CAS No.506-77-4,Cyanogen chloride Suppliers

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Synthetic route

: 7677-24-9
trimethylsilyl cyanide

A: 75-77-4
chloro-trimethyl-silane

B: 506-77-4
cyanogen chloride

C S, SO2: S, SO2

Conditions

Conditions	Yield
With thionyl chloride at 30 - 40℃; Product distribution; oth. reagent (SO2Cl2);	A 100% B 45% C n/a

...Expand

: 460-19-5
ethanedinitrile

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In water (CN)2/Cl2 = 1:1, at 560°C, in 10% CaCl2 soln.; cool and crystn. at -10°C;	100%
With chlorine In gas at 900K;	93%
With chlorine In gas at 1100K;	89%

: 773837-37-9
sodium cyanide

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In water continuous method, 15% NaCN soln.;	98.4%
With chlorine In neat (no solvent) alkali cyanides, liquid Cl2 mixed in autoclave at -30°C;	95%
With chlorine In hydrogenchloride at 0°C; distn.;	90%

: dipotassium tetracyanozincate(II)

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In water byproducts: KCl, ZnCl2; in suspension, 60-90 min. at room temp.; drying above CaCl2 and freezing with ice/NaCl or CO2/acetone mixt.; >99.9% pure;	98%
With chlorine In not given byproducts: ZnCl2, KCl; at 0-5°C; product sepd. below 45°C;
With Cl2 In not given byproducts: ZnCl2, KCl; at 0-5°C; product sepd. below 45°C;
With Cl2 In not given byproducts: ZnCl2, KCl; at 0-5°C; product sepd. below 45°C;

: 2Na(1+)*{Zn(CN)4}(2-)=Na2{Zn(CN)4}

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In water byproducts: NaCl, ZnCl2; in suspension, 60-90 min. at room temp.; drying above CaCl2 and freezing with ice/NaCl or CO2/acetone mixt.; >99.9% pure;	98%
With chlorine In not given byproducts: ZnCl2, NaCl; at 0-5°C; product sepd. below 45°;
With Cl2 In not given byproducts: ZnCl2, NaCl; at 0-5°C; product sepd. below 45°;
With Cl2 In not given byproducts: ZnCl2, NaCl; at 0-5°C; product sepd. below 45°;

: Ca(2+)*Zn(CN)4(2-)=CaZn(CN)4

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In water byproducts: CaCl2, ZnCl2; in suspension, 60-90 min. at room temp.; drying above CaCl2 and freezing with ice/NaCl or CO2/acetone mixt.; >99.9% pure;	98%
With chlorine In not given byproducts: ZnCl2, CaCl2; at 0-5°C; product sepd. below 45°C;
With Cl2 In not given byproducts: ZnCl2, CaCl2; at 0-5°C; product sepd. below 45°C;
With Cl2 In not given byproducts: ZnCl2, CaCl2; at 0-5°C; product sepd. below 45°C;

: 57-12-5
cyanide(1-)

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In tetrachloromethane with alkali cyanides, under 3°C;	98%
With chlorine In neat (no solvent) alkali cyanides, at -18°C;	85%
With chlorine In neat (no solvent) alkali cyanides mixed with sand at 3°C;	80%
With chlorine In tetrachloromethane alkali cyanides, at 0°C;
With hydrogenchloride In not given

: 330660-35-0
silver cyanide

: 7791-21-1
hypochlorous anhydride

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
In neat (no solvent) in closed U-tube, at room temp., AgCN free from water; fract. distn. at -78°C; pure prod.;	95%

: 74-90-8
hydrogen cyanide

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With hydrogenchloride; dihydrogen peroxide; iron(III) In water at 50-65°C, continuous method;	90%
With hydrogenchloride; dihydrogen peroxide; copper(II) ion In water at 50-65°C, continuous method;	90%
With dihydrogen peroxide In water at 30°C;	15%

: 57-12-5
cyanide(1-)

A: 74-90-8
hydrogen cyanide

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In hydrogenchloride alkali cyanides, pH=9;	A n/a B 90%

: 24331-09-7
tetracyanomethane

A: Lithium-tricyan-methanid

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With lithium chloride In acetonitrile 2h in vacuum at room temp. with mixing; fract. cond.;	A n/a B 79%

: 78707-99-0
perfluoro-(2-chloro-5-methyl-4-oxa-2,5-diazahexane)

A: 460-49-1
trifluoromethyl isocyanate

B: 38592-11-9
perfluoro-<1-(dimethylamino-oxy)-2-azapropene>

C: 38592-13-1
2H-octafluoro-5-trifluoromethyl-4-oxa-2,5-diazahexane

D: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With silver cyanide for 89h; Product distribution; Ambient temperature; other reagents;	A n/a B 54% C 30% D n/a

...Expand

: 106735-59-5, 106818-70-6
CCl2F5NOS

A: 106735-60-8
sulfur cyanate pentafluoride

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With mercury at 25℃; ultra sound;	A 10% B n/a

: 2972-96-5
1,2-dichloro-1,1,2,2-tetranitroethane

: 151-50-8
potassium cyanide

: 506-77-4
cyanogen chloride

: 2,4-dichloro-2-cyano-acetoacetic acid ethyl ester

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
Zersetzung;

: 302-04-5
Thiocyanate

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine
With chlorine In not given pH<11;

: 143-33-9
sodium cyanide

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With tetrachloromethane; chlorine; acetic acid at -10 - -5℃;
With tetrachloromethane; water; chlorine
With hydrogenchloride; water Electrolysis.an einer Graphitanode;

: 92114-96-0
mercury fulminate

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With aluminium trichloride in Gegenwart von aromatischen Kohlenwasserstoffen;

: 151-50-8
potassium cyanide

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With hydrogenchloride; water
With chlorine at 0℃;
With water; chlorine; zinc(II) sulfate at 0℃;
With chloroamine; water

: 7677-24-9
trimethylsilyl cyanide

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With tellurium chloride pentafluoride at -55 - 25℃;

: 7677-24-9
trimethylsilyl cyanide

A: 420-56-4
trimethylsilyl fluoride

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With tellurium chloride pentafluoride at -55 - 25℃;

: 7677-24-9
trimethylsilyl cyanide

A: 420-56-4
trimethylsilyl fluoride

B: 3313-35-7
thionyl cyanide

C: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With pentafluorosulfanyl chloride at -10℃; for 2h; Product distribution;

...Expand

: 150-30-1
Phenylalanine

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With sodium hypochlorite; Ammonium In water for 1h; Product distribution; Ambient temperature; other aromatic amines;

: (trifluoromethyl)chlorodicyanodifluorosulfur(VI)

A: 690-24-4
cyan-trifluoromethylsulfane

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
at 25℃; for 42h;

: 50-00-0
formaldehyd

A: 245520-53-0
N-chloroaminomethanol

B: N-chlorodimethanolamine

C: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chloroamine In phosphate buffer at 25℃; Kinetics; Equilibrium constant; Addition;

...Expand

: 73-40-5
2-amino-1,9-dihydro-6H-purin-6-one

: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In phosphate buffer for 0.5h; pH=7.0; Chlorination;

: 921-01-7, 3374-22-9, 4371-52-2, 40143-64-4, 40143-66-6, 40143-69-9, 52-90-4
rac-cysteine

A: 131543-46-9
Glyoxal

B: 3018-12-0
dichloroacetonitrile

C: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In phosphate buffer for 0.5h; pH=7.0; Chlorination;

...Expand

: 3130-87-8
ASPARAGINE

A: 3018-12-0
dichloroacetonitrile

B: N-chloroiminoacetonitrile

C: dichloroaminoacetonitrile

D: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In phosphate buffer for 0.5h; pH=7.0; Chlorination;

...Expand

: 71-30-7
Cytosine

A: 3018-12-0
dichloroacetonitrile

B: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In phosphate buffer for 0.5h; pH=7.0; Chlorination;

: 66-22-8
uracil

A: 67-66-3
chloroform

B: 3018-12-0
dichloroacetonitrile

C: 506-77-4
cyanogen chloride

Conditions

Conditions	Yield
With chlorine In phosphate buffer for 0.5h; pH=7.0; Chlorination;

...Expand

: 109-77-3
malononitrile

: 506-77-4
cyanogen chloride

: 36603-80-2
sodium tricyanomethanide

Conditions

Conditions	Yield
With phosphoric acid; sodium hydroxide In methanol; water at 25 - 30℃; for 3.5h; pH=7.0 - 7.2; Product distribution / selectivity;	100%
With ethanol; sodium

: 2492-26-4
sodium 2-mercaptobenzothiazole

: 506-77-4
cyanogen chloride

: 6011-99-0
benzo[d]thiazol-2-yl thiocyanate

Conditions

Conditions	Yield
Ambient temperature;	100%
With water
With ethanol
With ethanol
With water

: 5700-53-8
N-cyclohexylethylenediamine

: 506-77-4
cyanogen chloride

: 51099-11-7
1-cyclohexyl-2-iminoimidazolidine hydrochloride

Conditions

Conditions	Yield
In benzene for 3h;	100%

: 106-49-0
p-toluidine

: 506-77-4
cyanogen chloride

: 10532-64-6
N-(4-methylphenyl)cyanamide

Conditions

Conditions	Yield
With trimethylamine Ambient temperature;	100%

: 106-47-8
4-chloro-aniline

: 506-77-4
cyanogen chloride

: 13463-94-0
N-(4-chlorophenyl)cyanamide

Conditions

Conditions	Yield
With trimethylamine Ambient temperature;	100%
With sodium hydroxide In water; acetic acid	84%

: 104-94-9
4-methoxy-aniline

: 506-77-4
cyanogen chloride

: 13519-16-9
N-(4-methoxyphenyl)cyanamide

Conditions

Conditions	Yield
With trimethylamine Ambient temperature;	100%

: 1122-93-6
potassium p-methoxyphenolate

: 506-77-4
cyanogen chloride

: 2983-74-6
4-methoxyphenyl cyanate

Conditions

Conditions	Yield
Ambient temperature;	100%

: 15091-70-0
2-mercaptobenzoxazole sodium salt

: 506-77-4
cyanogen chloride

: 5285-95-0
2-thiocyanato-benzooxazole

Conditions

Conditions	Yield
Ambient temperature;	100%

: 1194-62-3
6-mercaptopurine sodium salt

: 506-77-4
cyanogen chloride

: 19447-73-5
6-thiocyanato-9H-purine

Conditions

Conditions	Yield
Ambient temperature;	100%

: 506-77-4
cyanogen chloride

: 58289-71-7
2-mercaptopyrimidine sodium salt

: 89283-87-4
2-thiocyanatopyrimidine

Conditions

Conditions	Yield
Ambient temperature;	100%

: Potassium; 3,4-dimethoxy-phenolate

: 506-77-4
cyanogen chloride

: 220075-82-1
4-cyanato-1,2-dimethoxy-benzene

Conditions

Conditions	Yield
Ambient temperature;	100%

: 75-05-8
acetonitrile

: 506-77-4
cyanogen chloride

: 1973-04-2
2,4-dichloro-6-methyl-1,3,5-triazine

Conditions

Conditions	Yield
With hydrogenchloride; aluminum (III) chloride In water; 1,2-dichloro-ethane at -5 - 5℃; for 8h; Reagent/catalyst; Solvent;	99%
With hydrogenchloride; aluminum (III) chloride In dichloromethane at -5 - 5℃; under 750.075 Torr; for 12h;

: 58765-11-0
4-hydroxybenzaldehyde potassium salt

: 506-77-4
cyanogen chloride

: 1126-84-7
4-cyanatobenzaldehyde

Conditions

Conditions	Yield
Ambient temperature;	98%

: silver hexafluoroantimonate

: 506-77-4
cyanogen chloride

: 117504-97-9
bis(cyanogen chloride-N)silver(I) hexafluoroantimonate(V)

Conditions

Conditions	Yield
In sulfur dioxide N2, exclusion of light, stirred for 12 h at room temp.;; filtrated, SO2 removed in vacuo, elem. anal.;	98%

: 66608-52-4
4-(propylthio)-1,2-phenylenediamine

: 506-77-4
cyanogen chloride

: 6-(propylthio)-1H-benzo[d]imidazol-2-amine

Conditions

Conditions	Yield
With sodium hydroxide In methanol at 3 - 45℃; for 2h; pH=4; pH-value; Temperature;	95.21%

: 82385-77-1
N-(methoxycarbonylmethyl)-N'-methoxydiazene-N-oxide

: 506-77-4
cyanogen chloride

: (N'-methoxydiazene-N-oxido)cyanoacetic acid methyl ester

Conditions

Conditions	Yield
With sodium hydride In tetrahydrofuran; hexane 1.) -10 - -5 deg C, 30 min, 2.) -50 deg C to 20 deg C, 1 h;	95%

: 542-92-7
cyclopenta-1,3-diene

: 506-77-4
cyanogen chloride

: 49805-30-3
2-azabicyclo[2.2.1.]hept-5-en-3-one

Conditions

Conditions	Yield
With sodium hydroxide In methanol at 0 - 5℃; for 8h; pH=4 - 5; Diels-Alder Cycloaddition;	95%

: 101990-44-7
N'-((6-chloropyridin-3-yl)methyl)ethane-1,2-diamine

: 506-77-4
cyanogen chloride

: 115970-17-7
Desnitro-imidacloprid

Conditions

Conditions	Yield
In water at 20℃; for 3h;	94.2%

: 420-04-2
CYANAMID

: 506-77-4
cyanogen chloride

A: 76989-89-4
sodium N-cyanoisourea

B: 1934-75-4
sodium dicyanamide

C: 7647-14-5
sodium chloride

Conditions

Conditions	Yield
With sodium hydroxide In water at 70 - 75℃; under 1050.11 Torr; pH=7.2 - 8.0; Purification / work up;	A n/a B 94% C n/a

...Expand

: 7647-18-9
antimonypentachloride

: 506-77-4
cyanogen chloride

: 22538-93-8, 24273-94-7
SbCl5(ClCN)

Conditions

Conditions	Yield
In neat (no solvent) under N2, excess of CN-compd. was condensed onto SbCl5 at -196 °C, mixt. was allowed to warm to room temp.; recrystn. from SO2, elem. anal.;	94%

: (η5-C5H5)2Ti(AsF6)2

: 506-77-4
cyanogen chloride

: (C5H5)2Ti(NCCl)2(2+)*2AsF6(1-)=(C5H5)2Ti(NCCl)2(AsF6)2

Conditions

Conditions	Yield
In sulfur dioxide (strictly anhydrous conditions, N2) SO2 was condensed in vessel with complex at -196°C, allowed to warm to room temp., cooled using liquid N2, 5-fold excess of ClCN was condensed in, warmed to room temp., stirred for 30 min; SO2 and ClCN were removed;	94%

: 25932-11-0
benzenesulfinic acid sodium dihydrate

: 506-77-4
cyanogen chloride

: 24224-99-5
benzenesulfonyl cyanide

Conditions

Conditions	Yield
In dichloromethane; water	93.8%

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