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inquiryCAS: 4048-33-3 MF: C6H15NO MW: 117.19 EINECS: 223-748-1 Mol File: 4048-33-3.mol Appearance: light yell
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inquiry6-Amino-1-hexanol CAS:4048-33-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
MolecularWeight: 118.1968 MolecularFormula: C6H16NO … Package:aluminium foil bag Application:Pharmaceutical and research. Transportation:No special requirement. Port:Suzhou
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 6-Amino-1-Hexanol CAS No.: 4048-33-3 Molecule Formula:C6H15NO Molecule Weight:117.19 Purity: 99.0% Package: 25kg/drum Description:White to off-white powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiry6-Amino-1-hexanol Chemical Properties Melting point 54-58 °C (lit.) Boiling point 135-140 °C/30 mmHg (lit.) density 0.8872 (estimate) refractive index 1.4444 (estimate) Fp 133 °C storage temp. Store at 0-5°C pk
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inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiry6-amino-1-hexanolAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Conditions | Yield |
---|---|
Stage #1: 6-aminohexanoic acid With sodium tetrahydroborate at 40℃; for 0.333333h; Sonication; Stage #2: In ethylene glycol at 90℃; for 16.5h; Reflux; Stage #3: With water In ethylene glycol Temperature; | 96% |
With sodium tetrahydroborate; iodine In tetrahydrofuran |
N-benzyloxycarbonyl-6-amino-1-hexanol
6-amino-1-hexanol
Conditions | Yield |
---|---|
With lithium borohydride; chloro-trimethyl-silane In tetrahydrofuran for 24h; Ambient temperature; | 95% |
With hydrogen bromide for 4h; | 79% |
Conditions | Yield |
---|---|
Stage #1: caprolactam With sodium hydroxide In toluene at 80℃; Stage #2: In toluene at 100℃; for 16h; Stage #3: With ammonium chloride for 0.25h; Temperature; | 87.2% |
With [RuCl2(Ph2PCH2CH2NH2)2]; potassium tert-butylate; hydrogen; zinc(II) trifluoroacetate In 1,4-dioxane at 100℃; under 22502.3 Torr; for 18h; Inert atmosphere; Autoclave; | 77% |
With ethanol; sodium |
N-CO2CH3-6-amino-1-hexanol
6-amino-1-hexanol
Conditions | Yield |
---|---|
With hydrogenchloride In water for 3h; Reflux; | 85% |
Conditions | Yield |
---|---|
With carbonylchloro[4,5-bis(diisopropylphosphinomethyl)acridine]hydridoruthenium(II) In 1,4-dioxane; water at 100℃; for 40h; Schlenk technique; Inert atmosphere; | A 70% B 10% |
6-(Boc-amino)-1-hexanol
6-amino-1-hexanol
Conditions | Yield |
---|---|
With trifluoroacetic acid at 20℃; for 12h; | 65% |
6-azidohexan-1-ol
6-amino-1-hexanol
Conditions | Yield |
---|---|
With aluminum oxide; potassium hydroxide; hydrazine In neat (no solvent) for 1h; Milling; | 60% |
1,6-hexanediol
A
hexamethylene imine
B
1,6-Hexanediamine
C
6-amino-1-hexanol
Conditions | Yield |
---|---|
With ammonia; hydrogen In water at 180℃; under 7500.75 - 27752.8 Torr; for 4h; Reagent/catalyst; Solvent; Pressure; Time; | A 19.5% B 23.4% C 17% |
With ammonia; chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) In toluene at 155℃; under 25502.6 Torr; for 12h; Autoclave; Inert atmosphere; | |
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics; Reagent/catalyst; | A 66.5 %Chromat. B 21.2 %Chromat. C 6.5 %Chromat. |
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics; Reagent/catalyst; | A 7.5 %Chromat. B 17.6 %Chromat. C 68.8 %Chromat. |
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; Kinetics; | A 23 %Chromat. B 31.3 %Chromat. C 19.1 %Chromat. |
Conditions | Yield |
---|---|
With water; cobalt at 210℃; | |
With water at 280℃; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
6-acetoxy-hexanenitrile
6-amino-1-hexanol
Conditions | Yield |
---|---|
With ammonia; nickel at 140℃; under 95616 Torr; Hydrogenation.beim Erhitzen des Reaktionsprodukts mit wss. Natronlauge; |
6-acetoxy-hexanenitrile
A
6-amino-1-hexanol
B
acetic acid-(6-amino-hexyl ester)
Conditions | Yield |
---|---|
With ammonia; nickel at 140℃; under 95616 Torr; |
1,6-Hexanediamine
A
hexamethylene imine
B
6-amino-1-hexanol
C
2-Methylpiperidin
Conditions | Yield |
---|---|
With water at 300℃; for 15h; Rate constant; | A 37 % Chromat. B n/a C 2 % Chromat. |
A
2-(tetrahydrofuran-2-yl)ethylamine
B
6-amino-1-hexanol
Conditions | Yield |
---|---|
With sodium hydroxide; ethanol; nickel under 88260.9 Torr; Hydrogenation; |
6-amino-1-hexanol
Conditions | Yield |
---|---|
With platinum under 1140 - 1520 Torr; Hydrogenation; |
1-hydroxy-6-((4-methoxyphenyl)-diphenylmethylamino)-hexane
6-amino-1-hexanol
Conditions | Yield |
---|---|
With sodium periodate In acetone at 20℃; for 16h; |
5-chloropentyl acetate
6-amino-1-hexanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium iodide; acetone / beim Erwaermen des Reaktionsprodukts mit Kaliumcyanid in wss. Aethanol 2: Raney nickel; ammonia / 140 °C / 95616 Torr / Hydrogenation.beim Erhitzen des Reaktionsprodukts mit wss. Natronlauge View Scheme | |
Multi-step reaction with 2 steps 1: sodium iodide; acetone / beim Erwaermen des Reaktionsprodukts mit Kaliumcyanid in wss. Aethanol 2: Raney nickel; ammonia / 140 °C / 95616 Torr View Scheme |
4-((6-hydroxyhexylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate
A
6-amino-1-hexanol
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium dichloride; ascorbic acid In d(4)-methanol for 4h; Photolysis; Inert atmosphere; | A 98 %Spectr. B n/a |
Conditions | Yield |
---|---|
With ammonia; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); 1,1,1-tris(diethylphosphinomethyl)ethane In toluene at 155℃; under 31503.2 Torr; for 12h; Product distribution / selectivity; Autoclave; | |
With ammonia; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); bis(2-diphenylphosphinoethyl)phenylphosphine In toluene at 155℃; under 30003 Torr; for 12h; Product distribution / selectivity; Inert atmosphere; | |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In toluene at 155℃; under 31503.2 Torr; for 12h; Inert atmosphere; Autoclave; | |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In toluene at 155℃; under 31503.2 Torr; for 12h; Pressure; Reagent/catalyst; Autoclave; Inert atmosphere; |
Conditions | Yield |
---|---|
With ammonia; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 155℃; under 27002.7 Torr; for 12h; Product distribution / selectivity; Inert atmosphere; | |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 155℃; under 27002.7 Torr; for 12h; Inert atmosphere; Autoclave; | |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 155℃; under 27002.7 Torr; for 12h; Pressure; Reagent/catalyst; Autoclave; Inert atmosphere; |
N-methyl N'-(6'-hydroxyhexyl)phthalicdiamide
methylamine
A
6-amino-1-hexanol
B
N1,N2-dimethylphthalamide
Conditions | Yield |
---|---|
In water at 20℃; for 0.166667h; Temperature; Reagent/catalyst; |
Conditions | Yield |
---|---|
With tris(2-carboxyethyl)phosphine; water In aq. phosphate buffer; water-d2 for 0.0833333h; |
5-hydroxymethylfuran-2-ylmethylamine
6-amino-1-hexanol
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran at 30℃; under 2250.23 Torr; for 72h; |
6-amino-1-hexanol
Conditions | Yield |
---|---|
With rhenium on alumina; hydrogen In dichloromethane at 90℃; under 13501.4 Torr; for 12h; |
n-Pent-4-enyl alcohol
carbon monoxide
benzylamine
A
6-amino-1-hexanol
B
7-azatridecane-1,13-diol
Conditions | Yield |
---|---|
Stage #1: n-Pent-4-enyl alcohol; carbon monoxide; benzylamine With C20H22N2ORh(1+)*C24H20B(1-); hydrogen In toluene at 85℃; under 37503.8 Torr; for 6h; Stage #2: With palladium 10% on activated carbon; hydrogen In ethanol at 75℃; under 3750.38 Torr; for 24h; |
Conditions | Yield |
---|---|
In dichloromethane for 12h; | 100% |
With triethylamine In tetrahydrofuran | 100% |
In dichloromethane at 0 - 20℃; for 15h; | 100% |
6-amino-1-hexanol
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
(9H-fluoren-9-yl)methyl (6-hydroxyhexyl)carbamate
Conditions | Yield |
---|---|
With pyridine In methanol at 23℃; for 16h; | 100% |
With pyridine In methanol at 23℃; | |
With sodium carbonate In 1,4-dioxane; water at 20℃; for 0.5h; | 11 g |
Conditions | Yield |
---|---|
With triethylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran | 100% |
Conditions | Yield |
---|---|
Reflux; | 100% |
for 20h; Reflux; | 27% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; ammonium acetate; hydrogen In methanol at 20℃; under 760.051 Torr; for 34h; | 100% |
6-amino-1-hexanol
6-bromo-1-aminohexane hydrobromide
Conditions | Yield |
---|---|
With hydrogen bromide In water for 3h; Inert atmosphere; Reflux; | 100% |
With hydrogen bromide In water at 0 - 100℃; for 24h; | 94% |
With hydrogen bromide at 0 - 80℃; for 20h; | 61% |
With hydrogen bromide In water for 20h; Reflux; | |
With hydrogen bromide at 0 - 80℃; for 20h; |
6,9-dichloro-1,2,3,4-tetrahydroacridine
6-amino-1-hexanol
6-((6-chloro-1,2,3,4-tetrahydroacridin-9-yl)amino)hexan-1-ol
Conditions | Yield |
---|---|
Stage #1: 6,9-dichloro-1,2,3,4-tetrahydroacridine In phenol at 105℃; for 0.5h; Stage #2: 6-amino-1-hexanol In phenol at 105℃; for 20h; | 100% |
In pentan-1-ol for 48h; Reflux; | 52% |
(R)-8-(benzyloxy)-5-(2-bromo-1-((tert-butyldimethylsilyl)oxy)ethyl)quinolin-2(1H)-one
6-amino-1-hexanol
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 80℃; for 18h; | 100% |
In 1-methyl-pyrrolidin-2-one at 80℃; for 18h; | 100% |
6-amino-1-hexanol
tert-butyldimethylsilyl chloride
6-((tert-butyldimethylsilyl)oxy)hexan-1-amine
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 18h; | 99.3% |
With dmap In dichloromethane at 20℃; for 15h; | 95% |
In pyridine | 86% |
With 1H-imidazole In N,N-dimethyl-formamide Ambient temperature; | 11.2 g |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropane)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 19h; | 99% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 760.051 Torr; for 46h; | 99% |
6-amino-1-hexanol
2-adamantanecarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 99% |
6-amino-1-hexanol
2,2,2-trifluoroethyl benzoate
6-aminohexyl benzoate
Conditions | Yield |
---|---|
With FeIII-salen In toluene at 120℃; for 2h; | 99% |
With [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene In tetrahydrofuran at 20℃; for 24h; Reagent/catalyst; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With dihydroxy-methyl-borane; water In o-xylene for 12h; Molecular sieve; Reflux; chemoselective reaction; | 99% |
6-amino-1-hexanol
di-tert-butyl dicarbonate
2,2,2-trifluoroethyl benzoate
6-((tert-butoxycarbonyl)amino)hexyl benzoate
Conditions | Yield |
---|---|
Stage #1: 6-amino-1-hexanol; 2,2,2-trifluoroethyl benzoate With (μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)] In toluene at 120℃; for 2h; Inert atmosphere; Schlenk technique; Stage #2: di-tert-butyl dicarbonate With triethylamine In dichloromethane at 4 - 20℃; for 4h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; dimethyl sulfoxide Cooling with ice; | 99% |
Conditions | Yield |
---|---|
With CaCl2 buffer; sodium acetate; acetic acid In chloroform at 30℃; for 4h; phospholipase D from Streptomyces sp., pH 6.5; | 98% |
6-amino-1-hexanol
(fluorenylmethoxy)carbonyl chloride
(9H-fluoren-9-yl)methyl (6-hydroxyhexyl)carbamate
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane at 0 - 25℃; for 12h; | 98% |
With sodium carbonate In 1,4-dioxane; water at 0 - 20℃; for 1h; | 97% |
With sodium hydrogencarbonate In 1,4-dioxane at 0 - 20℃; | 95% |
6-amino-1-hexanol
tert-butylchlorodiphenylsilane
1-O-(tert-butyldiphenylsilanyl)-6-hexylamine
Conditions | Yield |
---|---|
In pyridine for 16h; | 98% |
With 1-methyl-1H-imidazole; iodine In dichloromethane at 20℃; for 0.0833333h; | 93% |
With 1-methyl-1H-imidazole; iodine In dichloromethane at 20℃; for 0.0833333h; | 93% |
With pyridine |
6-amino-1-hexanol
trifluoroacetic anhydride
6-trifluoroacetamido-1-hexanol
Conditions | Yield |
---|---|
With triethylamine In methanol for 16h; | 98% |
With triethylamine In methanol at 0 - 20℃; Inert atmosphere; | 92% |
With triethylamine In dichloromethane at 20℃; for 12h; Inert atmosphere; Cooling with ice; |
6-amino-1-hexanol
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-5-(6-hydroxyhexylaminocarbonyl)-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 98% |
6-amino-1-hexanol
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N'-bis(6-hydroxyhexyl)perylene-3,4:9,10-bis(dicarboximide)
Conditions | Yield |
---|---|
With 1H-imidazole at 150℃; for 36h; | 98% |
With zinc acetate dehydrate In N,N-dimethyl acetamide at 110 - 160℃; for 18h; Inert atmosphere; | 86% |
In ethylene glycol at 140℃; for 16h; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at 20℃; for 1h; Inert atmosphere; | 98% |
6-amino-1-hexanol
2-Isocyanatoethyl methacrylate
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 2.25h; | 98% |
6-amino-1-hexanol
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride
Conditions | Yield |
---|---|
With 1H-imidazole at 180℃; for 5h; | 98% |
With 1H-imidazole at 150℃; for 6h; | |
With 1H-imidazole; N,N-dimethyl acetamide; zinc diacetate | |
With 1H-imidazole; zinc diacetate; p-dimethylaminocinnamaldehyde | |
With 1H-imidazole; N,N-dimethyl acetamide; zinc diacetate |
Conditions | Yield |
---|---|
In toluene for 6h; Reflux; Dean-Stark; | 98% |
Conditions | Yield |
---|---|
for 0.0333333h; Condensation; Irradiation; | 97% |
In toluene Reflux; | 96% |
at 160℃; for 0.0833333h; Microwave irradiation; | 94% |
6-amino-1-hexanol
2,4-Dinitrofluorobenzene
6-(2,4-dinitrophenylamino)hexan-1-ol
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane at 20℃; for 1h; | 97% |
In methanol for 12h; | 54% |
6-amino-1-hexanol
5-(dimethylamino)naphth-1-ylsulfonyl chloride
5-(dimethylamino)-N-(6-hydroxyhexyl)-1-naphthalenesulfonamide
Conditions | Yield |
---|---|
With sodium carbonate In tetrahydrofuran; water at 20℃; for 0.5h; | 97% |
With triethylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 7h; | 94% |
With triethylamine In dichloromethane at 20℃; for 16h; Darkness; | 68.5% |
With triethylamine In dichloromethane at 20℃; |
6-amino-1-hexanol
6-azidohexan-1-ol
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium hydrogencarbonate; perfluorobutanesulfonyl azide In methanol; diethyl ether; water at 20℃; for 6h; | 97% |
With sodium azide; copper(ll) sulfate pentahydrate; trifluoromethylsulfonic anhydride; potassium carbonate In methanol; dichloromethane; water at 20℃; for 48h; | 90% |
With triflic azide; sodium hydrogencarbonate; copper(II) sulfate In methanol; toluene at 20℃; for 14h; | 52% |
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