbonate In ethanol for 2h; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride at 100℃; for 0.25h; Condensation; microwave irradiation; | 100% |
With hydroxylamine hydrochloride In 1-methyl-pyrrolidin-2-one at 100℃; for 0.0833333h; | 100% |
With bismuth(lll) trifluoromethanesulfonate; acetylhydroxamic acid In acetonitrile for 16h; Reflux; | 95% |
phenylacetaldehyde
5-[(trimethylsilyl)methyl]-5,6-heptadiene-3-ol
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In diethyl ether at -78℃; for 3.5h; | 100% |
Conditions | Yield |
---|---|
100% |
phenylacetaldehyde
methyl 2-cyanoacetate
2-amino-5-phenylthiophene-3-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With sulfur; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 18 - 25℃; | 100% |
With sulfur; triethylamine In N,N-dimethyl-formamide at 20℃; for 21h; | 90% |
With sulfur; triethylamine In ethanol at 20℃; for 1h; Gewald reaction; Reflux; | 63% |
phenylacetaldehyde
4-hydrazinopyridine hydrochloride
N-[2-phenyl-eth-(Z)-ylidene]-N'-pyridin-4-yl-hydrazine
Conditions | Yield |
---|---|
Stage #1: phenylacetaldehyde; 4-hydrazinopyridine hydrochloride Stage #2: With sodium hydroxide In water | 100% |
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; | 100% |
phenylacetaldehyde
4-(1-phenethyl-piperidin-4-yl)-butyric acid methyl ester
Conditions | Yield |
---|---|
Stage #1: methyl 4-(piperidin-4-yl)butanoate hydrochloride; phenylacetaldehyde With sodium tris(acetoxy)borohydride In tetrahydrofuran at 20℃; for 4h; Stage #2: With water; sodium hydrogencarbonate In tetrahydrofuran; ethyl acetate | 100% |
Stage #1: methyl 4-(piperidin-4-yl)butanoate hydrochloride; phenylacetaldehyde With sodium tris(acetoxy)borohydride In tetrahydrofuran at 20℃; for 4h; Stage #2: With sodium hydrogencarbonate In tetrahydrofuran; water; ethyl acetate | 100% |
phenylacetaldehyde
N-Benzylethanolamine
2-[benzyl(phenethyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 14h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: Methoxyallene With n-butyllithium In diethyl ether; hexane at -40℃; for 0.5h; Inert atmosphere; Stage #2: phenylacetaldehyde In diethyl ether; hexane at -78℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
at 20℃; neat (no solvent); | 100% |
ethyl 2-(triphenylphosphoranylidene)butanoate
phenylacetaldehyde
Conditions | Yield |
---|---|
In toluene for 10h; Wittig olefination; Reflux; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: phenylacetaldehyde; 3-aminopentane In methanol at 64℃; for 3h; Borch Reduction; Stage #2: With sodium cyanoborohydride In methanol; ethanol at 20 - 64℃; for 5h; Borch Reduction; | 100% |
Conditions | Yield |
---|---|
Stage #1: phenylacetaldehyde; cyclohexylamine In methanol at 64℃; for 3h; Borch Reduction; Stage #2: With sodium cyanoborohydride In methanol; ethanol at 20 - 64℃; for 5h; Borch Reduction; | 100% |
phenylacetaldehyde
sodium cyanoborohydride
isopentyl-phenethyl-amine
Conditions | Yield |
---|---|
Stage #1: phenylacetaldehyde; sodium cyanoborohydride In methanol at 64℃; for 3h; Borch Reduction; Stage #2: With sodium cyanoborohydride In methanol; ethanol at 20 - 64℃; for 5h; Borch Reduction; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 20℃; Inert atmosphere; Schlenk technique; |
1,3-dioxolan-2-ylethylmagnesium bromide
phenylacetaldehyde
C13H18O3
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; Grignard Reaction; | 100% |
(R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether
phenylacetaldehyde
Conditions | Yield |
---|---|
In benzene-d6 at 25℃; for 48h; Inert atmosphere; Schlenk technique; Molecular sieve; | 100% |
Conditions | Yield |
---|---|
In ethanol at 20℃; | 100% |
Conditions | Yield |
---|---|
In dimethylsulfoxide-d6 at 20℃; for 1h; Molecular sieve; Inert atmosphere; | 100% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View