CAS No.506-65-0,GOLD(I) CYANIDE Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Gold(I) cyanide

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Aurous cyanide

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

GOLD(I) CYANIDE

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Henan Tianfu Chemical Co., Ltd.

Good quantity Storage:R.T. Package:as per buyers Application:Reagent Transportation:by air/sea

Gold(I) cyanide

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Gold(I) cyanide (99.9%-Au)

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Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

Gold(I) cyanide, PreMion|r, 99.99% (Metals b

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Panamit Intermational

Gold cyanide (Au(CN))

Cas:506-65-0

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Synthetic route

: tris(triphenylphosphinegold)oxonium fluoroborate

: 7646-69-7
sodium hydride

: 670-54-2
ethenetetracarbonitrile

A: 2P(C6H5)3*Au(1+)*BF4(1-)=(P(C6H5)3)2AuBF4

B: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In tetrahydrofuran stirring suspn. of all substances in abs. THF for 4 h; ppt. sepn., washing (THF, water and ether) and drying gave AuCN; soln. dild. with petroleum ether and cooled to 0°C; ppt. sepn. and washing with petroleum ether gave Au-complex;	A 100% B 67%

...Expand

: tris(triphenylphosphinegold)oxonium fluoroborate

: 670-54-2
ethenetetracarbonitrile

A: tricyanomethanidebis(triphenylphosphine)gold

B: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In tetrahydrofuran addn. of Au-complex to soln. of org. compd., stirring (4 h); ppt. sepn., washing (acetone) and drying gave AuCN; evapn. of combined solns. (dryness) and repptn. from acetone by pentane gave Au-complex;	A 80% B 20%

...Expand

: potassium cyanide

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
With sulfuric acid In sulfuric acid; water byproducts: HCN, K2SO4; conc. H2SO4 was added in excess to intermediate complex; elem. anal.;	70%

: 2,4-dihydro-1,3-diphenyl(triphenylphosphinegold)cyclopenta{b}indene

: 670-54-2
ethenetetracarbonitrile

A: 2,4-dihydro-1,3-diphenyl(triphenylphosphinegold)cyclopenta{b}indene-tetracyanoethyleneviolet

B: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In benzene stirring (4 h), ppt. sepn., washing with benzene; extn. by acetone gave AuCN (powder); acetone soln. evapn. to dryness, solid residue dissoln. in benzene, filktration and diln. with petroleum ether to turbidity; ppt. sepn., washing with pentane and drying gave C6H4CH2C5HPh2AuPPh3*TCE; elem. anal.;	A n/a B 69%

...Expand

: 2,4-dihydro-1,3-diphenyl(triphenylphosphinegold)cyclopenta{b}indene

: 670-54-2
ethenetetracarbonitrile

A: tricyanomethanidebis(triphenylphosphine)gold

B: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In benzene stirring (4 h); ppt. sepn., washing with benzene, extn. by acetone gave AuCN (powder); acetone soln. evapn. gave (PPh3)2AuC(CN)3; elem. anal.;	A 1.7% B 69%

...Expand

: 123528-41-6
tetracyanoethylene*C12H8(C6H5)2

: tris(triphenylphosphinegold)oxonium fluoroborate

A: tricyanomethanidebis(triphenylphosphine)gold

B: 33836-49-6
1,3-diphenyl-2,8-dihydrocyclopenta[a]indene

C: 506-65-0
gold(I) cyanide

Conditions

Conditions	Yield
In tetrahydrofuran addn. of Au-complex to soln. of org. compd., stirring (4 h); ppt. sepn., washing (THF) and drying gave AuCN; all solns. evapn. to dryness, residue extn. (benzene), ext. evapn. (dryness) gave C6H4CH2C5H2Ph2, residue extn. (benzene) and repptn. from acetone by hexane gave Au-complex;	A 59% B n/a C 33%

...Expand

: 506-65-0
gold(I) cyanide

: 6476-36-4
tris(1-methylethyl)phosphine

: ((CH3)2CH)3PAuCN

Conditions

Conditions	Yield
In methanol; water under an inert atmosphere; to a suspn. of AuCN in methanol/water was added a soln. of the phosphine in methanol, stirred for 2 h; decanted, evapd. to dryness, washed with H2O, extd. with methanol; elem. anal.;	79%

: [RuCp(Tpmd)]

: 506-65-0
gold(I) cyanide

: [RuCp(μ-Tpmd){AuCN}]

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube;	76%

: 506-65-0
gold(I) cyanide

: 534-13-4
N,N-dimethylthiourea

: 288088-85-7
dicyano-1κ(2)C-bis-(dimethylthiourea)-2κ(2)S-digold(I)(Au-Au)

Conditions

Conditions	Yield
In water AuCN added to thione soln., heated to 343 K for 30 min; crystn. on cooling, elem. anal.;	73%

: tetraphenylphosphonium tetraselenotungstate

: 506-65-0
gold(I) cyanide

: 672-66-2
Dimethyl(phenyl)phosphine

: P(C6H5)4(1+)*(CH3)2(C6H5)PAu(Se)2WSe2(1-)=[P(C6H5)4][((CH3)2(C6H5)P)Au(Se)2WSe2]

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; W-compd. addn. to Au compd. suspn., org. compd.addn., soln. stirring for 60 min, filtration (sintered glass frit), Et2O layering on filtrate top over 10 d, crystn.; crystals filtration off; elem. anal.;	63%

...Expand

: 2P(C6H5)4(1+)*(NC)Cu(Se)2Mo(Se)2(2-) = [P(C6H5)4]2[(NC)Cu(Se)2Mo(Se)2]

: 506-65-0
gold(I) cyanide

: 672-66-2
Dimethyl(phenyl)phosphine

: P(C6H5)4(1+)*((CH3)2(C6H5)P)2Cu(Se)2MoSe2(1-)=[P(C6H5)4][((CH3)2(C6H5)P)2Cu(Se)2MoSe2]

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; org. compd. addn. to mixed soln. of Au- and Cu-compds., stirring for 30 min, filtration (sintered glass frit), Et2O layering on filtrate top over 2 d, crystn.; crystals filtration off; elem. anal.;	60%

...Expand

: tetraphenylphosphonium tetraselenomolybdate

: 506-65-0
gold(I) cyanide

: 672-66-2
Dimethyl(phenyl)phosphine

: P(C6H5)4(1+)*(CH3)2(C6H5)PAu(Se)2MoSe2(1-)=[P(C6H5)4][((CH3)2(C6H5)P)Au(Se)2MoSe2]

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; org. compd. addn. to mixed soln. of Mo- and Au compds., stirring for 30 min, soln. filtration (sintered glass frit), Et2O layering on filtrate top over 2 d, crystn.; crystals filtration off; elem. anal.;	60%

...Expand

: tetraphenylphosphonium tetraselenomolybdate

: 506-65-0
gold(I) cyanide

: 2P(C6H5)4(1+)*(NC)Au(Se)2Mo(Se)2(2-)=[P(C6H5)4]2[(NC)Au(Se)2Mo(Se)2]

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; components mixed soln. stirring for 60 min, filtration (sintered glass frit), Et2O layering on filtrate top over 3 d, crystn.; crystals filtration off; elem. anal.;	60%

: tetraphenylphosphonium tetraselenotungstate

: 506-65-0
gold(I) cyanide

: 2P(C6H5)4(1+)*(NC)Au(Se)2W(Se)2(2-)=[P(C6H5)4]2[(NC)Au(Se)2W(Se)2]

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; components mixed soln. stirring for 3 h, filtration (sintered glass frit), Et2O layering on filtrate top over 3 d, crystn.; crystals filtration off; elem. anal.;	57%

: tetraphenylphosphonium tetraselenotungstate

: 506-65-0
gold(I) cyanide

: 75-05-8
acetonitrile

: 2P(C6H5)4(1+)*(NC)Au(Se)2W(Se)2Au(CN)(2-)*CH3CN=[P(C6H5)4]2[(NC)Au(Se)2W(Se)2Au(CN)]*CH3CN

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; stirring mixed soln. of components for 60 min, soln. filtration (sintered glass frit), Et2O layering on filtrate top over 10 d, crystn.; crystals filtration off; elem. anal.;	40%

...Expand

: tetraphenylphosphonium tetraselenomolybdate

: 506-65-0
gold(I) cyanide

: 75-05-8
acetonitrile

: 2P(C6H5)4(1+)*(NC)Au(Se)2Mo(Se)2Au(CN)(2-)*CH3CN=[P(C6H5)4]2[(NC)Au(Se)2Mo(Se)2Au(CN)]*CH3CN

Conditions

Conditions	Yield
In acetonitrile N2, Schlenk techniques; stirring mixed soln. of components for 30 min, soln. filtration sintered glass frit), Et2O layering on filtrate top over 5 d, crystn.; crystals filtration off; elem. anal.;	40%

...Expand

: [RuCp*(Tpmd)]

: 506-65-0
gold(I) cyanide

: [RuCp*(Tpmd){AuCN}]

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube;	36%

: Na2TeSe3

: 506-65-0
gold(I) cyanide

: 2751-90-8
tetraphenylphosphonium bromide

: 2P(C6H5)4(1+)*Au2(TeSe2)2(2-)=[P(C6H5)4]2[Au2(TeSe2)2]

Conditions

Conditions	Yield
With PEt3 In N,N-dimethyl-formamide Na2TeSe3 in DMF slowly added to DMF soln. of AuCN and PEt3 at room temp., stirred for 2 h, treated with solid PPh4Br, stirred for 2 h; filtered, crystd.(ether), elem. anal.;	33%

...Expand

: tellurium

: lithium telluride

: 506-65-0
gold(I) cyanide

: 3(C2H5)4N(1+)*AuTe7(3-)={(C2H5)4N}3{AuTe7}

Conditions

Conditions	Yield
With P(C2H5)3; (C2H5)4NCl In N,N-dimethyl-formamide; acetonitrile generation of a poytelluride soln. by react. of Li2Te and Te-powder in DMF, addn. of a mixt. of AuCN and PEt3 in DMF, stirring at room temp. for 1 h and filtn., addn. of NEt4Cl in CH3CN to the filtrate; crystn. upon layering of the resultant soln. with ether, manual sepn. of platelike from needle-shaped crystals; elem. anal. of platelike crystals;;	27%

Yield

With P(C2H5)3; (C2H5)4NCl In N,N-dimethyl-formamide; acetonitrile generation of a poytelluride soln. by react. of Li2Te and Te-powder in DMF, addn. of a mixt. of AuCN and PEt3 in DMF, stirring at room temp. for 1 h and filtn., addn. of NEt4Cl in CH3CN to the filtrate; crystn. upon layering of the resultant soln. with ether, manual sepn. of platelike from needle-shaped crystals; elem. anal. of platelike crystals;;

27%

...Expand

: 506-65-0
gold(I) cyanide

A: 2074-87-5
carbon nitride

B gold: gold

Conditions

Conditions	Yield
beim Gluehen;

: 506-65-0
gold(I) cyanide

potassium ferro cyanide: potassium ferro cyanide

potassium auro cyanide: potassium auro cyanide

: 506-65-0
gold(I) cyanide

: 7440-57-5, 457905-15-6
gold

Conditions

Conditions	Yield
With water In solid byproducts: HCN, O2; heating at 385-480°C in air;
With sodium hypophosphite In water formation of Au-coatings on metals;;
With water In solid byproducts: HCN, O2; heating at 350-700°C in air;
With NaH2PO2 In water formation of Au-coatings on metals;;

: 506-65-0
gold(I) cyanide

: cyano(triphenylphosphine)gold(I)

Conditions

Conditions	Yield
With P(C6H5)3 In chloroform treating with chloroform soln. of PPh3;

: 506-65-0
gold(I) cyanide

: gold cyanide monoammoniate

Conditions

Conditions	Yield
With ammonia In ammonia recrystn.; elem. anal.;

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