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inquiryProduct name: Fmoc-CL . Synonym:1-(9-fluorenyl)methylchloroformate;chloroformic acid-9-fluorenyl methyl ester;9-FluorenylmethoxycarbonylChloride CAS No: 28920-43-6. Molecular formula: C15H11ClO2. Molecular weight: 258.7. Appearance: Off-w
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inquiryItems Standard Result Appearance white to off-white microcrystalline powder White to off-white microcrystalline powder
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inquiryHebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ
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inquiryHigh quality 9-Fluorenylmethyl chloroformate CAS 28920-43-6 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates,
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inquiryProduct description: Product name 9-Fluorenylmethyl chloroformate CAS number 28920-43-6 Assay ≥99% Appearance White crystalline powder Capacity 200mt/year Application For sol
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry9-Fluorenylmethyl chloroformate Basic information Product Name: 9-Fluorenylmethyl chloroformate Synonyms: 1-(9-fluorenyl)methylchloroformate;chloro-formicacifluoren-9-ylmethylester;Formi
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inquiryDensity: 1.1780 (rough estimate) Melting point: 62-64 ° C (lit.) Boiling point: 365.79 ° C (rough estimate) Flash point: 143.6 ° C Steam pressure: 2.06E-06mmHg at 25 ° C Solubility: dioxane: 0.1g/mL, clear, colorless Refractive index:
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inquiryAppearance:White or light yellow crystalline powder Storage:R.T Package:25kg/drum Application:Organic Synthesis Transportation:Express/Sea/Air Port:Any port in China
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiry9-Fluorenylmethyl chloroformate CAS:28920-43-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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bis(trichloromethyl) carbonate
9-Fluorenylmethanol
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With tributyl-amine In toluene at 0℃; Reagent/catalyst; Solvent; Temperature; | 98% |
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | |
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | |
With tributyl-amine In toluene at 0℃; for 0.0666667h; Temperature; Flow reactor; | 98 %Chromat. |
With pyridine In toluene at 0 - 20℃; |
Conditions | Yield |
---|---|
In dichloromethane | 74% |
In dichloromethane | |
With pyridine In diethyl ether 1.) 1 h, 0 deg C, 2.) 8 h, 25 deg C; | |
With pyridine In tetrahydrofuran at 0 - 6℃; for 13.5h; Temperature; Large scale; |
9H-fluorene
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 25 percent 2: 74 percent / CH2Cl2 View Scheme |
Conditions | Yield |
---|---|
In tetrahydrofuran; water | 37.9 g (95.8%) |
9-Fluorenylmethanol
trichloromethyl chloroformate
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With dmap In toluene at 20℃; for 24h; |
Fmoc-OH
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In N,N-dimethyl-formamide at 83℃; for 2h; |
Conditions | Yield |
---|---|
With oxygen In acetonitrile at 20℃; for 3h; Irradiation; |
D-Threonine
(fluorenylmethoxy)carbonyl chloride
(((9H-fluoren-9-yl)methoxy)carbonyl)-D-threonine
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane | 100% |
4-aminophenylacetic acid
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With sodium carbonate for 16h; | 100% |
(fluorenylmethoxy)carbonyl chloride
(RS)-1-amino-2-methylpropylphosphinic acid
(1RS)-1-(N-(9-fluorenylmethoxycarbonyl)amino)-2-methylpropylphosphinic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water at 4℃; for 6h; | 100% |
(fluorenylmethoxy)carbonyl chloride
N-Boc-1,3-diaminopropane
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 20℃; | 100% |
With sodium carbonate In tetrahydrofuran for 12h; Ambient temperature; | 92% |
With sodium hydrogencarbonate In dichloromethane; water at 20℃; | 66% |
With sodium hydrogencarbonate In dichloromethane | 66% |
(fluorenylmethoxy)carbonyl chloride
Acetic acid (2S,3S,4R,5S,6R)-3-acetylamino-5-benzyloxy-6-hydroxymethyl-2-(4-methoxy-benzyloxy)-tetrahydro-pyran-4-yl ester
Acetic acid (2S,3S,4R,5S,6R)-3-acetylamino-5-benzyloxy-6-(9H-fluoren-9-ylmethoxycarbonyloxymethyl)-2-(4-methoxy-benzyloxy)-tetrahydro-pyran-4-yl ester
Conditions | Yield |
---|---|
With pyridine at 0℃; for 2h; | 100% |
p-aminomethylbenzoic acid
(fluorenylmethoxy)carbonyl chloride
N-(9-fluorenylmethyloxycarbonyl)-4-(aminomethyl)benzoic acid
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water | 100% |
With sodium carbonate In 1,4-dioxane; water at 20℃; for 12h; | 90% |
With sodium hydrogencarbonate In 1,4-dioxane at 0℃; for 3h; | 68.1% |
(fluorenylmethoxy)carbonyl chloride
L-methyltyrosine
Fmoc-L-(α-Me)Tyr-OH
Conditions | Yield |
---|---|
With sodium hydroxide In acetonitrile at 20℃; for 3h; Acylation; | 100% |
(fluorenylmethoxy)carbonyl chloride
L-tryptophan methyl ester
methyl (((9H-fluoren-9-yl)methoxy)carbonyl)-L-tryptophanate
Conditions | Yield |
---|---|
100% |
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
Conditions | Yield |
---|---|
With sodium hydride | 100% |
(fluorenylmethoxy)carbonyl chloride
3-Amino-3-phenylpropionic acid
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In 1,4-dioxane; water at 0 - 20℃; for 25h; | 100% |
With sodium hydroxide In 1,4-dioxane at 20℃; for 4h; | 77% |
With N-ethyl-N,N-diisopropylamine |
(fluorenylmethoxy)carbonyl chloride
γ-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)glutamate
Conditions | Yield |
---|---|
With potassium carbonate In 1,4-dioxane at 20℃; for 4h; | 100% |
(fluorenylmethoxy)carbonyl chloride
(2S,3R)-2-(1-Carboxy-2-methyl-propenylcarbamoyl)-3-hydroxy-3-methyl-pyrrolidine-1-carboxylic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane at 20℃; for 23h; | 100% |
(fluorenylmethoxy)carbonyl chloride
3-nitrobenzylamine hydrochloride
(3-nitrobenzyl)carbamic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 100% |
(fluorenylmethoxy)carbonyl chloride
hydroxy L-proline
(4S)-Nα-Fmoc-4-hydroxy-L-proline
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 0 - 20℃; Inert atmosphere; | 100% |
With sodium carbonate In 1,4-dioxane; water at 0 - 20℃; | 92% |
With sodium hydrogencarbonate In 1,4-dioxane; water at 0 - 20℃; for 9h; |
(E)-(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-3-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-allylamine
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane at 20℃; for 23h; | 100% |
C12H15NO2
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone at 25℃; for 20h; | 100% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine | 100% |
methyl (2RS,3SR)-2-amino-3-(1H-indol-3-yl)butanoate
(fluorenylmethoxy)carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 0.166667h; | 100% |
(fluorenylmethoxy)carbonyl chloride
cis-1-(1,1-dimethylethyoxycarbonyl)-4-amino-L-proline
(2S,4S)-4-(9H-fluoren-9-ylmethoxycarbonylamino)-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane at 20℃; for 5h; | 100% |
With sodium hydrogencarbonate In 1,4-dioxane; water |
[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-acetic acid cyclopentyl ester
(fluorenylmethoxy)carbonyl chloride
[[4-(tert-butoxycarbonylamino-methyl)-benzyl]-(9H-fluoren-9-ylmethoxy-carbonyl)-amino]-acetic acid cyclopentyl ester
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; dichloromethane; water at 0 - 20℃; | 100% |
(E)-1-(3-(2-aminoethyl)phenyl)-2-(O-methyl hydrocinnam-3’-yl)-ethene
(fluorenylmethoxy)carbonyl chloride
methyl trans-3-{3-[2-[3-[2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]phenyl]vinyl]phenyl}propionate
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 20℃; for 24h; | 100% |
With sodium carbonate In 1,4-dioxane at 20℃; for 17h; | 82% |
With sodium carbonate In 1,4-dioxane; water at 20℃; | 3.74 g |
(fluorenylmethoxy)carbonyl chloride
benzyl (1S,3S,5S)-2-azabicyclo<3.3.0>octane-3-carboxylate
1-(9H-fluoren-9-yl)methyl 2-benzyl (2S,3aS,6aS)-hexahydro-cyclopenta[b]pyrrole-1,2(2H)-dicarboxylate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 0 - 20℃; | 100% |
ethyl 5-(4-aminophenylthio)-4-nitrothiophene-2-carboxylate
(fluorenylmethoxy)carbonyl chloride
ethyl 5-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)phenylthio)-4-nitrothiophene-2-carboxylate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 18h; | 100% |
C9H17NO2
(fluorenylmethoxy)carbonyl chloride
(3R,3aR,6S,6aR)-(9H-fluoren-9-yl)methyl 3-hydroxy-6-propyltetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 0℃; for 0.75h; Cooling; | 100% |
With sodium carbonate In 1,4-dioxane; water at 0℃; |
diphenyl diselenide
(fluorenylmethoxy)carbonyl chloride
O-(9H-fluoren-9-yl)methyl Se-phenyl carbonoselenoate
Conditions | Yield |
---|---|
With indium In dichloromethane for 12h; Inert atmosphere; Reflux; | 100% |
With hydrogenchloride; zinc In water at 20℃; for 0.05h; Ionic liquid; Inert atmosphere; | 89% |
With zinc at 130℃; for 0.0333333h; Microwave irradiation; Neat (no solvent); | 60% |
With indium; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 50℃; for 1h; Inert atmosphere; | 25% |
With caesium carbonate; copper(II) oxide at 80℃; for 1h; Ionic liquid; Inert atmosphere; | 90 %Chromat. |
allyl 3,6-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranoside
(fluorenylmethoxy)carbonyl chloride
allyl 3,6-di-O-benzyl-4-O-9-fluorenylmethyloxycarbonyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
H-o-Abc2K(Boc)-OCH2COPh
(fluorenylmethoxy)carbonyl chloride
Fmoc-o-Abc2K(Boc)-OCH2COPh
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 25℃; | 100% |
tert-butyl [(1R,2S)-2-amino-6,6-difluorocyclohexyl]carbamate
(fluorenylmethoxy)carbonyl chloride
tert-butyl 9H-fluoren-9-ylmethyl [(1S,2R)-3,3-difluorocyclohexane-1,2-diyl]biscarbamate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetonitrile for 1.5h; | 100% |
With sodium hydrogencarbonate In water; acetonitrile for 1.5h; |
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