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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
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inquiryProduct informations Product Name 2-(Benzylamino)ethanol CAS No. 104-63-2
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N-Benzylethanolamine Basic information Product Name: N-Benzylethanolamine Synonyms: (N-Benzylamino)ethanol;2-(Phenylmethyl)amino-ethanol;N-Benzyl-2-aminoethanol;N-Benzyl-2-hydroxyethylamine;N-Benzyl-N-(2-hydroxyethyl)amine;N-Benzylethanolamine
Cas:104-63-2
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inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; ethanolamine In methanol at 20℃; for 0.25h; Stage #2: With methanol; sodium tetrahydroborate at 0 - 20℃; | 100% |
With copper chromium spinel oxide; hydrogen; barium(II) oxide at 130℃; under 37503 Torr; for 1h; | 97.8% |
Stage #1: benzaldehyde; ethanolamine With magnesium sulfate In methanol at 20℃; for 18h; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; for 1h; | 95% |
[benzyl-(2-hydroxyethyl)-amino]-acetonitrile
N-Benzylethanolamine
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In ethanol | 98% |
N-Benzylethanolamine
Conditions | Yield |
---|---|
With methanol; 1,3-disulfonic acid imidazolium hydrogen sulfate at 20℃; for 0.0666667h; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With diborane In tetrahydrofuran for 5h; Heating; | 96% |
With lithium aluminium tetrahydride In diethyl ether |
Conditions | Yield |
---|---|
With sodium cyanoborohydride In methanol at 20℃; for 12h; Inert atmosphere; Cooling with ice; | 94% |
With hydrogen; palladium on activated charcoal Yield given; | |
With sodium tetrahydroborate In methanol at 5 - 20℃; |
Conditions | Yield |
---|---|
With Dowex 1*8-100 resin (hydroxide form) In tetrahydrofuran; methanol at 20℃; for 18h; | 94% |
2-oxo-3-phenylmethyl-1,2,3-oxathiazolidine
N-Benzylethanolamine
Conditions | Yield |
---|---|
With thiophenol In methanol at 20℃; for 0.5h; | 84% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 1h; Heating; | 80% |
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 20℃; for 1h; | 80% |
C9H11NO
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 0℃; for 3h; Inert atmosphere; Reflux; | 79% |
N-benzyl-2-(benzyloxy)ethan-1-amine
N-Benzylethanolamine
Conditions | Yield |
---|---|
With triphenylphosphine hydrobromide In acetonitrile at 100℃; for 0.5h; Microwave irradiation; sealed tube; | 72% |
Conditions | Yield |
---|---|
With 1-(3-amino-2,4-dihydroxyphenyl)-1-ethanone In methanol at 20℃; for 4h; Inert atmosphere; Electrochemical reaction; chemoselective reaction; | 68% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; iodine In tetrahydrofuran Heating; | 64% |
With lithium aluminium tetrahydride |
(E)-2-(benzylideneamino)ethanol
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 0 - 20℃; for 21h; | 61.3% |
With sodium tetrahydroborate In ethanol at 0 - 20℃; |
N-benzyl-β-vinyloxyethylamine
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; for 3h; Heating; | 60% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 6h; | 58% |
3-benzylcyclohexanospiro-2-oxazolidine
A
1-benzyl-4,5,6,7-tetrahydro-1H-indole
B
N-Benzylethanolamine
C
cyclohexanol
Conditions | Yield |
---|---|
With potassium hydroxide Heating; CH3ONa as reagent; | A 43% B n/a C n/a |
oxirane
benzylamine
A
N-benzyl-diethanolamine
B
N-Benzylethanolamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | |
With borane In tetrahydrofuran | |
With lithium aluminium tetrahydride In tetrahydrofuran |
Conditions | Yield |
---|---|
With ethanol; sodium Durch Reduktion; |
2-chloroethyl N-benzylcarbamate
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium hydroxide at 80℃; |
benzyl chloride
ethanolamine
A
N,N-dibenzyl-2-aminoethanol
B
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium hydroxide; ethanol |
1-benzyl-4,5-dihydro-1H-[1,2,3]triazole
A
1-benzylaziridine
B
acetaldehyde
C
benzylamine
D
N-Benzylethanolamine
Conditions | Yield |
---|---|
With water at 25℃; Rate constant; Product distribution; Mechanism; pH 10.75 (lysine buffer); other solvent, other pH (other buffer concentration, other buffer), H/D isotope effect; |
benzyl bromide
ethanolamine
A
O-benzylethanolamine
B
N-benzyl-2-(benzyloxy)ethan-1-amine
C
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium hydride; tetra(tert-butyl)-ammonium fluoride 1.) THF, reflux, 0.5 h, 2.) THF, 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; | |
With sodium hydride; tetra(tert-butyl)-ammonium fluoride 1.) THF, reflux, 0.5 h, 2.) THF, 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given; |
benzyl chloride
ethanolamine
A
O-benzylethanolamine
B
N-benzyl-2-(benzyloxy)ethan-1-amine
C
N-Benzylethanolamine
Conditions | Yield |
---|---|
With sodium hydride 1.) THF, reflux, 0.5 h, 2.) TH , reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given; |
bromoacetic acid methyl ester
N-Benzylethanolamine
4-benzyl-morpholin-2-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 0 - 20℃; for 24h; Reagent/catalyst; Solvent; | 100% |
With toluene-4-sulfonic acid; triethylamine 1.) benzene, r.t., 12 h, 2.) benzene, reflux, 1 d; Yield given. Multistep reaction; |
2-Chloroacrylonitrile
N-Benzylethanolamine
3-(benzyl(2-hydroxyethyl)amino)-2-chloro-propanenitrile
Conditions | Yield |
---|---|
In diethyl ether at 40℃; | 100% |
In diethyl ether for 120h; Ambient temperature; | |
at 15 - 29℃; Neat (no solvent); |
di-tert-butyl dicarbonate
N-Benzylethanolamine
N-(tert-butoxycarbonyl)-N-benzylethanolamine
Conditions | Yield |
---|---|
In tetrahydrofuran | 100% |
In acetonitrile at 20℃; Condensation; | 100% |
With sodium hydroxide In dichloromethane; water at 20℃; for 24h; | 100% |
N-Benzylethanolamine
2-(3-fluorophenyl)acetaldehyde
2-[benzyl(3'-fluorophenethyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane | 100% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 14h; Inert atmosphere; | 100% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane | 100% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 14h; | 100% |
With sodium tris(acetoxy)borohydride at 20℃; for 14h; | 91% |
N-Benzylethanolamine
2-oxo-3-phenylmethyl-1,2,3-oxathiazolidine
Conditions | Yield |
---|---|
With 1H-imidazole; sulfuryl dichloride; triethylamine In dichloromethane at 0℃; for 1h; pH=15; | 100% |
bromoacetic acid tert-butyl ester
N-Benzylethanolamine
tert-butyl 2-(benzyl-(2-hydroxyethyl)amino)-acetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; for 24h; | 100% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 24h; | 100% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 25℃; for 12h; | 100% |
2-Chloro-pyridin-3-yl acetic acid
N-Benzylethanolamine
N-benzyl-2-(2-chloropyridin-3-yl)-N-(2-hydroxyethyl)acetamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 96h; | 100% |
tert-butyldicarbonate
N-Benzylethanolamine
N-(tert-butoxycarbonyl)-N-benzylethanolamine
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at 20℃; for 24h; | 100% |
phenylacetaldehyde
N-Benzylethanolamine
2-[benzyl(phenethyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 14h; Inert atmosphere; | 100% |
4-fluorophenylacetaldehyde
N-Benzylethanolamine
2-[benzyl(4'-fluorophenethyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 14h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; | 100% |
In dichloromethane at 0 - 20℃; |
3-chloro-5-[(3R)-3-methylmorpholin-4-yl]pyrazine-2-carbaldehyde
N-Benzylethanolamine
2-[benzyl({3-chloro-5-[(3R)-3-methylmorpholin-4-yl]pyrazin-2-yl}methyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In acetonitrile at 10 - 30℃; | 100% |
N-Benzylethanolamine
3-benzyl-2-(2-methylhex-5-en-3-yl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
N-Benzylethanolamine
3-benzyl-2-(7-benzyloxyhept-1-en-4-yl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-(2-bromophenyl)pent-4-enal
N-Benzylethanolamine
3-benzyl-2-(1-(2-bromophenyl)but-3-enyl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-(dibenzylamino)pent-4-enal
N-Benzylethanolamine
N,N-dibenzyl-1-(3-benzyloxazolidin-2-yl)but-3-en-1-amine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-trityloxypent-4-enal
N-Benzylethanolamine
3-benzyl-2-(3-trityloxybut-3-en-4-yl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-trityloxymethylpent-4-enal
N-Benzylethanolamine
3-benzyl-2-(1-trityloxypent-3-enyl)oxazoline
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
(E)-2-allyl-5-phenylpent-4-enal
N-Benzylethanolamine
3-benzyl-2-((E)-1-phenylhepta-1,6-dien-4-yl)oxazoline
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-phenyl-4-penten-1-al
N-Benzylethanolamine
3-benzyl-2-(1-phenylbut-3-enyl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
tert-butyl (S)-(1-oxopent-4-en-2-yl)carbamate
N-Benzylethanolamine
tert-butyl (S)-1-(3-benzyloxazolidin-2-yl)but-3-enylcarbamate
Conditions | Yield |
---|---|
In benzene at 50℃; for 2h; Inert atmosphere; | 100% |
2-propenyl-octanal
N-Benzylethanolamine
3-benzyl-2-(dec-1-en-4-yl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
(+/-)-α-allyl-α-(p-methoxyphenyl)acetaldehyde
N-Benzylethanolamine
3-benzyl-2-[1-(4-methoxyphenyl)but-3-enyl]oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
2-(benzyloxy)-4-pentenal
N-Benzylethanolamine
3-benzyl-2-(3-benzyloxybut-3-en-4-yl)oxazolidine
Conditions | Yield |
---|---|
In toluene for 3h; Inert atmosphere; Heating; | 100% |
3-chloro-5-[methyl(propan-2-yl)amino]pyrazine-2-carbaldehyde
N-Benzylethanolamine
2-[benzyl({3-chloro-5-[methyl(1-methylethyl)amino]pyrazin-2-yl}methyl)amino]ethanol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In acetonitrile at 10 - 30℃; for 5h; | 100% |
tert-Butyl chloroacetate
N-Benzylethanolamine
tert-butyl 2-(benzyl-(2-hydroxyethyl)amino)-acetate
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In acetonitrile Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; for 1.5h; | 100% |
With potassium carbonate In acetonitrile |
N-Benzylethanolamine
(S)-Propylene oxide
Conditions | Yield |
---|---|
at 100℃; for 1h; Microwave irradiation; | 100% |
bromoacetic acid methyl ester
N-Benzylethanolamine
methyl 2-(benzyl(2-hydroxyethyl)amino)acetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 24h; Reagent/catalyst; Solvent; | 100% |
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