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inquirySodium dichloroacetate Basic information Product Name: Sodium dichloroacetate Synonyms: dichloroacetate,sodiumsalt;dichloro-aceticacisodiumsalt;dichloroctansodny;Sodiumdichloracetate;NATRIUMDICHLORACETAT;SDA;SODIUM DICHLOROACETATE;erlcyiuanna
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inquirySodium dichloroacetate Basic information Product Name: Sodium dichloroacetate Synonyms: dichloroacetate,sodiumsalt;dichloro-aceticacisodiumsalt;dichloroctansodny;Sodiumdichloracetate;NAT
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Min.Order:1 Kilogram
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inquiryConditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; for 2h; | 96% |
With sodium hydrogencarbonate In N,N-dimethyl-formamide |
sodium dichloroacetate
1,2-dichloro-tetramethyl-distannane
Conditions | Yield |
---|---|
In water to stirred soln. of tin compd. in degassed H2O was slowly added soln. of Na- (or NH4-) CHCl2COO (50-100% excess); formed ppt. was filtered off, washed with water, then with a little MeOH and dried in vac. at room temp.; recrystn. from PE(40/60); elem. anal.; | 99% |
Conditions | Yield |
---|---|
Stage #1: cisplatin With nitric acid; silver nitrate In water at 20℃; for 48h; Darkness; Stage #2: sodium dichloroacetate In water | 87% |
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride
sodium dichloroacetate
[Pd(O2CHCl2)2(1,1'-bis(diphenylphosphino)ferrocene)]
Conditions | Yield |
---|---|
With AgNO3 In dichloromethane (Ar); mixing palladium complex, sodium and silver salts in CH2Cl2, stirring at room temp. for 16 h in the dark; filtration through celite column, concn., addn. of hexane; elem. anal.; | 84% |
sodium dichloroacetate
A
2-chloro-4-chloromethylsulfonylphenoxyacetic acid
Conditions | Yield |
---|---|
In water at 95℃; for 8h; | A n/a B 82% |
In water at 95℃; for 8h; | A n/a B 82% |
sodium dichloroacetate
Conditions | Yield |
---|---|
In water at 95℃; for 8h; | A n/a B 80.3% |
sodium p-chlorobenzenesulphinate
sodium dichloroacetate
chloromethyl p-chlorophenyl sulfone
Conditions | Yield |
---|---|
In water at 90℃; for 7h; | 74% |
sodium dichloroacetate
A
4-chloromethylsulfonylphenoxyacetic acid
Conditions | Yield |
---|---|
In water at 95℃; for 8h; | A n/a B 73.1% |
sodium dichloroacetate
Conditions | Yield |
---|---|
In water at 95℃; for 8h; | A n/a B 72.8% |
Conditions | Yield |
---|---|
Stage #1: 3-hydroxy-2-phenyl-1H-quinolin-4-one With potassium carbonate In N,N-dimethyl-formamide Reflux; Inert atmosphere; Stage #2: sodium dichloroacetate In N,N-dimethyl-formamide for 1.83333h; Inert atmosphere; | 72% |
[(-CH2C6H2(S)(tert-butyl)CH2N(methyl)C2H4N(methyl)C2H4N(methyl)CH2C6H2(S)(tert-butyl)CH2N(methyl)C2H4N(methyl)C2H4N(methyl)-)Ni2(μ-Cl)](perchlorate)
sodium dichloroacetate
[((t-Bu)2C24H28N6S2(Me)6)Ni2(μ-O2CCHCl3)]ClO4
Conditions | Yield |
---|---|
With LiClO4*3H2O In methanol byproducts: NaCl; (Ar), Schlenk techniques; addn. of soln. of Na compd. in MeOH to soln. of Ni complex in MeOH, stirring for 2 to 3 h, addn. of soln. of LiClO4*3H2O in MeOH; filtration, air drying, dissolving in MeCN, filtration, addn. of EtOH, concn., storage for 6 h, filtration, crystn. from MeCN/EtOH (1:1), air drying, elem. anal.; | 70% |
sodium dichloroacetate
Conditions | Yield |
---|---|
In water at 95℃; for 8h; | A 69.5% B n/a |
bis(cyclopentadienyl)titanium dichloride
2,2,6,6-tetramethylheptane-3,5-dione
sodium dichloroacetate
Conditions | Yield |
---|---|
In water mixture of Cp2TiCl2(0.01mole) and corresponding dione (0.011mole) in water (60ml) was stirred at 60-65°C (6h), filtered, and the filtrate then added to concd. soln. of acetate (0.01mole) until no more ppt. was formed;; the formed ppt. was digested over a water bath (3h), allowed to stand for a few h, filtered, washed and dried under vacuum; elem. anal.;; | 68% |
Conditions | Yield |
---|---|
With Et3N In methanol Na dichloroacetate and MeOH soln. of Et3N added to suspn. of Na salt of ligand and FeCl3 in hot MeOH; refluxed for 1 h; filtered; NH4PF6 added to filtrate; stirred at room temp. for 8 h; ppt. dissolved in MeCN; crystd. by diffusion of Et2O; elem. anal.; | 68% |
bis(cyclopentadienyl)titanium dichloride
sodium dichloroacetate
acetylacetone
Conditions | Yield |
---|---|
In water addn. of dione (0.012mole) to a concd. aq. soln. of Cp2TiCl2 (0.01mole in 60ml H2O), stirring mixture (2h), removal of ppt. by filtration, slow addn. of filtrate to concd. aq. soln. of NaCl2HCCO2 (equimolar: 0.01mole) with continous stirring;; digesting of formed ppt. over a water bath at 60°C (2h), standing overnight, filtration, washing and drying under vacuum, dissolving ppt. in dichloromethane and repptg. by adding of light petroleum ether; elem. anal.;; | 65% |
bis(cyclopentadienyl)titanium dichloride
sodium dichloroacetate
1-phenylbutan-1,3-dione
Conditions | Yield |
---|---|
In water stirring Cp2TiCl2 (0.01mole) in water (60ml) with an excess of corresponding dione (0.014mole) for 3h (formation of soln. of ((Cp2Ti(MeCOCHCOPh))Cl), filtration, slow addn. of filtrate to a hot aq. soln. of acetate (0.01mole), further stirring (4h);; digesting of formed ppt. over a water bath at 60°C (0.5h), standing overnight, filtration, washing and drying under reduced pressure; elem. anal.;; | 62% |
sodium dichloroacetate
Conditions | Yield |
---|---|
In acetonitrile excess carboxylate; alternatively used solvent: methanol; free acid was neutralized with stoichiometric LiOH or triethylamine;; elem. anal.;; | 53% |
sodium dichloroacetate
Conditions | Yield |
---|---|
In dichloromethane; acetone byproducts: NaCl; addn. of acetate suspension (acetone) to Ru complex soln. (CH2Cl2); stirring, room temp., 12h; filtering off pptd. NaCl; evapn.; recrystn. (chlorofome/diethyl ether 1/1 v/v); filtration; air-drying; elem. anal.; | 50% |
4-bromo-phenol
sodium dichloroacetate
ethylenediamine
ethylenediamine-N,N'-bis(α-2-hydroxy-5-bromophenyl)acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 85℃; for 24h; | 30% |
Conditions | Yield |
---|---|
With dichloro-acetic acid In ethanol for 10h; Reflux; | 28% |
Chloromethyl-phenyl-carbamic acid isopropyl ester
sodium dichloroacetate
Dichloro-acetic acid (isopropoxycarbonyl-phenyl-amino)-methyl ester
Isopropyl-N-chloromethyl-N-(3-chlorophenyl)-carbamate
sodium dichloroacetate
Dichloro-acetic acid [(3-chloro-phenyl)-isopropoxycarbonyl-amino]-methyl ester
sodium dichloroacetate
sodium dichloroacetate
Conditions | Yield |
---|---|
for 50h; Ambient temperature; |
diphenyltellurium dichloride
sodium dichloroacetate
diphenyltellurium(IV) bis(dichloroacetate)
Conditions | Yield |
---|---|
In benzene for 24h; |
chloro-5 hydroxy-2 α-methyl α-phenyl benzene methanol
sodium dichloroacetate
acide benzodioxine-(1,3)> caboxylique-2 trans
acide benzodioxine-(1,3)> caboxylique-2 cis
Conditions | Yield |
---|---|
With sodium amide In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene for 9h; Heating; Yield given. Yields of byproduct given; |
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