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inquirySelenic acid CAS NO 7783-08-6 Application:Selenic acid CAS NO 7783-08-6
Supply top quality products with a reasonable price Application:api
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Selenic acid CAS NO 7783-08-6 Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/She
Selenic acid CAS NO 7783-08-6 Application:Selenic acid CAS NO 7783-08-6
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
Conditions | Yield |
---|---|
In water byproducts: BaSO4; heating of BaSeO4, H2SO4 and H2O in a crucible for about 2.5 h;; | 85% |
In water byproducts: BaSO4; heating;; | |
In water |
Conditions | Yield |
---|---|
In nitromethane dry air atm.; -20-30°C, 2 d - 6 weeks; | A 51% B n/a C n/a |
Conditions | Yield |
---|---|
In water | |
In water |
selenic acid
Conditions | Yield |
---|---|
With bromine In water oxidation of Ag2SeO3 with Br2;; | >99 |
With bromine In water byproducts: AgBr; addn. of Br2 to a suspension of Ag2SeO3 in H2O under vigorous stirring; passing of a stream of air through the soln. after 2 h;; filtration; passing of air through the filtrate; addn. of HBr; addn. of aq. Br2; filtration; successive concn. of the filtrate in air and in vac.;; | |
With bromine In water byproducts: AgBr; |
Conditions | Yield |
---|---|
With bromine In water byproducts: AgBr; treatment of a suspension of Ag2SeO3 in H2O with Br2;; | |
With Br2 In water byproducts: AgBr; treatment of a suspension of Ag2SeO3 in H2O with Br2;; |
selenium
water
ozone
A
selenious acid
B
selenic acid
Conditions | Yield |
---|---|
In water | A 0% B n/a |
In water | A 0% B n/a |
Conditions | Yield |
---|---|
In water reaction of ozone and Se in presence of H2O;; | A 0% B n/a |
In water |
Conditions | Yield |
---|---|
With lead(II) nitrate In neat (no solvent) byproducts: PbS; melting of clausthalite and KNO3; dissolving of the melt in HNO3; boiling; addn. of Pb(NO3)2; decompn. of the formed PbSeO4 with H2S;; | |
With Pb(NO3)2 In neat (no solvent) byproducts: PbS; melting of clausthalite and KNO3; dissolving of the melt in HNO3; boiling; addn. of Pb(NO3)2; decompn. of the formed PbSeO4 with H2S;; | |
With Pb(NO3)2 |
selenium
water
chlorine
A
selenious acid
B
selenic acid
Conditions | Yield |
---|---|
In water | |
In water |
selenic acid
Conditions | Yield |
---|---|
In not given Electrolysis; |
Conditions | Yield |
---|---|
In water byproducts: CuS; | |
In water byproducts: CuSO4, CuS; | |
In water |
Conditions | Yield |
---|---|
In not given | |
In not given |
Conditions | Yield |
---|---|
With nitric acid In water byproducts: Cl2; dissolving of a suspension of Se in H2O by addn. of HNO3; concg.; addn. of HClO3; evapn.; concn. on passing of air through the soln. under reduced pressure; concn. at 150°C under reduced pressure;; diln. with H2O; filtration; concn. in vac.;; | 90-95 |
In not given | |
With HNO3 In water byproducts: Cl2; dissolving of a suspension of Se in H2O by addn. of HNO3; concg.; addn. of HClO3; evapn.; concn. on passing of air through the soln. under reduced pressure; concn. at 150°C under reduced pressure;; diln. with H2O; filtration; concn. in vac.;; | 90-95 |
In not given |
Conditions | Yield |
---|---|
In not given at elevated temp.;; | |
In not given at elevated temp.;; |
selenium(IV) oxide
nitric acid
A
selenious acid
B
selenic acid
Conditions | Yield |
---|---|
In not given | A n/a B 0% |
In not given |
Conditions | Yield |
---|---|
In nitric acid formation of small amounts of selenic acid, addition of HCl, avoids formation of selenic acid;; |
Conditions | Yield |
---|---|
In not given | A n/a B 0% |
In not given |
selenic acid
Conditions | Yield |
---|---|
In water Electrolysis; cathode: Pt vessel, anode: Pt spiral, cathodic current density: 0.2 A/dm*dm, ambient temp.;; |
Conditions | Yield |
---|---|
In water incomplete reaction;; |
Conditions | Yield |
---|---|
In water byproducts: PbS; introduction of H2S into an aq. soln. of PbSeO4;; filtration; boiling of the filtrate; concn.;; | |
In water byproducts: PbS; | |
In water introduction of H2S into a suspension of PbSeO4 in H2O;; |
Conditions | Yield |
---|---|
In melt oxidation with melting KNO3;; |
Conditions | Yield |
---|---|
With lead(II) nitrate In not given melting of SeO2 and KNO3; dissolving of the melt in aq. HNO3; boiling; addition of Pb(NO3)2; decomposition of the formed PbSeO4 with H2S;; | |
With Pb(NO3)2 In not given melting of SeO2 and KNO3; dissolving of the melt in aq. HNO3; boiling; addition of Pb(NO3)2; decomposition of the formed PbSeO4 with H2S;; | |
With Pb(NO3)2 |
Conditions | Yield |
---|---|
In melt oxidation with melting KNO3;; |
Conditions | Yield |
---|---|
With hydrogen peroxide In water 50°C in O2 atm.; dehydrated with P2O5-dried oxygen stream and a partial vac.; |
Conditions | Yield |
---|---|
With mercury(I) chloride In hydrogenchloride | |
In hydrogenchloride |
Conditions | Yield |
---|---|
In water repeated evapn. of SeO2 and an excess of 30% H2O2 in an open vessel;; | |
In water boiling of SeO2 and 30% H2O2 under reflux for some hours;; | |
In water repeated evapn. of SeO2 and an excess of 30% H2O2 in an open vessel;; | |
With O2 In water; dihydrogen peroxide storage of an aq. soln. of SeO2 and H2O2 for 24 hours; boiling for 12 hours under reflux and passing of O2 through the solution;; concn. under reduced pressure;; | |
In water boiling of SeO2 and 30% H2O2 under reflux for some hours;; |
Conditions | Yield |
---|---|
In melt oxidation with melting NaNO3;; |
Conditions | Yield |
---|---|
In water Electrolysis; use of Pb-anode;; |
Conditions | Yield |
---|---|
In nitric acid Electrolysis; free of SeO2;; | |
With bromine In water equilibrium reaction;; not isolated;; | |
With bromine In water equilibrium reaction;; |
Conditions | Yield |
---|---|
In water Electrolysis; various conditions;; | |
In water Electrolysis; use of a diaphragm, mixture of 6% H2SeO4 and 10% Na2SeO4 as catholyte, aq. H2SeO3 as anolythe;; |
Conditions | Yield |
---|---|
at 10 °C, with excess of H2SeO4; washing with water and acetone; | 100% |
with dild. soln. of H2SeO4, mixing, at 10 °C; | 100% |
at 10 °C, with excess of H2SeO4; washing with water and acetone; | 100% |
with dild. soln. of H2SeO4, mixing, at 10 °C; | 100% |
Conditions | Yield |
---|---|
compd. is heated with selenic acid in a sealed tube at 553 K (1 wk); | 99.9% |
Conditions | Yield |
---|---|
In neat (no solvent) Pd powder (30 mg) and H2SeO4 (1 ml) sealed in glass ampoule; heated (350°C, 72 h); cooled (3°C/h); | 99% |
Conditions | Yield |
---|---|
In neat (no solvent) Pd powder (15 mg) and H2SeO4 (1 ml) sealed in glass ampoule; heated (350°C, 72 h); cooled (3°C/h); | 99% |
In further solvent(s) on dissolving Pd sponge in a hot mixture of H2SeO4 and HNO3 and slow cooling down of concd. soln.;; on evaporization of soln. of Pd in H2SeO4, selenate is not obtained without impurity of H2SeO4 or H2SeO3;; | |
In further solvent(s) on dissolving Pd sponge in a hot mixture of H2SeO4 and HNO3 and slow cooling down of concd. soln.;; on evaporization of soln. of Pd in H2SeO4, selenate is not obtained without impurity of H2SeO4 or H2SeO3;; |
Conditions | Yield |
---|---|
In neat (no solvent) Pd powder (8 mg) and H2SeO4 (1 ml) and SeO3 (50 mg) sealed in glass ampoule; heated to 250°C; cooled (3°C/h); | 99% |
Conditions | Yield |
---|---|
at 20℃; | 97% |
Conditions | Yield |
---|---|
In water mixt. of butylamine, H2SeO4 and U compd. in H2O was stirred until complete homogenization; poured into watch glass and evapd. for 6-7 d; | 90% |
Conditions | Yield |
---|---|
In water refluxing MoO3 and pyrazole with excess H2SeO4; recrystn. (Me2CO diffusion into aq. soln.); elem. anal.; | 89% |
selenic acid
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: Cl2; H2SeO4 and Cr-complex were warmed at 70°C for 6 h, soln. was allowed to cool to room temp., MeOH was added; collected, washed with MeOH; elem. anal.; | 89% |
Conditions | Yield |
---|---|
In water High Pressure; AgNO3, MoO3, H2SeO4 and H2O placed in autoclave, sealed, heated at 200°C for 3 d, cooled to room temp. at 9°C/h; ppt. washed with H2O and MeOH, dried; | 88.8% |
Conditions | Yield |
---|---|
With sulfuric acid; potassium iodide In sulfuric acid byproducts: I2; sepn. of the formed I2 by distn.;; | 87.8% |
With sulfuric acid; potassium iodide In sulfuric acid byproducts: I2, H2O; storage at room temperature for 4 weeks;; | 38.4% |
With sodium hypophosphite In water heating for a longer period of time;; | >99 |
Conditions | Yield |
---|---|
With Si(OEt)4; HNO3 In water High Pressure; Nd2O3 (1 equiv.) (acidified with HNO3), KOH (2 equiv.) and H2SeO4 (3 equiv.) were mixed in H2O; soln. was stirred for 30 min; Si(OEt)4 was addedgradually; stirred at 353 K; sealed in autoclave; heated at 483 K for 3 d; elem. anal.; | 85% |
water
selenic acid
triphenylphosphine
[Ag(P(C6H5)3)2(HSeO4)(H2O)]*[Ag(P(C6H5)3)2(HSeO4)]*H2O
Conditions | Yield |
---|---|
In ethanol mixt. of Ag salt and ligand dissolved in warm EtOH, cooled, H2SeO4/H2O added, heated with stirring; crystd. on slow cooling to room temp., washed (ice-cold aq. EtOH); elem.anal.; | 84% |
Conditions | Yield |
---|---|
With KNO3 In water High Pressure; under hydrothermal conditions; appropriate amt. Pd(NO3)2, KNO3, concd. H2SeO4 and H2O placed in autoclave; sealed; heated at 200°C for 4 d; cooled to room temp. (9°C/h); crystals washed with H2O and MeOH; dried; detd. by EDX analysis; | 82% |
Conditions | Yield |
---|---|
With KOH; Si(OEt)4; HNO3 In water High Pressure; La2O3 (1 equiv.) (acidified with HNO3), KOH (2 equiv.) and H2SeO4 (3 equiv.) were mixed in H2O; soln. was stirred for 30 min; Si(OEt)4 was addedgradually; stirred at 353 K; sealed in autoclave; heated at 473 K for 3 d; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In water High Pressure; a few pieces of Au and concd. selenic acid placed in steel autoclave; heated at 250°C for 10 h; cooled slowly (5°C/h); crystals washed with water; dried in air; | 80% |
Conditions | Yield |
---|---|
In water High Pressure; under hydrothermal conditions; U compd., H2SeO4 and piperazine (molar ratio 1:23:2.7) loaded in autoclave; water added; sealed; heated at 130°C for 2 d; cooled to 23°C (9°C/h); mother liquor decanted; crystals washed with MeOH; dried; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In water at 200℃; for 120h; Autoclave; | 80% |
Conditions | Yield |
---|---|
at 20℃; under 760.051 Torr; | 77% |
Conditions | Yield |
---|---|
With potassium nitrate In water at 220℃; for 96h; Glovebox; Autoclave; | 73.6% |
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