img _fcksavedurl="/UserAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:111-69-3 Transportation:by air or by sea Port:Shanghai
Cas:111-69-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:111-69-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
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Cas:111-69-3
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry1,4-Dicyanobutane Basic information Product Name: 1,4-Dicyanobutane Synonyms: Adipic acid nitrile;adipicacidnitrile;Adipicdinitrile;adipinsaeuredinitril;Adipodinitrile;adiponitril;Adipyl
Cas:111-69-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name 1,4-Dicyanobutane Synonyms 1,4-Dicyanobutane;Adiponitrile CAS: 111-69-3 MF: - MW: - EINECS: -
Cas:111-69-3
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
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Cas:111-69-3
Min.Order:1 Metric Ton
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Type:Trading Company
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Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:111-69-3
Min.Order:4 Kilogram
Negotiable
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:111-69-3
Min.Order:10 Gram
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Type:Lab/Research institutions
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We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:111-69-3
Min.Order:1 Gram
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Type:Lab/Research institutions
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Min.Order:20 Metric Ton
Negotiable
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:111-69-3
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
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TIANFUCHEM--High purity 111-69-3 1,4-Dicyanobutane Application:TIANFUCHEM--High purity 111-69-3 1,4-Dicyanobutane
Cas:111-69-3
Min.Order:0
Negotiable
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Cas:111-69-3
Min.Order:0
Negotiable
Type:Trading Company
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1,4-Dicyanobutane Basic information Product Name: 1,4-Dicyanobutane
Cas:111-69-3
Min.Order:100 Gram
Negotiable
Type:Trading Company
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At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
Conditions | Yield |
---|---|
With 18-crown-6 ether In acetonitrile for 15h; Heating; | 96% |
With Polysorbate 80 (1) In acetonitrile for 1.5h; Product distribution; Heating; other alkyl halides; | 70% |
With Polysorbate 80 (1) In acetonitrile for 1.5h; Heating; | 70% |
Conditions | Yield |
---|---|
With phosphorus pentachloride; toluene-4-sulfonic acid for 2h; Reagent/catalyst; Temperature; Reflux; | 96% |
With di(n-butyl)tin oxide In toluene Heating; | 84% |
With phosphorus pentoxide under 15.0015 - 37.5038 Torr; for 1h; Temperature; Heating; | 83% |
hydrogen cyanide
2-pentenenitrile
4-Pentenenitrile
3-pentenenitrile
hexanedinitrile
Conditions | Yield |
---|---|
With zinc(II) chloride at 50℃; for 49 - 53h; Product distribution / selectivity; | 95% |
With zinc(II) chloride at 50℃; for 49 - 53h; Product distribution / selectivity; | 95% |
With iron(II) chloride at 50℃; for 69 - 78h; Product distribution / selectivity; | 94.4% |
Conditions | Yield |
---|---|
In acetone at 70℃; for 1.83333h; Temperature; | 94% |
Conditions | Yield |
---|---|
With nickel(II) sulphate; sodium hydroxide; dipotassium peroxodisulfate In dichloromethane for 24h; Ambient temperature; | 93% |
With potassium hydroxide In water; tert-butyl alcohol at 40℃; for 4h; electrolysis at a Ni(OH)2 anode and a steel cathode, current - 2 A, cell voltage - 2.0 V; | 93% |
With tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 20℃; for 0.0833333h; Inert atmosphere; Molecular sieve; | 86% |
hydrogen cyanide
4-Pentenenitrile
3-pentenenitrile
hexanedinitrile
Conditions | Yield |
---|---|
With zinc(II) chloride at 50℃; for 45 - 48h; Product distribution / selectivity; | 93% |
With zinc(II) chloride at 50℃; for 45 - 48h; Product distribution / selectivity; | 93% |
With zinc(II) chloride at 50℃; for 46 - 54h; Product distribution / selectivity; | 92.5% |
Conditions | Yield |
---|---|
With water; triphenylphosphine; zinc; diiodobis(triphenylphosphine)cobalt(II) In acetonitrile at 80℃; for 24h; | 89% |
With potassium phosphate; tetraethylammonium phosphate at 20 - 22℃; Product distribution; electrolytic hydrodimerization, var. quaternary ammonium salts, var. electrodes; | 86.9% |
With potassium phosphate; tetraethylammonium phosphate at 20 - 22℃; electrolysis; | 86.9% |
Conditions | Yield |
---|---|
With formic acid In methanol; water at 100℃; for 12h; Green chemistry; chemoselective reaction; | 88% |
With hydrogen; (o-OC6H4CH3)3PRuCl(PPh3)2 at 130℃; under 3620.04 Torr; for 20h; | 78 % Chromat. |
With hydrogen; (o-OC6H4CH3)3PRuCl(PPh3)2 at 130℃; under 3620.04 Torr; for 20h; Product distribution; | 78 % Chromat. |
Conditions | Yield |
---|---|
With sulfonamide; toluene-4-sulfonic acid In toluene at 120℃; for 3h; | 85% |
Multi-step reaction with 2 steps 1: ammonia 2: phosphorus pentachloride / 150 °C View Scheme |
Conditions | Yield |
---|---|
In sulfolane; iron(III) chloride | 84% |
Conditions | Yield |
---|---|
at 70℃; for 3h; | 82% |
at 70℃; for 3h; | 81% |
at 70℃; for 3h; | 81% |
1,4-dibromo-butane
N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid
A
hexanedinitrile
B
1,1,2,2,3,3-Hexamethylguanidiniumbromid
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | A 78% B n/a |
Conditions | Yield |
---|---|
With cyanide(1-); <p>-(CH2)3-<sup>+</sup>PBu3</p> In water at 110℃; for 0.5h; | 74% |
Conditions | Yield |
---|---|
Stage #1: 3-cyano-propionic acid methyl ester With potassium hydroxide In methanol at 60℃; for 0.5h; Kolbe coupling; Stage #2: In acetone at 60℃; Kolbe coupling; Electrochemical reaction; | 74% |
Conditions | Yield |
---|---|
With ammonia In 1,4-dioxane at 150℃; under 4500.45 Torr; for 25h; Temperature; Reagent/catalyst; Solvent; | 73.2% |
Conditions | Yield |
---|---|
With bis(acetylacetonate)oxovanadium In tetrachloromethane at 150℃; for 6h; Autoclave; | 72% |
With phosphoric acid at 300℃; | |
With ammonium phosphate at 300℃; | |
With sulfuric acid at 300℃; |
Conditions | Yield |
---|---|
With ammonia; iodine In water; acetonitrile at 70℃; | 70% |
Conditions | Yield |
---|---|
With ammonia; iodine In water at 70℃; for 6h; | 70% |
Conditions | Yield |
---|---|
With trimethylsilylazide; silver carbonate In dimethyl sulfoxide at 100℃; for 12h; | 65% |
Conditions | Yield |
---|---|
With sodium bromide In methanol at 10℃; electrooxidation (0.3 A, 75 mA/cm2, 5-7 V) 8.4 F/mol; | 60% |
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate; ammonium hydroxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In acetonitrile at 20℃; for 12h; | 58% |
Conditions | Yield |
---|---|
With potassium phosphate; C9H20NO3PS3*C5H13N at 20 - 22℃; electrolysis; | A 55.1% B 41% |
4-Pentenenitrile
2-hydroxy-2-methylpropanenitrile
A
3-pentenenitrile
B
hexanedinitrile
Conditions | Yield |
---|---|
With Lewis acid; C70H84O8P2 In tetrahydrofuran at 90℃; for 4h; | A 53% B n/a |
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; zinc In toluene for 24h; Inert atmosphere; Sealed tube; Heating; Green chemistry; | 28% |
Conditions | Yield |
---|---|
With ammonia; iodine In water at 60℃; for 24h; | A 24% B 17% |
acrylonitrile
A
cis-1,4-dicyano-1-butene
B
trans-1,4-dicyanobut-1-ene
C
hexanedinitrile
D
propiononitrile
Conditions | Yield |
---|---|
With hydrogen; (η6-1,3,5-cyclooctatriene)(η4-1,5-cyclooctadiene)ruthenium(0) at 150℃; under 19000 Torr; for 3h; Dimerization; hydrogenation; | A 20% B 20% C 2% D 19% |
3-pentenenitrile
2-hydroxy-2-methylpropanenitrile
A
4-Pentenenitrile
B
hexanedinitrile
Conditions | Yield |
---|---|
With Lewis acid; bis(1,5-cyclooctadiene)nickel (0); C70H84O8P2 In tetrahydrofuran at 90℃; for 4h; Product distribution / selectivity; | A 19% B n/a |
Conditions | Yield |
---|---|
With deuterium; (η6-1,3,5-cyclooctatriene)(η4-1,5-cyclooctadiene)ruthenium(0) at 150℃; under 10640 Torr; for 5h; Dimerization; hydrogenation; | A 1% B 15% C 16% D 16% |
Conditions | Yield |
---|---|
With N-(4-sulphonic acid)butylpyridinium hydrogen sulphate; 1-sulfobutyl pyridine bisulfate hydroxylamine salt In acetonitrile at 80℃; under 760.051 Torr; for 1h; Solvent; Temperature; Time; | 11.34% |
Conditions | Yield |
---|---|
In dimethyl amine | 100% |
Conditions | Yield |
---|---|
In N-butylamine | 100% |
Conditions | Yield |
---|---|
With [RuH(tBu-PNP(-))(CO)]; water In tert-butyl alcohol at 50℃; for 24h; | 99% |
With water; dihydridotetrakis(triphenylphosphine)ruthenium In 1,2-dimethoxyethane at 120℃; for 24h; | 91% |
With water at 150℃; under 5171.62 - 6205.94 Torr; for 5h; Inert atmosphere; Microwave irradiation; | 89% |
Conditions | Yield |
---|---|
With sodium hydroxide; tricyclohexylphosphine; {Rh(OMe)(cod)}2 In isopropyl alcohol at 25℃; for 48h; | A 1% B 99% |
With Pseudomonas chlororaphis B23 immobilized on alginate bead at 5℃; pH=7; hydration; Microbiological reaction; | A 93% B 3% |
With Acetaldehyde oxime In methanol at 65℃; for 4h; | A 46% B 54% |
hexanedinitrile
Conditions | Yield |
---|---|
In toluene (N2), Schlenk technique; cyanide was added to a suspn. of complex in toluene, the soln. was stirred for 14 h at room temp.; volatiles were removed in vac.; as oil; | 99% |
Conditions | Yield |
---|---|
With Bradyrhizobium japonicum strain USDA110 nitrilase bll6402 In phosphate buffer at 30℃; for 24h; pH=7.2; | 97% |
With potassium phosphate buffer; nitrilase from Alcaligenes faecalis ATCC8750 at 30℃; for 53h; pH=7.3; | 90% |
With Arabidopsis thaliana nitrilase In methanol for 19h; pH=8.5; | 3.92% |
With potassium phosphate buffer; diothiothreitol at 30℃; Rhodococcus rhodochrous K22 nitrilase; | |
With hydrogenchloride 1) microbial hydrolysis by Comamonas testosteroni 5-MGAM-4D, ATCC 55744; pH 7.0 (potassium phosphate buffer), 27 deg C, 86 h; 2) pH 2.5; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 1.1% B 97% |
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 1.3% B 90.1% |
With ammonium hydroxide; hydrogen In water; isopropyl alcohol at 130℃; under 41254.1 Torr; for 4h; Autoclave; | A 9% B 90% |
With hydrogen; iron catalyst at 140℃; under 233483 Torr; |
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen In propan-1-ol; water at 60 - 70℃; under 375.038 Torr; for 18h; Flow reactor; | 97% |
Stage #1: hexanedinitrile With ammonium hydroxide; hydrogen In water; isopropyl alcohol at 140℃; under 37503.8 Torr; for 3h; Autoclave; Stage #2: With hydrogenchloride In methanol | 95% |
Stage #1: hexanedinitrile With fac-[Mn(1,2-bis(di-n-propylphosphino)ethane)(CO)3(CH3)]; hydrogen In toluene at 100℃; under 37503.8 Torr; for 48h; Autoclave; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 95% |
hexanedinitrile
m-Fluorobenzonitrile
2-(3-fluorophenyl)-6,7-dihydro-5H-cyclopentapyrimidin-4-ylamine
Conditions | Yield |
---|---|
With potassium tert-butylate In para-xylene at 120℃; for 4h; Inert atmosphere; | 96% |
hexanedinitrile
((1,2-bis(diisopropylphosphino)ethane)NiH)2
[(1,2-bis(diisopropylphosphano)ethane)Ni(η2-N,C-(CH2)4-CN)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: H2; under Ar, in glove box; ((dippe)NiH)2 dissolved in dry THF at room temp., 2 equiv. of dinitrile added, mixt. stirred for 15 min; evapd. under vac., residue dried under vac. for 6 h; | 95% |
Conditions | Yield |
---|---|
With hydrogenchloride In benzene at 15℃; | 94% |
With hydrogenchloride beim anschliessend Feuchtigkeitsausshluss; | |
With hydrogenchloride In diethyl ether | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; tris-(dibenzylideneacetone)dipalladium(0); 2,2,2-trifluoroacetic acid ammonia; trifluoroacetic acid In methanol at 90℃; for 48h; Schlenk technique; | 93% |
Conditions | Yield |
---|---|
With water at 150℃; under 5171.62 - 6205.94 Torr; for 1.5h; Inert atmosphere; Microwave irradiation; | 92% |
With hydrogenchloride; diethyl ether at -20℃; Versetzen des Reaktionsprodukts mit 1 Mol Wasser und Behandeln des erhaltenen Hydrochlorids mit wss.Natriumcarbonat-Loesung; | |
With basic ion exchanger; water at 75℃; |
allyl iodid
hexanedinitrile
(+/-)-1-allyl-2-oxo-1-cyclopentanecarbonitrile
Conditions | Yield |
---|---|
Stage #1: hexanedinitrile Thorpe-Ziegler reaction; Stage #2: allyl iodid | 92% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel; sodium hydroxide In methanol; water at 30 - 60℃; | 90% |
With hydrogen In ethanol at 75℃; under 1500.15 - 15001.5 Torr; for 3h; | 80% |
With ammonia; hydrogen In toluene at 120℃; under 22502.3 Torr; for 16h; Autoclave; | 75% |
hexanedinitrile
<2,2,5,5-2H4>adiponitrile
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; water-d2 at 70℃; for 24h; Inert atmosphere; | 90% |
With water-d2; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane for 24h; Heating; | 70% |
With deuteromethanol; sodium methylate | |
With water-d2; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane at 100℃; for 2h; |
hexanedinitrile
(+/-)-1-methyl-2-oxo-1-cyclopentanecarbonitrile
Conditions | Yield |
---|---|
Stage #1: hexanedinitrile Thorpe-Ziegler reaction; Stage #2: methylating agent | 90% |
4-Cyanochlorobenzene
hexanedinitrile
2-(4-chlorophenyl)-6,7-dihydro-5H-cyclopentapyrimidin-4-ylamine
Conditions | Yield |
---|---|
With potassium tert-butylate In para-xylene at 120℃; for 4h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; palladium(II) trifluoroacetate; water; trifluoroacetic acid In tetrahydrofuran at 80℃; for 36h; Inert atmosphere; Schlenk technique; | 90% |
With 1,10-Phenanthroline; water; palladium diacetate; trifluoroacetic acid In 2-methyltetrahydrofuran at 80℃; for 48h; Inert atmosphere; Schlenk technique; | 89% |
Conditions | Yield |
---|---|
With water In 1,2-dimethoxyethane at 160℃; for 18h; amidation; | 89% |
Conditions | Yield |
---|---|
With diphosphorus pentasulfide In toluene at 90℃; for 10h; thio-Pinner's reaction; | 89% |
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