high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:534-52-1
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With (NH4)2Ce(NO3)6 on pillared bentonite In methanol at 25℃; for 48h; | 100% |
With thionyl chloride; bismuth subnitrate In dichloromethane at 20℃; for 2h; | 83% |
With cupric nitrate trihydrate supported on K 10 montmorillonite clay; nitric acid; acetic anhydride In tetrachloromethane for 1h; Ambient temperature; | 80% |
Conditions | Yield |
---|---|
With zirconyl nitrate In acetone at 20℃; for 0.45h; | A 43% B 52% |
With bismuth(III) nitrate In acetone at 20℃; for 0.0666667h; | A 35% B 45% |
ortho-cresol
A
2-methyl-4-nitrophenol
B
2-methyl-6-nitrophenol
C
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With Montmorillonite KSF; nitric acid; hafnium oxychloride In tetrahydrofuran at 20℃; for 16h; | A 36% B 46% C 4% |
With Yb-Mo-modified montmorillonite HKSF; nitric acid In tetrahydrofuran at 20℃; for 12h; | A 45% B 39% C 9% |
With Eu-Mo-modified montmorillonite HKSF; nitric acid In tetrahydrofuran at 20℃; for 12h; | A 42% B 40% C 9% |
With Montmorillonite KSF; nitric acid; bismuth(III) nitrate In tetrahydrofuran at 20℃; for 16h; | A 26% B 24% C 22% |
With sulfuric acid; calcium(II) nitrate In water at 2℃; for 5h; Product distribution; other substituted phenols; other nitrating agent, var. temp.; |
2-Methyl-4-cyclopropyl-6-nitrophenol
A
2-methyl-4,6-dinitrophenol
B
5,6-Dinitro-2-methyl-4-cyclopropylphenol
C
3-Nitrooxy-1-(3-methyl-4-hydroxy-5-nitrophenyl)-1-propanol
D
3,4,6-Trinitro-2-hydroxy-2-methyl-4-cyclopropyl-5-cyclohexen-1-one
Conditions | Yield |
---|---|
With dinitrogen tetraoxide In dichloromethane at -10℃; for 3h; Product distribution; | A 30% B 18% C 10% D 17% |
ethanol
2-hydroxy-toluene-3,5-disulfonyl chloride
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
anschliessen Behandeln mit 2n-Salpetersaeure; |
2-Methyl-4-t-butylphenol
A
5-Nitro-6-hydroxy-1-methyl-3-tert.-butyl-benzol
B
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With nitric acid; benzene |
Conditions | Yield |
---|---|
With nitric acid; acetic acid at -20℃; | |
With nitric acid; benzene unter Kuehlung; |
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid; sodium nitrite at 0℃; | |
Multi-step reaction with 2 steps 1: glacial acetic acid; nitrosylsulfuric acid / -15 - -10 °C 2: diluted nitric acid / 40 °C View Scheme | |
Multi-step reaction with 2 steps 1: nitric acid 2: NaOH-solution View Scheme |
Conditions | Yield |
---|---|
With nitric acid; cis-nitrous acid Erwaermen der erhaltenen Diazoniumsalz-Loesung auf 35-50grad; |
5-Nitro-6-hydroxy-1-methyl-3-tert.-butyl-benzol
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With nitric acid |
2-methyl-4,6-dinitroanisole
2-methyl-4,6-dinitrophenol
2-methyl-4,6-dinitroanisole
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With nitrogen oxides; sulfuric acid; water |
Conditions | Yield |
---|---|
With diethyl ether; dinitrogen tetraoxide | |
With nitric acid | |
With nitric acid at 40℃; |
Conditions | Yield |
---|---|
Diazotization.Erhitzen der Diazoniumverbindung mit verd. Salpetersaeure; | |
With nitrogen oxides; water |
Conditions | Yield |
---|---|
With sodium acetate |
Conditions | Yield |
---|---|
With ethanol; nitric acid |
1-methoxy-2-methyl-4-nitrosobenzene
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With nitric acid at 40℃; |
2-bromo-6-methyl-[1,4]benzoquinone-4-oxime
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With nitric acid | |
With nitric acid |
2-hydroxy-toluene-3,5-disulfonyl chloride
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With ethanol nachf. Erhitzen mit Salpetersaeure; |
2,4-dinitro-6-methylphenyl p-toluenesulfonate
sodium phenoxide
A
2-methyl-4,6-dinitrophenol
B
toluene-4-sulfonic acid phenyl ester
2-amino-1-methylbenzene-3,5-disulfonic acid
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With nitrogen oxides; water |
diethyl ether
amyl nitrate
ortho-cresol
2-methyl-4,6-dinitrophenol
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite |
Conditions | Yield |
---|---|
Diazotization.Eintragen der Diazoniumnitratloesung in Salpetersaeure; |
2-methyl-4,6-dinitrophenyl acetate
A
2-methyl-4,6-dinitrophenol
B
acetic acid
Conditions | Yield |
---|---|
With buffer solution; pilocarpine hydrochloride In water; acetonitrile at 24.9℃; Rate constant; other catalysts, var. pH-values; | |
With water at 24℃; Kinetics; |
2-methyl-4,6-dinitrophenol
4.6-diamino-o-cresol
Conditions | Yield |
---|---|
With hydrogen; Raney nickel In methanol at 20℃; under 3750.38 Torr; for 4h; | 98% |
With hydrogen In methanol at 50℃; under 1500.15 Torr; for 0.25h; Inert atmosphere; | 75% |
With hydrogenchloride; tin |
2-methyl-4,6-dinitrophenol
p-toluenesulfonyl chloride
2,4-dinitro-6-methylphenyl p-toluenesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 80% |
With sodium carbonate |
2-methyl-4,6-dinitrophenol
acetic anhydride
2-methyl-4,6-dinitrophenyl acetate
Conditions | Yield |
---|---|
68% | |
With sulfuric acid |
Conditions | Yield |
---|---|
With ethanol | |
With water |
Conditions | Yield |
---|---|
With ammonia at 175 - 185℃; | |
Multi-step reaction with 2 steps 1: K2CO3; acetone 2: water; methanol; ammonia View Scheme |
Conditions | Yield |
---|---|
With ammonium sulfide |