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inquiryProduct Name: (2-METHYLPHENOXY)ACETIC ACID Synonyms: (2-methylphenoxy)acetic;(2-methylphenoxy)aceticacid(asimpurity);(o-Tolyloxy)acetic acid;(o-tolyloxy)-aceticaci;(o-tolyloxy)aceticacid;Acetic acid, (2-methylphenoxy)-;Acetic acid, (o-
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inquiry(2-METHYLPHENOXY)ACETIC ACID CAS:1878-49-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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(2-Methylphenoxy)acetic acid cas 1878-49-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
best seller Application:API
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
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potassium chloroacetate
potassium o-cresolate
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
Stage #1: potassium chloroacetate; potassium o-cresolate In water for 2h; Reflux; Stage #2: With hydrogenchloride In water at 30℃; pH=1; | 98% |
Conditions | Yield |
---|---|
With sodium hydroxide; bentonite In water for 0.0833333h; microwave irradiation; | 94% |
With sodium hydroxide In water at 100℃; for 2h; Inert atmosphere; | 51% |
With sodium hydroxide In water Reflux; | 15% |
methyl 2-methylphenoxy acetate
A
o-methylphenoxyacetic acid
B
ortho-cresol
Conditions | Yield |
---|---|
With lithium chloride In N,N-dimethyl-formamide for 22h; Heating; | A 90% B 5% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water for 1h; Reflux; | 89.3% |
With sodium hydroxide at 120℃; pH=8 - 9; pH-value; |
ethyl (2-methylphenoxy)acetate
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol Reflux; | 86% |
With sodium hydroxide In ethanol; water Reflux; | 81% |
Conditions | Yield |
---|---|
With copper(l) iodide; caesium carbonate In water; dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 82% |
Conditions | Yield |
---|---|
With butan-1-ol anschliessend Erhitzen mit wss. NaOH; |
ortho-methylphenoxyacetamide
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With ethanol Erwaermen des Reaktionsgemisches mit wss. NaOH; |
Conditions | Yield |
---|---|
In ethyl acetate |
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With air moisture |
Conditions | Yield |
---|---|
With sodium hydroxide In methanol | |
With sodium hydroxide In water for 0.05h; microwave irradiation; | |
With water; sodium hydroxide Microwave irradiation; | |
With lithium hydroxide In methanol; water at 50℃; for 12h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3; KI; PEG-600 / dimethylformamide / 0.07 h / microwave irradiation 2: NaOH / H2O / 0.05 h / microwave irradiation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaH 2: aq. LiOH / tetrahydrofuran View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 / dimethylformamide 2: aq. NaOH / methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 160 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: MCPA With naphthalene radical anion sodium salt In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; water chemoselective reaction; | |
With 0.5% Pd/Sibunit carbon material; hydrogen In water at 30℃; under 760.051 Torr; for 100h; | |
With hydrogen In water at 30℃; under 760.051 Torr; | |
With palladium/alumina; titanium(IV) oxide for 0.5h; Irradiation; |
Conditions | Yield |
---|---|
Stage #1: ethyl bromoacetate; ortho-cresol With potassium carbonate In acetonitrile at 80℃; for 4h; Stage #2: With water; sodium hydroxide In ethanol at 50℃; for 4h; | |
Stage #1: ethyl bromoacetate; ortho-cresol With potassium carbonate In dimethyl sulfoxide at 50℃; for 6h; Stage #2: With water; sodium hydroxide In acetone at 50℃; for 3h; Stage #3: With hydrogenchloride In water at 25℃; pH=1 - 2; | |
Stage #1: ethyl bromoacetate; ortho-cresol With potassium carbonate In acetonitrile at 80℃; for 4h; Stage #2: With water; sodium hydroxide In ethanol at 50℃; for 4h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 12 h / 75 °C 2: potassium hydroxide / ethanol; water / 1.5 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / water / 8 h / Reflux 2: hydrogenchloride / water / pH 1 View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 5 h / Reflux 2: water; sodium hydroxide / ethanol / 4 h / 20 °C View Scheme |
Sodium; o-tolyloxy-acetate
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water pH=1; |
A
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium tert-butylate / tetrahydrofuran / 24 h / 20 °C 2: glucose dehydrogenase; D-glucose; SyADH from sphingobium yanoikuyae; nicotinamide adenine dinucleotide phosphate / aq. acetate buffer / 1 h / 30 °C / pH 5 / Enzymatic reaction View Scheme |
A
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With glucose dehydrogenase; D-glucose; SyADH from sphingobium yanoikuyae; nicotinamide adenine dinucleotide phosphate In aq. acetate buffer at 30℃; for 1h; pH=5; Enzymatic reaction; stereoselective reaction; | A n/a B n/a C n/a |
o-methylphenoxyacetic acid
(2-methylphenoxy)acetyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; | 100% |
With thionyl chloride In benzene for 3h; Reflux; | 92% |
o-methylphenoxyacetic acid
triethanolamine hydrochloride
2-(2-methylphenyloxy)acetate of tris(2-hydroxyethyl)-ammonium
Conditions | Yield |
---|---|
Stage #1: o-methylphenoxyacetic acid for 1h; Reflux; Alkaline conditions; Stage #2: triethanolamine hydrochloride Reflux; | 99.8% |
Stage #1: o-methylphenoxyacetic acid for 1h; Alkaline conditions; Reflux; Stage #2: triethanolamine hydrochloride Alkaline conditions; | 99.8% |
o-methylphenoxyacetic acid
1-(2,6-dichlorobenzyl)-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one
Conditions | Yield |
---|---|
With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine In dichloromethane at 0 - 20℃; | 99% |
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With calcium oxide In benzene Reflux; | 99% |
Conditions | Yield |
---|---|
With sulfuryl dichloride; aluminium In diethyl ether for 4h; Reflux; | 98% |
With dihydrogen peroxide; chlorine In chlorobenzene at 75℃; | 98% |
With chlorine In toluene at 50 - 55℃; for 2h; Temperature; | 76.8% |
o-methylphenoxyacetic acid
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
Conditions | Yield |
---|---|
In methanol at 20℃; for 12h; | 98% |
Conditions | Yield |
---|---|
In benzene soln. of aroxyacetic acid in benzene contg. ZnO refluxed under stirring for 8 h; evapn. under vac., residue washed with ether, dried under vac.; elem. anal.; | 97% |
Conditions | Yield |
---|---|
In benzene prepn. by refluxing mixt. of 2-methylphenoxyacetic acid and ZnO in C6H6 for 8 h; elem. anal.; | 97% |
In not given | 97% |
o-methylphenoxyacetic acid
1,1-dimethylhydrazine
1,1-dimethylhydrazinium 2-(2-methylphenoxy)acetate
Conditions | Yield |
---|---|
at 45℃; for 0.25h; | 97% |
benzo[b]furan-2-carbohydrazide
o-methylphenoxyacetic acid
C18H14N2O3
Conditions | Yield |
---|---|
With pyridine; trichlorophosphate for 8h; Reflux; | 96% |
o-methylphenoxyacetic acid
N-(3-silatranylpropyl)ammonium-2-methylphenyloxyacetate
Conditions | Yield |
---|---|
In methanol at 15℃; for 0.166667h; | 96% |
Conditions | Yield |
---|---|
With sulfuric acid for 0.0333333h; microwave irradiation; | 95% |
acid at 30℃; Rate constant; other temperature: 40 deg C; | |
With hydrogenchloride | |
With sulfuric acid for 3h; Heating; |
1-hydroxygermatrane monohydrate
o-methylphenoxyacetic acid
C15H21GeNO6
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene for 4h; Heating; Dean-Stark; | 94.3% |
N,N-dimethyl-mono(2-hydroxyethyl)amine-N-oxide
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
In methanol at 25℃; for 1h; | 94% |
N-methyl-N-(3-pyridyl)amine
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 93% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 43% |
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 0 - 20℃; | 92% |
o-methylphenoxyacetic acid
copper
Conditions | Yield |
---|---|
In benzene soln. of aroxyacetic acid in benzene contg. activated Cu refluxed under stirring for 12 h; evapn. under vac., residue washed with ether, dried under vac.; elem. anal.; | 92% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
In methanol at 65℃; | 92% |
o-methylphenoxyacetic acid
benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride
Conditions | Yield |
---|---|
Stage #1: o-methylphenoxyacetic acid; benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride With benzotriazol-1-ol; triethylamine In dichloromethane at 0 - 25℃; for 0.25h; Inert atmosphere; Stage #2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 12.5h; Inert atmosphere; | 92% |
o-methylphenoxyacetic acid
[(1S,2S)-1-Benzyl-3-((R)-4-tert-butylcarbamoyl-thiazolidin-3-yl)-2-hydroxy-3-oxo-propyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; | 91% |
o-methylphenoxyacetic acid
Conditions | Yield |
---|---|
In methanol soln. of Zn compd. and aroxyacetic acid in MeOH refluxed for 12 h; evapn. under vac., crystd. from THF; | 90% |
Conditions | Yield |
---|---|
89% | |
89% | |
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
In methanol at 45℃; for 3h; | 89% |
Conditions | Yield |
---|---|
With triethylamine; 2-hydroxy-2-methylpropanenitrile; 1,1'-carbonyldiimidazole In dichloromethane at 25℃; for 12h; | 88% |
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