Product Detail Minimum Order Qty. 10 Gram
Cas:123-35-3
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:123-35-3
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryUnique advantages for Myrcene Cas 123-35-3 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Light yellow to yellow transparent liquid Storage:Store in 2-8℃ Package:175kg/
Cas:123-35-3
Min.Order:175 Kilogram
FOB Price: $10.0 / 12.0
Type:Trading Company
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:123-35-3
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Name: Myrcene Synonyms: Myrcene technical grade;Myrcene CAS;BETA-MYRCENE;FEMA 2762;7-METHYL-3-METHYLEN-1,6-OCTADIENE;7-METHYL-3-METHYLENE-1,6-OCTADIENE;OIL;MYRCENE CAS: 123-35-3 MF: C10H16 MW: 136.23 EIN
Cas:123-35-3
Min.Order:1 Gram
FOB Price: $8900.0
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $2.0 / 6.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:123-35-3
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $3.0 / 5.0
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:123-35-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: Myrcene CAS: 123-35-3 MF: C10H16 MW: 136.23 EINECS: 204-622-5 Mol File: 123-35-3.mol Myrcene Structure Myrcene Chemical Properties Melting point <-10 °C Boiling point 167 °C (lit.) density 0.79
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $80.0 / 100.0
Type:Trading Company
inquiryMyrcene CAS:123-35-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, ster
Cas:123-35-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
Cas:123-35-3
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryMyrcene CAS:123-35-3 Specification MELTING POINT <-10°C boiling point 167°C (Lit.) Density 0.791 g/l at 25°C (lit.) Vapor Density 4.7(vs air) vapor pressure ~ 7 MMHG (20°C) FEMA2762 | Myrcene refractive index n20/D1.469
Appearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:123-35-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:123-35-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:200kg/drum, or as per your request. Application:Used as Pharmace
1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:123-35-3
Min.Order:1 Kilogram
FOB Price: $7.0 / 9.0
Type:Trading Company
inquiry(2-methylene-3-butenyl)-trimethyltin
prenyl bromide
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran at 65℃; | 94% |
2-chloromethyl-1,3-butadiene
3-methyl-2-butenylmagnesium chloride
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 10h; | 92% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); 2-Propynylzinc bromide In tetrahydrofuran for 3h; Ambient temperature; | 90% |
geranyl 2-tetrahydropyranyl ether
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran for 6h; Heating; | 89% |
With 18-crown-6 ether; potassium tert-butylate In tetrahydrofuran at 60℃; for 12h; Inert atmosphere; | 73.1% |
O-(trans-3,7-dimethylocta-2,6-dien-1-yl)trimethylsilane
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With tetrahydrofuran; lithium diisopropylamide at -78℃; for 5h; | 85% |
neryl 2-tetrahydropyranyl ether
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran for 18h; Heating; | 83% |
geraniol methyl ether
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With potassium tert-butylate; 18-crown-6 ether In tetrahydrofuran for 2h; Heating; | 76% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -50℃; for 1h; | 76% |
4-methyl-3-pentenylmagnesium bromide
buta-2,3-dien-1-yl diethyl phosphate
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; Ambient temperature; | 75% |
beta-pinene
A
7-methyl-3-methene-1,6-octadiene
B
pseudolimonene
C
(-)-(S)-limonene
Conditions | Yield |
---|---|
In ethanol at 400℃; under 91206.1 Torr; for 0.0194444h; Product distribution; Further Variations:; Temperatures; | A 72% B 8% C n/a |
geraniol methyl ether
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
In tetrahydrofuran at -30℃; for 15h; | 66% |
6-Methyl-2-(toluene-4-sulfonyl)-2-vinyl-hept-5-en-1-ol
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 2h; Heating; | 62% |
4,4,4-Trifluoro-3-oxo-butyric acid (E)-3,7-dimethyl-octa-2,6-dienyl ester
A
7-methyl-3-methene-1,6-octadiene
B
1,1,1-trifluoro-6,10-dimethyl-undeca-5,9-dien-2-one
Conditions | Yield |
---|---|
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,2-bis-(diphenylphosphino)ethane In tetrahydrofuran Heating; | A n/a B 56% |
(E)-N,N-diethyl-3,7-dimethyl-2,6-octadienylamine
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
at 130℃; under 20 Torr; for 5h; | 50% |
A
7-methyl-3-methene-1,6-octadiene
B
(Z)-ocimene
C
trans ocimene
D
3,5,7-trimethyltropolone
Conditions | Yield |
---|---|
at 180℃; pyrolysis; | A 30% B 8% C 49% D n/a |
at 140℃; pyrolysis; | A 23% B 12% C 36% D n/a |
geranyl phenyl sulfide
acetic anhydride
acetic acid
A
7-methyl-3-methene-1,6-octadiene
B
3,7-dimethyl-2E,6-octadien-1-yl acetate
C
(Z)-ocimene
Conditions | Yield |
---|---|
With lithium acetate; copper diacetate; copper at 85 - 90℃; | A n/a B 43% C n/a |
phthalimide
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With 18-crown-6 ether In N,N-dimethyl-formamide at 100℃; for 16h; | 43% |
Conditions | Yield |
---|---|
With potassium tert-butylate; 18-crown-6 ether In tetrahydrofuran for 7h; Heating; | 35% |
A
7-methyl-3-methene-1,6-octadiene
B
5-(3,7-dimethyl-2,6-octadienyl)tropolone
Conditions | Yield |
---|---|
at 140℃; for 2h; pyrolysis; Further byproducts given; | A 3 % Chromat. B 32% C 31% |
A
7-methyl-3-methene-1,6-octadiene
B
5-(3,7-dimethyl-2,6-octadienyl)tropolone
D
isoprene
Conditions | Yield |
---|---|
at 140℃; for 2h; pyrolysis; Further byproducts given; | A 3 % Chromat. B 32% C 31% D 10 % Chromat. |
Conditions | Yield |
---|---|
32% | |
23% | |
In tetrahydrofuran | 15% |
With sodium; N-cyclohexyl-cyclohexanamine In tetrahydrofuran Mechanism; K, Li various dialkylamines; | |
In tetrahydrofuran at 10℃; Rate constant; Na, dicyclohexylamine; |
geranyl methyl carbonate
A
7-methyl-3-methene-1,6-octadiene
B
(Z)-ocimene
Conditions | Yield |
---|---|
With hexacarbonyl molybdenum In toluene at 110℃; for 72h; | A 7% B 31% |
3,7-dimethyl-oct-6-enal
A
7-methyl-3-methene-1,6-octadiene
B
3,7-Dimethyl-octa-1,3,6-trien
C
1-methyl-4-isopropyl-1,3-cyclohexadiene
D
3,8-p-Menthadien
E
limonene.
Conditions | Yield |
---|---|
With aluminum oxide; carbon dioxide In hexane at 190℃; Supercritical conditions; | A 15.8% B 6.2% C 11.9% D 30.8% E 5.2% |
Conditions | Yield |
---|---|
at 140℃; | A 29% B 9% C 27% |
at 140℃; pyrolysis; | A 29% B 9% C 27% |
Geraniol
A
7-methyl-3-methene-1,6-octadiene
B
(Z)-ocimene
C
trans ocimene
D
Terpinolene
E
limonene.
Conditions | Yield |
---|---|
With tin(ll) chloride In dimethyl sulfoxide at 139.84℃; for 2h; | A 27% B 24% C 17% D 10% E 22% |
Conditions | Yield |
---|---|
With copper(II) sulfate In neat (no solvent) at 125℃; under 25 Torr; for 1.5h; | 25% |
Multi-step reaction with 3 steps 1: 86 percent 2: NaI / acetone / 1 h / 0 - 2 °C 3: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme | |
With bis(acetylacetonato)palladium(II); carbon monoxide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; trifluoroacetic acid In toluene at 105℃; under 30003 Torr; for 18h; chemoselective reaction; | |
Multi-step reaction with 2 steps 1: Castellaniella defragrans linalool dehydratase isomerase / 20 h / Enzymatic reaction 2: Castellaniella defragrans linalool dehydratase isomerase / 20 h / Enzymatic reaction View Scheme | |
Multi-step reaction with 2 steps 1: toluene-4-sulfonic acid / tetrahydrofuran / 20 °C 2: potassium tert-butylate; 18-crown-6 ether / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere View Scheme |
3,7-dimethyl-oct-6-enal
A
7-methyl-3-methene-1,6-octadiene
B
1-methyl-4-isopropyl-1,3-cyclohexadiene
C
3,8-p-Menthadien
D
3-p-menthene
Conditions | Yield |
---|---|
With aluminum oxide; carbon dioxide In hexane at 190℃; Supercritical conditions; | A 6.9% B 8.2% C 21.4% D 6.3% E 6.6% |
Conditions | Yield |
---|---|
at 180℃; for 15h; Further byproducts given; | A 15% B 6% C 19% D n/a |
at 180℃; for 0.25h; pyrolysis; Further byproducts given; | A 15% B 6% C 19% D n/a |
at 180℃; for 15h; pyrolysis; Further byproducts given; | A 15 % Chromat. B 6 % Chromat. C 19 % Chromat. D n/a |
tert-butylamine
diisopropylamine
isoprene
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
18.6% |
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran at 70℃; for 48h; Diels-Alder Cycloaddition; Sealed tube; | 100% |
7-methyl-3-methene-1,6-octadiene
acrylic acid methyl ester
1(4-methyl-3-pentenyl)-4-carbmethoxy-cyclohex-1-ene
Conditions | Yield |
---|---|
With K10 supported ecological catalyst (0.1equiv. Zn) In toluene at 110℃; for 1h; | 99% |
silica gel at 100℃; for 4h; | 60% |
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium; 1,3-bis-(diphenylphosphino)propane In toluene at 130℃; for 48h; Inert atmosphere; | 99% |
With dodecacarbonyl-triangulo-triruthenium; 2,2'-bis(diphenylphosphino)biphenyl In toluene at 130℃; for 48h; Inert atmosphere; diastereoselective reaction; | 84% |
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxyphenyl)-3-phenylprop-2-en-1-one With borane-THF; (2R)-(+)-3,3'-diphenyl-[2,2'-dinaphthalene]-1,1'-diol; acetic acid In tetrahydrofuran at 20℃; for 1h; Diels-Alder Cycloaddition; Molecular sieve; Inert atmosphere; Stage #2: 7-methyl-3-methene-1,6-octadiene In tetrahydrofuran at 20℃; for 12h; Diels-Alder Cycloaddition; Molecular sieve; Inert atmosphere; enantioselective reaction; | 99% |
Stage #1: 1-(2-hydroxyphenyl)-3-phenylprop-2-en-1-one With triphenylborane; (S)-2,15-dichlorotetraphenylene-1,16-diol In 1,2-dichloro-ethane at 100℃; for 2h; Diels-Alder Cycloaddition; Inert atmosphere; Schlenk technique; Sealed tube; Molecular sieve; Stage #2: 7-methyl-3-methene-1,6-octadiene In 1,2-dichloro-ethane at 30℃; Diels-Alder Cycloaddition; Inert atmosphere; Schlenk technique; Sealed tube; Molecular sieve; stereoselective reaction; | 89% |
7-methyl-3-methene-1,6-octadiene
ethyl 2-((2-oxo-2-phenylethyl)thio)acetate
Conditions | Yield |
---|---|
In dichloromethane at -10℃; for 0.5h; Inert atmosphere; UV-irradiation; Flow reactor; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With nickel(II) bis(octanoate); hydrogen; 1,4-bis(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabuta-1,3-diene; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In benzene-d6 at 50℃; under 3040.2 Torr; for 24h; Reagent/catalyst; | 98% |
With cobalt In tetrahydrofuran Heating; High pressure; | 79% |
With 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthenecobalt(II) dibromide; hydrogen; lithium triethylborohydride In tetrahydrofuran at 20℃; under 7500.75 Torr; for 24h; | 76% |
7-methyl-3-methene-1,6-octadiene
PVS
[4-(4-Methyl-pent-3-enyl)-cyclohex-3-enesulfonyl]-benzene
Conditions | Yield |
---|---|
In benzene at 155℃; for 22h; | 98% |
With hydroquinone In benzene at 155℃; for 22h; | 88.6% |
7-methyl-3-methene-1,6-octadiene
6,7-epoxymyrcene
Conditions | Yield |
---|---|
With dihydrogen peroxide; tungsten(VI) oxide; [CH3(n-C8H17)3N]+H2PO4- In toluene at 21℃; for 3h; | 98% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 22℃; for 0.0833333h; | 97% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane for 0.0833333h; cooling; | 95.2% |
7-methyl-3-methene-1,6-octadiene
3-(4-methylpent-3-en-1-yl)-2,5-dihydrothiophene-1,1-dioxide
Conditions | Yield |
---|---|
Stage #1: 7-methyl-3-methene-1,6-octadiene With 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate In acetonitrile at 20℃; Inert atmosphere; Sealed tube; Stage #2: With boron trifluoride diethyl etherate In acetonitrile at 0 - 70℃; for 12h; Inert atmosphere; Sealed tube; | 97% |
With sodium metabisulfite; 1,1,1,3',3',3'-hexafluoro-propanol In water at 100℃; under 517.162 - 1034.32 Torr; for 14h; Reagent/catalyst; Sealed tube; | 86% |
With diethyl ether; sulfur dioxide at 100℃; |
7-methyl-3-methene-1,6-octadiene
1-benzyl-3-hydroxy-5-methoxyindolin-2-one
(E)-1-benzyl-3-(3,7-dimethylocta-2,6-dien-1-yl)-3-hydroxy-5-methoxyindolin-2-one
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium; tricyclohexylphosphine In toluene at 110℃; for 48h; Inert atmosphere; Sealed tube; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With iron perchlorate hexahydrate In acetonitrile at 20℃; for 24h; Diels-Alder Cycloaddition; regioselective reaction; | 97% |
With C26H18N10Ru(2+)*2C32H12BF24(1-) In dichloromethane for 1.5h; Diels-Alder Cycloaddition; Irradiation; | 88% |
With 9-(2-trifluoromethylphenyl)-1,3,6,8-tetramethoxythioxanthylium trifluoromethanesulfonate In nitromethane at 20℃; for 1h; Diels-Alder Cycloaddition; UV-irradiation; | 84% |
With iron(III) chloride In dichloromethane; acetonitrile at 0℃; for 3h; | 76% |
methanol
7-methyl-3-methene-1,6-octadiene
6-Bromo-7-methoxy-7-methyl-3-methylene-oct-1-ene
Conditions | Yield |
---|---|
With N-Bromosuccinimide; sulfuric acid In 1,4-dioxane Ambient temperature; | 96% |
7-methyl-3-methene-1,6-octadiene
4-Methoxybenzyl alcohol
1-(4-methoxyphenyl)-2,7-dimethyl-3-methyleneoct-6-en-1-one
Conditions | Yield |
---|---|
With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); trifluoroacetic acid In toluene at -78 - 110℃; Inert atmosphere; regioselective reaction; | 96% |
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)palladium(II); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; under 30003 - 67506.8 Torr; for 20h; Inert atmosphere; Autoclave; | 96% |
7-methyl-3-methene-1,6-octadiene
1,2-bis-(p-methylphenylsulfonamido)-benzene
Conditions | Yield |
---|---|
With oxygen; palladium diacetate In acetonitrile at 70℃; under 760.051 Torr; for 48h; Sealed tube; Molecular sieve; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With [(2,6-iPr2PhBDI)Mn(μ-H)]2 In benzene-d6 at 130℃; for 48h; Inert atmosphere; | 96% |
7-methyl-3-methene-1,6-octadiene
(1Z,5Z)-1,6-bis(4-methylpent-3-en-1-yl)cycloocta-1,5-diene
Conditions | Yield |
---|---|
With [(MePI)FeCl(μ-Cl)]2; (butadiene)magnesium(THF)2 In neat (no solvent) at 23℃; for 3h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube; regioselective reaction; | 96% |
diazomethane
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
Stage #1: 7-methyl-3-methene-1,6-octadiene With benzophenone In diethyl ether at 20℃; Stage #2: diazomethane In diethyl ether at 20 - 35℃; for 1.5h; | 95.19% |
diiron nonacarbonyl
7-methyl-3-methene-1,6-octadiene
(η4-myrcene)tricarbonyliron
Conditions | Yield |
---|---|
In benzene Sonication; addn. of 1.1 equivalents of Fe2(CO)9 to a soln. of the diene in benzene, sonication for 1h or until all solid Fe2(CO)9 had disappeared, concn. of the soln.;; chromatography (SiO2, eluation with petroleum ether/ether); | 95% |
7-methyl-3-methene-1,6-octadiene
ethene
(Z)-2-methyl-6-(3-propenyl)-octa-2,6-diene
Conditions | Yield |
---|---|
With CoCl2(1,4-bis(diphenylphosphino)butane); trimethylaluminum In dichloromethane; toluene at 0℃; under 760.051 Torr; for 6h; Reagent/catalyst; regioselective reaction; | 95% |
With C30H40FeN2 In pentane at 23℃; for 6h; Inert atmosphere; Schlenk technique; Glovebox; regioselective reaction; | 92% |
With CoCl2(1,4-bis(diphenylphosphino)butane); trimethylaluminum In dichloromethane; toluene at 0℃; under 760.051 Torr; for 0.0833333h; Inert atmosphere; | 97.1 mg |
Conditions | Yield |
---|---|
With carbonyldihydridotris(triphenylphosphine)ruthenium(II); trifluoroacetic acid In toluene at 110℃; for 18h; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
With C37H47FeN5 at 23℃; for 48h; Diels-Alder Cycloaddition; stereoselective reaction; | 95% |
7-methyl-3-methene-1,6-octadiene
4-bromo-2'-hydroxylchalcone
Conditions | Yield |
---|---|
Stage #1: 4-bromo-2'-hydroxylchalcone With (2R)-(+)-3,3'-diphenyl-[2,2'-dinaphthalene]-1,1'-diol; α,α,α-trifluorotoluene; triphenylborane at 100℃; for 1h; Stage #2: 7-methyl-3-methene-1,6-octadiene for 9h; Reflux; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
In toluene at 50℃; for 144h; | 94% |
7-methyl-3-methene-1,6-octadiene
1-benzyl-3-hydroxy-5-methylindolin-2-one
(E)-1-benzyl-3-(3,7-dimethylocta-2,6-dien-1-yl)-3-hydroxy-5-methylindolin-2-one
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium; tricyclohexylphosphine In toluene at 110℃; for 48h; Inert atmosphere; Sealed tube; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With carbonyldihydridotris(triphenylphosphine)ruthenium(II); trifluoroacetic acid In toluene at 110℃; for 18h; Schlenk technique; | 94% |
Conditions | Yield |
---|---|
With C28H32N2; sodium triethylborohydride; iron(II) chloride In tetrahydrofuran at 20 - 40℃; for 2h; Inert atmosphere; Sealed tube; regioselective reaction; | 94% |
7-methyl-3-methene-1,6-octadiene
Conditions | Yield |
---|---|
With naphthalene-1,8-trisulfide-2-oxide In chlorobenzene for 6h; Heating; | 93% |
With bicyclo[3.3.1]nonylidenebicyclo[3.3.1]nonanethiirane 1-oxide In toluene Cycloaddition; Heating; | 68% |
With dimethyl acetylenedicarboxylate In dichloromethane at 20℃; for 0.5h; | 27% |
7-methyl-3-methene-1,6-octadiene
β-naphthol
3',3'-dimethyl-1,2-dihydrospiro[benzo[f]chromene-3,1'-cyclohexane]
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper(II) bis(trifluoromethanesulfonate) In 1,2-dichloro-ethane at 50℃; for 18h; | 93% |
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