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Cas:104-85-8
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inquiryp-Tolunitrile CAS number: 104-85-8 Molecular formula: C8H7N Molecular weight: 117.1478 Property: Colorless transparent or crystal. Uses: U
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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p-Tolunitrile 104-85-8 p-Tolunitrile Basic information Product Name: p-Tolunitrile Synonyms: 1-Methyl-4-cyanobenzene;4-methyl-benzonitril;4-Toluenkarbonitril;Benzonitrile,4-methyl-;Nit
Cas:104-85-8
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inquiry4-Methylbenzonitrile CAS NO 104-85-8 p-Tolunitrile Basic information Product Name: p-Tolunitrile Synonyms: 1-Methyl-4-cyanobenzene;4-methyl-benzonitril;4-Toluenkarbonitril;Benzonitrile,4-methyl-;Nitril kyseliny p-toluylove;nitrilkyselinyp-tol
Cas:104-85-8
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Product Name:p-Tolunitrile CAS:104-85-8 Purity:98% Package:100g;500g Application:Product Name:p-Tolunitrile CAS:104-85-8 Purity:98% Package:100g;500g
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:104-85-8
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:104-85-8
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inquiryProduct name: P-Tolunitrile CAS No.:104-85-8 Molecule Formula:C8H7N Molecule Weight:117.15 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTIN
Cas:104-85-8
Min.Order:1 Kilogram
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Hunan chemfish Pharmaceutical co.,Ltd a comprehensive enterprise, is located in High-Tech Science Park,Changsha,Chia . Specializing in R&D, manufacture and marketing, we provide a wide range of products and the most professional services to meet the
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:104-85-8
Min.Order:1 Kilogram
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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reagent grade ex stockAppearance:white or off-white crystalline powder Storage:Keep away of light,cool place Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:by Fedex, ship or plane
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in storeAppearance:Colorless transparent liquid Package:500g Application:Organic Chemicals
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Cas:104-85-8
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inquiryp-Tolunitrile Basic information Product Name: p-Tolunitrile Synonyms: 1-Methyl-4-cyanobenzene;4-methyl-benzonitril;4-Toluenkarbonitril;Benzonitrile,4-methyl-;Ni
Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
Conditions | Yield |
---|---|
With 2,3'-bipyridine; ammonium hydroxide; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In ethanol at 20℃; for 24h; | 100% |
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 130℃; under 3750.38 Torr; for 24h; | 100% |
Stage #1: 4-Methylbenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With methyl 4-azidobenzoate at 70℃; for 2h; Inert atmosphere; | A 94% B 100% |
Conditions | Yield |
---|---|
With ammonium hydroxide; periodic acid; potassium iodide at 60℃; for 65745h; Sealed tube; Green chemistry; | 99% |
With ammonium sulfate; sodium carbonate; sulfur In dimethyl sulfoxide at 120℃; for 12h; Reagent/catalyst; Solvent; Time; Temperature; | 99% |
With trifluorormethanesulfonic acid; O-benzenesulfonyl-acetohydroxamic acid ethyl ester In dichloromethane at 23℃; for 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; copper(l) chloride In toluene at 100℃; for 24h; | 99% |
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide for 13h; Ambient temperature; | 95% |
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide for 13h; Product distribution; Ambient temperature; also in (C2H5O)3PO, other temperature, other time; | 95% |
Conditions | Yield |
---|---|
at 520 - 550℃; under 0.01 Torr; | 99% |
In 1,3,5-trimethyl-benzene Thermodynamic data; ΔG(excit.), ΔH(excit.), ΔS(excit.), t1/2; | |
With 1,1-Diphenylethylene In various solvent(s) at 210℃; Rate constant; Thermodynamic data; ΔG(excit.) <250 deg C>; ΔH(excit.), ΔS(excit.); | 100 % Chromat. |
Conditions | Yield |
---|---|
With oxygen In acetone at 20℃; for 3.8h; Electrochemical reaction; | 99% |
With trichloroisocyanuric acid; ammonia In water at 20 - 60℃; | 98% |
With C22H22Cl2FeN2O8(2-)*2C16H36N(1+); oxygen In neat (no solvent) at 100℃; under 760.051 Torr; for 0.5h; Green chemistry; | 98% |
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one; water at 200℃; under 10343 Torr; for 0.166667h; Product distribution; Further Variations:; Solvents; Reaction partners; Temperatures; reaction times; absence of microwave irradiation; microwave irradiation; | 99% |
{cis-Fe(4-MeC6H4N2H)(4-MeC6H4CN)(P(OEt)3)4}(BPh4)2
B
para-methylbenzonitrile
Conditions | Yield |
---|---|
With triethylamine In dichloromethane not isolated; IR spectroscopy; | A 99% B n/a C n/a |
{cis-Fe(4-MeC6H4N2H)(4-MeC6H4CN)(PPh(OEt)2)4}(BPh4)2
B
para-methylbenzonitrile
Conditions | Yield |
---|---|
With triethylamine In dichloromethane not isolated; IR spectroscopy; | A 99% B n/a C n/a |
N-(Diphenylmethylen)-p-toloylsaeureamid
para-methylbenzonitrile
Conditions | Yield |
---|---|
With chlorotriphenoxyphosphonium chloride; triethylamine In chloroform at -30 - 20℃; von Braun degradation; | 99% |
Conditions | Yield |
---|---|
With Pd-PEPPSI-IPrAn In tetrahydrofuran; 1,4-dioxane at 0 - 20℃; for 0.5h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
p-methylbenzaldehyde oxime
para-methylbenzonitrile
Conditions | Yield |
---|---|
copper diacetate In acetonitrile for 4h; Heating; | 98% |
With trichloro(trifluoromethanesulfonato)titanium(IV) at 80℃; for 10h; Dehydration; | 97% |
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; | 97% |
tert-butylisonitrile
4-tolyl iodide
para-methylbenzonitrile
Conditions | Yield |
---|---|
With copper (II) trifluoroacetate hydrate; palladium diacetate In dimethyl sulfoxide at 130℃; for 4h; Sealed tube; Inert atmosphere; | 98% |
4-methylbenzoyl cyanide
para-methylbenzonitrile
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 12h; | 97% |
Conditions | Yield |
---|---|
With ammonia; oxygen; VCrO; silica gel at 210℃; for 8h; | 97% |
With sodium azide; palladium diacetate; triphenylphosphine In acetone at 80℃; for 36h; Schlenk technique; | 92% |
With trichloroisocyanuric acid; ammonia In water at 20 - 60℃; | 90% |
Conditions | Yield |
---|---|
With bromotriphenoxyphosphonium bromide; triethylamine In chloroform at -60℃; von Braun degradation; Reflux; | 97% |
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [{Cu(NO3)}(μ-3-(6-(1H-pyrazol-1-yl)pyridin-2-yl)pyrazol-1-ide)]2; oxygen; potassium carbonate at 50℃; for 24h; | 97% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; tributyltin chloride; tris(dibenzylideneacetone)dipalladium (0) In acetonitrile at 80℃; for 17h; | 96% |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene In various solvent(s) at 60℃; for 4h; | 94% |
Methyl-(4-oxo-5-phenyl-2-p-tolyl-4H-4λ4-[1,4,3]oxathiazin-6-yl)-phenyl-amine
A
C15H13NO2S
B
para-methylbenzonitrile
Conditions | Yield |
---|---|
for 24h; Ambient temperature; | A 96% B n/a |
for 24h; Ambient temperature; other 1,4,3-oxathiazin-4-oxides; | A 96% B n/a |
4-cyanobenzyl bromide
para-methylbenzonitrile
Conditions | Yield |
---|---|
With sodium tetrahydroborate; cetyltributylphosphonium bromide In dichloromethane; water at 18℃; for 0h; Product distribution; | 96% |
With indium(III) chloride; lithium dimethylamino borohydride In tetrahydrofuran at 25℃; for 4h; Inert atmosphere; chemoselective reaction; | 70% |
With Perbenzoic acid; tri-n-butyl-tin hydride In benzene at 90℃; for 12h; Mechanism; in the presence of α-bromotoluene (competitor), relative reactivity; other solvent (MeCN); |
Conditions | Yield |
---|---|
bis(triphenylphosphine)nickel(II) chloride In benzene at 80℃; for 6h; Substitution; | 96% |
With tri-tert-butyl phosphine; [(CO)3Co]2(μ-CO)Pd[μ-(Ph2PCH2)2] In benzene at 120℃; for 2.5h; | 95 % Chromat. |
4-cyanophenyl trifluoromethanesulfonate
methyltriisopropoxytitanium(IV)
para-methylbenzonitrile
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)); (R*)-(S*)-PPFA In tetrahydrofuran for 3h; Heating; | 96% |
Conditions | Yield |
---|---|
With 1,8-bis(diisopropylphosphino)triptycene; potassium phosphate; palladium diacetate In N,N-dimethyl-formamide at 85℃; for 24h; | 96% |
N-tert-butyl-4-methylbenzamide
para-methylbenzonitrile
Conditions | Yield |
---|---|
With bromotriphenoxyphosphonium bromide; triethylamine In chloroform at -60 - 20℃; von Braun degradation; | 96% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Catalytic behavior; Solvent; Temperature; Reagent/catalyst; | 96% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 5h; Reagent/catalyst; Solvent; Temperature; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 10h; Inert atmosphere; | 95% |
tetra-n-butylammonium cyanide
para-methylbenzonitrile
Conditions | Yield |
---|---|
In acetonitrile at 22℃; for 0.25h; Sandmeyer Reaction; | 96% |
4-tolyl perfluorobutanesulfonate
para-methylbenzonitrile
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate at 40℃; for 3h; Catalytic behavior; Time; Temperature; Green chemistry; | 96% |
para-methylphenylmagnesium bromide
pyridin-2-yl cyanate
para-methylbenzonitrile
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 0.166667h; | 95% |
Conditions | Yield |
---|---|
With trimethylsilylazide; titanium tetrachloride In dichloromethane for 2h; Ambient temperature; | 95% |
para-methylbenzonitrile
p-toluamidoxime
Conditions | Yield |
---|---|
With hydroxylamine In ethanol; water Reflux; | 100% |
With hydroxylamine In ethanol; water at 25 - 78℃; for 18h; Reagent/catalyst; Temperature; | 100% |
With hydroxylamine hydrochloride; sodium hydrogencarbonate In ethanol for 6h; Reflux; | 96% |
para-methylbenzonitrile
p-methylselenobenzamide
Conditions | Yield |
---|---|
With selenium; carbon monoxide; water; triethylamine In tetrahydrofuran at 100℃; under 3800 Torr; for 5h; | 100% |
Stage #1: para-methylbenzonitrile With woollins’ reagent In toluene for 4h; Heating; Stage #2: With water In toluene for 1h; | 100% |
With selenium; carbon monoxide; water In N,N-dimethyl-formamide at 90℃; under 760.051 Torr; for 5h; | 96% |
para-methylbenzonitrile
4-methylbenzylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor; | 100% |
Stage #1: para-methylbenzonitrile With [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]triethylphosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; diethylphenylsilane at 20℃; for 18h; Glovebox; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether at 20℃; for 1h; Glovebox; Inert atmosphere; | 99% |
Stage #1: para-methylbenzonitrile With [RhCl2(p-cymene)]2; dimethylamine borane In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; Sealed ampoule; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) In toluene at 135℃; for 24h; Addition; | 100% |
para-methylbenzonitrile
Conditions | Yield |
---|---|
In tetrahydrofuran at 55℃; for 3h; | 100% |
Conditions | Yield |
---|---|
In tetrachloromethane | 100% |
para-methylbenzonitrile
Conditions | Yield |
---|---|
In chloroform at 20℃; for 2h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: para-methylbenzonitrile With hydrogen bromide; dihydrogen peroxide In tetrachloromethane; water at 20℃; for 1h; Irradiation; Stage #2: With ammonia; iodine In tetrachloromethane; water; acetonitrile at 20 - 60℃; for 18h; | 99% |
With 1,10-Phenanthroline; ammonium acetate; dihydrogen peroxide; oxygen In N,N-dimethyl acetamide at 180℃; under 11400.8 Torr; for 24h; Autoclave; | 66% |
With tert.-butylnitrite; N-hydroxyphthalimide; palladium diacetate In acetonitrile at 80℃; for 24h; Inert atmosphere; Sealed tube; | 64% |
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide In ethanol at 20℃; for 2.5h; | 99% |
With water; tricyclohexylphosphine; {Rh(OMe)(cod)}2 In isopropyl alcohol at 25℃; for 24h; | 99% |
With cobalt(II,III) oxide; water at 140℃; for 24h; | 99% |
Conditions | Yield |
---|---|
With hydrogen; silica gel; nickel In methanol; ammonia at 120℃; under 7600 Torr; for 6h; | 99% |
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); potassium tert-butylate; hydrogen bromide; hydrogen; 2-((di-iso-propylphosphino)methyl)-1-methyl-1H-imidazole In tetrahydrofuran; water; acetone; toluene at 20℃; under 37503.8 Torr; for 5.5h; Inert atmosphere; Schlenk technique; Autoclave; | 99% |
With C19H34Cl2CoN2P; hydrogen; sodium ethanolate; sodium triethylborohydride In benzene at 135℃; under 22502.3 Torr; for 36h; Autoclave; | 99% |
Conditions | Yield |
---|---|
With hypochlorous anhydride In tetrachloromethane at 25℃; | 99% |
para-methylbenzonitrile
5-(4-methylphenyl)-2H-tetrazole
Conditions | Yield |
---|---|
Stage #1: para-methylbenzonitrile With α,α,α-trifluorotoluene; tris(2-perfluorohexylethyl)tin azide at 80℃; for 12h; Cyclization; Stage #2: With hydrogenchloride In diethyl ether at 25℃; for 12h; Hydrolysis; | 99% |
With sodium azide; acetic acid In butan-1-ol for 96h; Heating; | 90% |
With sodium azide; zinc(II) chloride In water for 24h; Heating; | 82% |
para-methylbenzonitrile
5-(p-tolyl)-1H-tetrazole
Conditions | Yield |
---|---|
Stage #1: para-methylbenzonitrile With sodium azide In N,N-dimethyl-formamide at 120℃; for 36h; Stage #2: With hydrogenchloride In water; ethyl acetate for 0.0833333h; | 99% |
With sodium azide; acetic acid In 1-methyl-pyrrolidin-2-one; water at 220℃; under 5250.53 Torr; for 0.0833333h; Microwave irradiation; | 98% |
With sodium azide; gold In N,N-dimethyl-formamide at 80℃; for 1.5h; Reagent/catalyst; Inert atmosphere; | 98% |
para-methylbenzonitrile
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With C37H59AlN2 In neat (no solvent) at 60℃; for 1.5h; Inert atmosphere; | 99% |
With silver hexafluoroantimonate at 60℃; for 12h; Inert atmosphere; Glovebox; | 99% |
With manganese(II) triflate bis-acetonitrile solvate; potassium tert-butylate In benzene-d6 at 20℃; for 3h; Inert atmosphere; Glovebox; | 99% |
para-methylbenzonitrile
N-benzyl-3-phenylprop-2-en-1-amine
Conditions | Yield |
---|---|
With tris(bis(trimethylsilyl)amido)ytterbium(III) In toluene at 25℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
With tris(bis(trimethylsilyl)amido)ytterbium(III) In toluene at 22℃; for 12h; Inert atmosphere; | 80% |
ethyl 5-phenyl-1,2,3-thiadiazole-4-carboxylate
para-methylbenzonitrile
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; chloro(1,5-cyclooctadiene)rhodium(I) dimer In chlorobenzene at 130℃; for 2h; Glovebox; | 99% |
para-methylbenzonitrile
2,3-dimethyl-buta-1,3-diene
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane
Conditions | Yield |
---|---|
Stage #1: para-methylbenzonitrile; 2,3-dimethyl-buta-1,3-diene; dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane With tris(3,5-dimethylphenyl)phosphine; copper diacetate In toluene at 20℃; for 19h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: With hydrogenchloride In water; toluene at 20℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; para-methylbenzonitrile With hydrogen In 2-methyltetrahydrofuran at 100℃; under 11251.1 Torr; for 20h; High pressure; Autoclave; Stage #2: With hydrogenchloride In diethyl ether | 99% |
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