CAS No.7440-05-3,Palladium Suppliers,MSDS download

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Items Standard Result Appearance Silvery white powder Silvery white powder Pd ≥99.95%

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Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）

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Synthetic route

: potassium hexachloropalladate

: 7440-05-3
palladium

Conditions

Conditions	Yield
With hydrogen In neat (no solvent) on calcination in a stream of H2, complete redn. to Pd;;	100%
With H2 In neat (no solvent) on calcination in a stream of H2, complete redn. to Pd;;	100%
With copper(l) chloride redn. of salt to metal with CuCl;;

: 113665-70-6
π-methallyl palladium chloride

: 107-31-3
Methyl formate

A: 25859-52-3
methyl 3-methyl-3-butenoate

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With carbon monoxide; sodium butyrate In neat (no solvent) mixt. of PdCl(C3H5), HCO2Me, Na butyrate (as nucleophile) stirred at room temp. for 30 min, addn. of CO, react. time 2 h; react. mixt. filtered, colourless liquid analysed by GLC;	A 100% B n/a
With carbon monoxide In neat (no solvent) mixt. of PdCl(C3H5), HCO2Me and nucleophile (propionate,acetate,benzoate,chloroacetate,trifluoroacetate,t-BuO(1-),EtO(1-),MeO(1-),PhO(1-),p-Nitro-PhO(1-) or F3-EtO(1-), alkoxides under CO) stirred at room temp. for 30 min, addn. of CO, react. time 2 h; react. mixt. filtered, colourless liquid analysed by GLC;

...Expand

: NNO-[Pd(II)(CH3)((C5H4N)CHN2CO(C6H5))] complex

A: 264876-22-4
formyl 2-pyridyl aldehyde N-acetyl benzoylhydrazone

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With CO In dichloromethane (Ar) in schlenk tube; CO bubbled through soln. at room temp. for 5 min;stirred under CO atmosphere; or at 0°C, or at -40°C; filtered through celite; evapd.; MS anal.; elem. anal.;	A 100% B >99

: palladium dichloride

: 7440-05-3
palladium

Conditions

Conditions	Yield
With hydrazine hydrate In methanol cellulose (5 g) added to soln. of PdCl2 (0.443 g) in MeOH; stirred (15 min); 80% hydrazine hydrate added dropwise (15 min); stirred (12 h, room temp.); solid filtered; washed with methanol and acetone; dried (vac.);	99%
With hydrogenchloride; hydrazine In water	98%
With formic acid In not given refluxing a soln. of PdCl2 and HCOOH for 30 min; decantation, washing with water, drying for 2 h at 120°C;	96%

: π-allyl-palladium chloride

: 107-31-3
Methyl formate

A: 3724-55-8
methyl but-3-enoate

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With carbon monoxide; sodium butyrate In neat (no solvent) mixt. of PdCl(C3H5), HCO2Me and NaC4H9O (as nucleophile) stirred at room temp. for 30 min, addn. of CO, react. time 2 h; react. mixt. filtered, colourless liquid analysed by GLC;	A 99% B n/a
With carbon monoxide In neat (no solvent) mixt. of PdCl(C3H5), MeOH and nucleophile (propionate,acetate,benzoate,chloroacetate,trifluoroacetate,t-BuO(1-),EtO(1-),MeO(1-),PhO(1-),p-Nitro-PhO(1-) or F3-EtO(1-), alkoxides under CO) stirred at room temp. for 30 min, addn. of CO, react. time 2 h; react. mixt. filtered, colourless liquid analysed by GLC;

...Expand

: sodium octahydrotriborate tridioxanate

: palladium (II) ion

: 7440-05-3
palladium

Conditions

Conditions	Yield
In water room temp.; X-ray diffraction, gravimetric anal.;	99%

: palladium (II) acetate

: 7440-05-3
palladium

Conditions

Conditions	Yield
With tetraglyme In further solvent(s) Pd nanoparticles formed in soln. of Pd3(OAc)6 in tetraglyme at tems. 25-270°C for 3 h; UV/Vis spectroscopy;	99%
With H2 In methanol γ-Al2O3 placed in sealed vessel, purged with Ar; in flowing Ar support impregnated with soln. of Pd3(OAc)6 in MeOH with stirring for 2 h; granules dried in air for 15 h and in vac. at 80°C for 5 h; in H2flow at.450°C for 10 h; elem. anal. (ICP AES), XANES;

: 81602-81-5
Pd2(μ-CH3O)2(F6acac)2

: palladium(II) hexafluoroacetylacetonate

B: 7440-05-3
palladium

Conditions

Conditions	Yield
heating in vac. at 110°C;	A 67% B 98%

: 3375-31-3
palladium diacetate

: 7440-05-3
palladium

Conditions

Conditions	Yield
In ethanol; dimethyl sulfoxide Pd(CH3COO)2 dissolved in DMSO under stirring at room temp., treated withEtOH, kept for 1 h at 70°C; collected, centrifuged, washed (EtOH);	96%
Stage #1: palladium diacetate With sodium hydride In tetrahydrofuran at 20℃; Stage #2: With tert-butyl alcohol In tetrahydrofuran at 63℃; for 0.5h; Heating / reflux;
With hydrogen In acetic acid interaction of Pd(OAc)2 with H2 in acetic acid;

: 111138-77-3, 110970-70-2
di-μ-chloro-bis[2-(2-benzothiazolyl)-2-methylpropyl-C(1),N]dipalladium(II)

A: 110978-36-4
methyl 3-(2-benzothiazolyl)-3-methylbutyrate

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With carbon monoxide In methanol High Pressure; carbonylating at 80°c under 50 atm CO for 20 h with stirring; filtn. of Pd, evapn. to dryness, extg. (pentane), evapn., drying in vac., elem. anal;	A 96% B n/a

: (CH3C6H6OC(CH2)2Pd)2Cl2

A: (CH3C6H6OCCH2CH2)2

B: 7440-05-3
palladium

Conditions

Conditions	Yield
In acetonitrile Irradiation (UV/VIS);	A 96% B n/a

: di-μ-acetatobis(cis-2-acetoxycyclooct-5-enyl)dipalladium(II)

: 7440-05-3
palladium

Conditions

Conditions	Yield
In diethyl ether byproducts: exo-C8H11OCOCH3, cyclooctenone; Irradiation (UV/VIS); Pd-complex was irradiated in ether soln. under N2 at room temp. for 3 d;	95%

: bis(triphenylphosphine)dichloro-μ,.mu'.-dichlorodipalladium(II)

: 72926-36-4
[((C6H5)3P)Pd(P(C6H5)2)Cl]2

B: [((C6H5)3P)3(P(C6H5)2)2Pd3Cl](1+)*Cl(1-)=[(P(C6H5)3)3(P(C6H5)2)2Pd3Cl]Cl

C: 7440-05-3
palladium

Conditions

Conditions	Yield
With C6H5NH2; H2 In further solvent(s) byproducts: C6H6, aniline hydrochloride; complex suspn. in C6H5NH2 stirred under H2 at 50°C; evapd. (vac.), washed (Et2O and C6H6), C6H6 filtrate concd. (vac.), hexane added (Ar), ppt. washed with hexane and ether, dried (vac.), recrystd. (toluene under Ar); elem. anal.;	A n/a B 95% C n/a

...Expand

: (2-methylallyl)palladium-chloride dimer

: 744250-78-0
(CH3O)2C6H3CH2P(C(CH3)3)2

A: 744250-84-8
((CH3O)2C6H3CH2P(C(CH3)3)2)2Pd2Cl(C4H7)

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With NaOH In methanol under N2 atm. soln. ligand in MeOH was added to stirred suspn. ((2-methylallyl)PdCl)2 in MeOH (1:1) immediately followed by addn. NaOH in MeOH and stirred at room temp. overnight; ppt. was extd. with benzene and evapd.; elem. anal.;	A 95% B n/a

...Expand

: 15617-18-2, 39958-10-6, 14220-64-5
bis(benzonitrile)palladium(II) dichloride

: rac-2-pyrazol-1-ylcyclohexanonoxime

: 208576-55-0
dichloro(2-pyrazol-1-yl-cyclohexanonoxime)palladium(II)

B: 7440-05-3
palladium

Conditions

Conditions	Yield
In dichloromethane byproducts: benzonitrile; stirring (30 min); filtering, pptn. on n-pentane addn., washing (Et2O), drying (vac.); elem. anal.;	A 92% B 1%

...Expand

: [Pd2Cl2((C6H4)CH(CH3)S(C(CH3)3))2]

: 98-80-6
phenylboronic acid

A: 1067194-59-5
1-(1-tert-butylsulfanylethyl)-2-phenylbenzene

B: 62252-48-6
(+/-)-tert-butyl(1-phenylethyl)sulfane

C: 7440-05-3
palladium

Conditions

Conditions	Yield
With potassium phosphate; triphenylphosphine In N,N-dimethyl-formamide under Ar atm., mixt. of PhB(OH)2, Pd complex, undecane, PPh3, K3PO3 in DMF heated at 50°C for 20 h, heated at 80°C for 3 h; detd. by gas chromy./mass-spectrometry, NMR, IR-spectroscopy, TEM;	A 92% B 2% C n/a
With potassium phosphate In N,N-dimethyl-formamide under Ar atm., mixt. of PhB(OH)2, Pd complex, undecane, K3PO3 in DMF heated at 50°C for 20 h, heated at 80°C for 3 h; detd. by gas chromy./mass-spectrometry, NMR, IR-spectroscopy, TEM;	A 70% B 17% C n/a

...Expand

: 925-90-6
ethylmagnesium bromide

: palladium dichloride

A: 74-84-0
ethane

B: 74-85-1
ethene

C: 7440-05-3
palladium

D: magnesium bromide

E: 7786-30-3
magnesium chloride

Conditions

Conditions	Yield
In tetrahydrofuran To a soln. of anhydrous salt is added C2H5MgBr at 20°C with stirring. The reaction mixture is left for 5 - 6 h at room temp.; decantation, washing with THF, water and ethanol; electron diffraction;	A n/a B n/a C 90% D n/a E n/a

...Expand

: C17H21ClN2O2Pd*0.5H2O

: 7732-18-5
water

A: 1410788-11-2
(S)-1-methylen-2,2-dimethyl-4-(methoxycarbonyl)-2,3,4,5-tetrahydro-indolo[2,1-d]azepinium chloride

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With carbon monoxide In chloroform for 12h;	A 90% B n/a

...Expand

: 112945-77-4
PdCl(OC6H3CH3N2C6H4SOCH3)

A: 112945-76-3
2-(methylsulfinyl)-2'-hydroxy-5'-methylazobenzene

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With hydrazine hydrate In acetonitrile stirring for 0.5 h; pptn. of metallic Pd, filtration, evapn. in vac., chromy. of the CH2Cl2-soln. on silica gel by benzene, evapn. in vac.;	A 89% B n/a

: 35037-11-7
π-crotyl palladium chloride

: 107-31-3
Methyl formate

A: 818-58-6
methyl (E)-pent-3-enoate

B: 51747-33-2
methyl 2-methyl-3-butenoate

C: 36781-66-5
cis-3-pentenoic acid methyl ester

D: 7440-05-3
palladium

Conditions

Conditions	Yield
With carbon monoxide; sodium butyrate In neat (no solvent) mixt. of PdCl(C3H5), HCO2Me, Na butyrate (as nucleophile) stirred at room temp. for 30 min, addn. of CO, react. time 2 h; react. mixt. filtered, colourless liquid analysed by GLC;	A 87.6% B 4.3% C 8% D n/a

...Expand

: bis(chloro(cycloheptene)palladium)

A: 55759-30-3
3-(2-cycloheptenyl)cycloheptene

B: 7440-05-3
palladium

Conditions

Conditions	Yield
In acetonitrile Irradiation (UV/VIS);	A 87% B n/a

: bis(η3-allyl)palladium

: 557-40-4
Allyl ether

A: 210691-22-8
(diallyl ether)(triphenylphosphane)palladium(0)

B: 7440-05-3
palladium

Conditions

Conditions	Yield
With triphenyl phosphine In neat (no solvent) (Ar); heating of soln. of Pd complex and PPh3 (equimolar amts., 90°C, several min) in diallyl ether, cooling (20°C), filtration, cooling (below 0°C), crystn.; removal of mother liquor, washing (cold C5H12), drying (in vacuo, 20°C); elem. anal.;	A 86% B n/a

...Expand

: bis(η3-allyl)palladium

A: 210691-12-6
((CH3)2CH)3PPd(η(2),η(2)-C7H12)

B: 7440-05-3
palladium

Conditions

Conditions	Yield
In further solvent(s) (Ar); addn. of P(iPr)3 to soln. of equimolar amt. of Pd complex in hepta-1,6-diene, heating (80°C, 2 h), evapn., dissoln. (C5H12), filtration (Pd), cooling (-30 to -78°C), crystn.; removal of mother liquor, washing (cold C5H12), drying (in vacuo, 20°C);	A 85% B n/a

: 598-25-4
Dimethylallene

: [Pd2{κ2(C,N)-C6H4CH2NH2-2,OMe-5}2(μ-Br)2]

A: 1410788-52-1
3,3-dimethyl-4-methylen-6-methoxy-1,2,3,4-tetrahydroisoquinolinium bromide

B: 7440-05-3
palladium

Conditions

Conditions	Yield
In dichloromethane for 12h; Inert atmosphere;	A 85% B n/a

...Expand

: C34H26Cl2N10Pd

: 7440-05-3
palladium

Conditions

Conditions	Yield
With tetrabutylammomium bromide In neat (no solvent) at 120℃; for 12h;	85%

: trans[iodobis(triphenylphosphine)phenylpalladium(II)]

A: 23523-32-2, 22180-54-7
diiodobis(triphenylphosphino)palladium(II)

B: 2065-67-0
tetraphenylphosphonium iodide

C: 7440-05-3
palladium

Conditions

Conditions	Yield
In toluene byproducts: PPh3; under N2 at 110 °C for 16 h;	A <0.1 B 84% C n/a

...Expand

: 102238-17-5
6-(4,5-dimethoxy-2-nitrophenyl)-2,3-dimethoxynaphthalene

: 7440-05-3
palladium

: 102012-70-4
6-(2-amino-4,5-dimethoxyphenyl)-2,3-dimethoxynaphthalene

Conditions

Conditions	Yield
In ethyl acetate	100%

: {4-[2,4-Dihydroxyphenyl]cyclohexylidene}acetic acid

: 7440-05-3
palladium

: trans-[4-(2,4-Dihydroxyphenyl)cyclohexyl]acetic acid

Conditions

Conditions	Yield
In ethanol	100%
In ethanol	100%

: 295788-95-3
8-[2,4-Bis(methoxymethoxy)phenyl]-1,4-dioxaspiro[4.5]dec-7-ene

: 7440-05-3
palladium

: 295788-96-4
8-[2,4-bis(methoxymethoxy)phenyl]-1,4-dioxaspiro[4.5]decane

Conditions

Conditions	Yield
	100%
	100%
	100%

: 296764-27-7
tert-butyl (4-{4-[2,4-bis(methoxymethoxy)phenyl]-3-cyclohexen-1-yl}phenoxy) dimethylsilane

: 7440-05-3
palladium

: tert-Butyl (4-{4-[2,4-bis(methoxymethoxy)phenyl]cyclohexyl}phenoxy) Dimethyl Silane

Conditions

Conditions	Yield
In ethanol	100%

: 111-69-3
hexanedinitrile

: 7440-05-3
palladium

: tetramethylhexamethylenediamine

Conditions

Conditions	Yield
In dimethyl amine	100%

: 3-(3,5-difluoro-4-methoxyphenyl)propenoic acid

: 7440-05-3
palladium

: 105219-44-1
3-(3,5-Difluoro-4-methoxyphenyl)propanoic acid

Conditions

Conditions	Yield
In tetrahydrofuran; pyrographite; ethyl acetate	100%

: 7646-69-7
sodium hydride

: 7440-05-3
palladium

: sodium palladium hydrate

Conditions

Conditions	Yield
In neat (no solvent) 2:1 molar mixture of educts, 700K;	100%
In neat (no solvent, solid phase) according to: W. Bronger, P. Mueller, D. Schmitz, H. Spittank, Z. anorg. allg. Chem. 516 (1984) 35; heating reaction mixt. (molar ratio NaH:Pd=4:1) in H2 atmosphere (360°C, 6 h); X-ray anal.;

: 7697-37-2
nitric acid

: 7440-05-3
palladium

: palladium (II) nitrate

Conditions

Conditions	Yield
With sulfur trioxide pyridine complex at 25 - 100℃; for 180h; Sealed tube;	100%
In nitric acid in presence of air;
In nitric acid byproducts: N-oxide; by heating; in presence of air;

: hydrous titanium(IV) oxide

: 7440-05-3
palladium

: O3PdTi, orthorhombic

Conditions

Conditions	Yield
In neat (no solvent, solid phase) Pd:Ti ratio = 1:1, without addn. of carbonate or addn. of 0.42 mass% Li2CO3 or 0.52 mass% Na2CO3, grinding in ethanol, pelletizing, heating in air at 760 to 780°C with repeated grinding and compressing, annealing time 40 or 12 h;	100%

: fuming sulphuric acid

: 7440-05-3
palladium

: 2HO7S2(1-)*Pd(2+)

Conditions

Conditions	Yield
With nitronium trifluoromethanesulfonate at 25 - 90℃; for 103h;	100%

: 75-75-2
methanesulfonic acid

: 7440-05-3
palladium

: Pd(2+)*2CH3SO3(1-)=Pd(CH3SO3)2

Conditions

Conditions	Yield
With nitric acid at 20 - 120℃; for 225h; Sealed tube;	100%

: 7647-01-0
hydrogenchloride

: 420-04-2
CYANAMID

: 7440-05-3
palladium

: Cl4Pd(2-)*2CH4ClN2(1+)

Conditions

Conditions	Yield
Stage #1: palladium With hydrogenchloride; nitric acid In water Stage #2: hydrogenchloride In water Stage #3: CYANAMID With hydrogenchloride In water	100%

...Expand

: 7647-01-0
hydrogenchloride

: 7440-05-3
palladium

: 603-35-0
triphenylphosphine

: 13965-03-2
bis-triphenylphosphine-palladium(II) chloride

Conditions

Conditions	Yield
Stage #1: hydrogenchloride; palladium With aqua regia at 80℃; Stage #2: triphenylphosphine In ethanol at 70℃; Stage #3: In ethanol at 70℃; for 1h; Temperature; Solvent;	100%

...Expand

: 7647-01-0
hydrogenchloride

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 7440-05-3
palladium

: 72287-26-4, 95464-05-4
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride

Conditions

Conditions	Yield
In tetrahydrofuran; ethanol; water at 55 - 60℃; for 3h; Solvent; Temperature; Inert atmosphere;	99.7%

...Expand

: 294852-07-6
4-(tert-butoxycarbonylamino)naphthalen-1-ylboronic acid

: 497-19-8
sodium carbonate

: 7440-05-3
palladium

: 515843-39-7
7-(4-amino-naphthalen-1-yl)-1H-pyrido [2,3-b][1,4]oxazin-2-one Hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride; ammonium formate; acetic acid; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; ethyl acetate; N,N-dimethyl-formamide	99%

...Expand

: 7440-05-3
palladium

: 338948-29-1
6-(2-nitrophenyl)-2,3-dimethoxynaphthalene

: 338948-30-4
6-(2-aminophenyl)-2,3-dimethoxynaphthalene

Conditions

Conditions	Yield
In ethyl acetate	99%

: 7440-44-0
pyrographite

: 7440-05-3
palladium

: 5-nitro-biphenyl-2-carboxylic acid methyl ester

: 51990-95-5
5-amino-biphenyl-2-carboxylic acid methyl ester

Conditions

Conditions	Yield
With ammonium formate In methanol; chloroform	99%

...Expand

: 292638-84-7
styrene

: 7440-05-3
palladium

: 38053-74-6, 38053-75-7, 7726-28-5
(1-phenylethyl)trichlorosilane

Conditions

Conditions	Yield
With trichlorosilane; bis(η3-allyl-μ-chloropalladium(II))	99%

: 7440-05-3
palladium

: 64-19-7
acetic acid

: 3375-31-3
palladium diacetate

Conditions

Conditions	Yield
With nitric acid In nitric acid; acetic acid boiling Pd-sponge in mixt. of glacial AcOH and concd. HNO3 (100:3 v/v), addn. of further Pd to end of evolution of N-oxides (if necessary); hot filtration, cooling (crystn.), washing (AcOH, water), drying in air;	99%
With nitric acid for 0.5h; Reflux;	92%
With nitric acid In acetic acid Pd oxidized with HNO3 in CH3COOH for 30 h according to Stephenson, T.A.,Morehouse, S.M., Powell, A.R., Heffer, J.P., and Wilkinson, G., J. Chem . Soc., 1965, vol. 6, no. 6, p. 3632; crystd.;	80%

: arsenic

: niobium

: 7440-05-3
palladium

: Nb5Pd4As4

Conditions

Conditions	Yield
In neat (no solvent) Nb, Pd and As powders (molar ratio 5:4:4) loaded into alumina tube; evacuated; heated at 600°C for 1 d and 1000°C for 3 d; detd. by X-ray powder diffraction;	99%

...Expand

: 7783-08-6
selenic acid

: 7440-05-3
palladium

: palladium selenite

Conditions

Conditions	Yield
In neat (no solvent) Pd powder (30 mg) and H2SeO4 (1 ml) sealed in glass ampoule; heated (350°C, 72 h); cooled (3°C/h);	99%

: 7783-08-6
selenic acid

: 7440-05-3
palladium

: palladium (II) selenate

Conditions

Conditions	Yield
In neat (no solvent) Pd powder (15 mg) and H2SeO4 (1 ml) sealed in glass ampoule; heated (350°C, 72 h); cooled (3°C/h);	99%
In further solvent(s) on dissolving Pd sponge in a hot mixture of H2SeO4 and HNO3 and slow cooling down of concd. soln.;; on evaporization of soln. of Pd in H2SeO4, selenate is not obtained without impurity of H2SeO4 or H2SeO3;;
In further solvent(s) on dissolving Pd sponge in a hot mixture of H2SeO4 and HNO3 and slow cooling down of concd. soln.;; on evaporization of soln. of Pd in H2SeO4, selenate is not obtained without impurity of H2SeO4 or H2SeO3;;

: 7783-08-6
selenic acid

: 13768-86-0
selenium trioxide

: 7440-05-3
palladium

: palladium diselenite

Conditions

Conditions	Yield
In neat (no solvent) Pd powder (8 mg) and H2SeO4 (1 ml) and SeO3 (50 mg) sealed in glass ampoule; heated to 250°C; cooled (3°C/h);	99%

...Expand

: N,N'-dimethylperhydrodiazepine-2,3-di(thionediiodine)

: 7440-05-3
palladium

: [(N,N'-dimethylperhydrodiazepine-2,3-dithione)palladium(II)] di(triiodide)

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: I2; at room temp. for 1 h;	99%

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